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contrAA 600
Analytik Jena contrAA 600 User Manual
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contrA
A 600
HR-CS Atomic
Absorption Spec
trometer
Operating
manual
2
Table of Contents
Default Chapter
3
Table of Contents
3
1 Basic Information
6
Intended Use
6
User Manual Notes
6
2 Safety Instructions
8
General Safety Instructions
8
Warning Signs on the Contraa 600
13
Fig. 1 Warning Signs on the Contraa 600
14
3 Specification
15
Technical Data
15
Data on Contraa 600
15
Control Computer Data
17
Graphite Tube Technique Data
17
Data for Hydrea Technique Accessories
18
Guidelines and Standards
19
4 Installation Conditions
20
Environmental Conditions
20
Space Requirement and Weight
21
Energy Supply
21
Gas Supply
22
Exhaust Unit
23
Device Layout and Space Requirement
24
Fig. 3 Dimensions of the Contraa 600 - Top View
25
Fig. 4 Installation Layout of the Contraa 600
25
Functions and Setup of the Contraa 60024
26
Physical Measuring Principle HR-CS AAS
26
Fig. 5 Schematic Comparison of the Physical
26
Aas
26
Fig. 6 Beam Path in the Contraa 600
27
Xenon Lamp
28
Fig. 7 Xenon Lamp Without Housing
28
Electrothermal Atomizer
29
Fig. 8 Electrothermal Atomizer - Graphite Tube Furnace
29
Graphite Tube Furnace
30
Fig. 9 Graphite Tube Furnace
30
Gas Flows in the Graphite Tube Furnace
31
Fig. 10 Inner and Outer Gas Flows in the Graphite Tube Furnace
31
Graphite Tube Variations, Furnace Parts and Inserts
32
Fig. 11 Graphite Tube Furnace
32
Fig. 12 Graphite Tube Variations
32
Radiation Sensor
33
Furnace Camera
33
Fig. 13 Furnace Jacket, Adapters and Inserts
33
Accessories for the Graphite Tube Technique
34
Autosampler AS-GF
34
Fig. 14 Autosampler AS-GF
34
Solid Sampler SSA 600 and SSA 6Z
35
Fig. 15 Solid Sampler
35
Supplementary Accessories
36
Mercury/Hydride Systems for Hydrea Technique
36
Autosampler AS-F and AS-FD for Hydrea Technique
36
Fig. 16 Autosampler AS-FD with Separate Fluidik Module
37
6 Installation and Start-Up
38
Supply and Control Connections
38
Connections on the Right Side of the Contraa 600
38
Setting up the Contraa 600
39
Fig. 17 Mains Switch and Bar for Supply and Control Fig
39
Fig. 18 Bar for Supply and Control Connections
39
Electricity as Well as the Fuse Holders
39
Installation and Start of the Aspect CS Program
40
Graphite Tube Technique
41
Connections in the Sample Chamber for the Graphite Tube Technique
41
Fig. 19 Rear View of the Contraa 600 with Fig
41
Fig. 21 Connections at the Graphite Tube Furnace
41
Software Presets for the Graphite Tube Technique
42
Elements in the Sample Chamber for the Graphite Tube Technique
42
Fig. 23"Main Settings" Window for Graphite Tube Technique
42
Inserting the Graphite Tube into the Graphite Tube Furnace
43
Fig. 20 Graphite Tube Atomizer in Sample Chamber39 Fig
43
Furnace / Control" Window
43
Graphite Tube Furnace Opened with Inserted Graphite Tube
44
Formatting the Graphite Tube
45
Cleaning the Graphite Tube / Cleanout
45
Complete and Install the AS-GF Autosampler44
46
Installing the AS-GF
46
Installing the AS-GF
47
Adjusting the AS-GF
48
Aligning the AS-GF with the Furnace Using the Set Screw and Adjusting Screw 1
48
AS-GF Adjustment
49
Populating the Sample Tray of the AS-GF
50
Uninstalling the Autosampler AS-GF
50
Notes on Installing the Automatic Solid Autosampler SSA 600
51
Attaching Holding Pin and Crossbar to the AS-GF Support in the Sample Chamber
51
Installations for Hydrea Operation
52
Hydrea System HS 60 Modular
52
Rear of the Autosampler AS-FD
53
Starting up the Contraa 600 with Accessories52
54
Dosing Unit at the Fluidik Module of the AS- FD
54
7 Care and Maintenance
56
Maintenance Overview
56
Base Device
57
Replacing the Fuses
57
Reactivating the Safety Circuits of the Cooling Water Circuit
58
Cleaning the Sample Chamber
59
Removing and Installing the Xenon Lamp
59
Safety Circuit Switch for Hardware
59
Check the Cooling Water Level
61
Xenon Lamp Housing
61
Xenon Lamp, Installed
61
Cooling Water Container under the Graphite Tube Furnace
61
Maintaining the Graphite Tube Furnace
62
Cleaning the Furnace Windows
62
Cleaning the Graphite Surfaces
63
Identical Markings at the Furnace Windows Facing Upward
63
Cleaning and Changing the Graphite Tube
64
Replacing the Electrodes and the Furnace Jacket
64
Furnace Tools
64
Autosampler AS-GF
69
Washing the Dosing Tube
69
Servicing the Dosing Tube
70
Window "Autosampler / Function Tests" in the Aspect CS Software
70
Dosing Tube at the AS-GF
71
Replacing the Metering Syringe
73
Dosing Unit at AS-GF and AS-FD
73
Automatic Samplers AS-F, AS-FD
74
Washing the Mixing Cup of the AS-FD
74
Replacing the Canulas and Guide on the Autosampler Arm
74
Replacing the Intake Tube
75
Replacing the Tube Set for Diluent and Washing Liquid
75
Clean-Up after Cup Overflow
75
8 Transporting the Contraa 600
76
9 Waste Disposal
77
10 Abbreviations / Terms
78
11 Index
80
12 EC Declaration of Conformity
82
4
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Analytik Jena contrAA 600 Specifications
General
Brand
Analytik Jena
Model
contrAA 600
Category
Laboratory Equipment
Language
English
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