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Analytik Jena multi N/C 3100 User Manual

Analytik Jena multi N/C 3100
29 pages
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Bedienungsanleitung/Operating Manual
Manuelles TIC-Feststoffmodul
Manual TIC solids module
multi N/C 3100/2100S/UVHS

Table of Contents

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Analytik Jena multi N/C 3100 Specifications

General IconGeneral
Power Supply230 V, 50/60 Hz
Measurement PrincipleHigh-temperature catalytic combustion
Detection MethodNDIR (Non-Dispersive Infrared Spectroscopy), CLD (Chemiluminescence Detector)
Sample TypesLiquid, Solid
Carrier GasOxygen

Summary

Basic Information

Safety Instructions

Safety Instructions for Handling Ortho-Phosphoric Acid

Detailed safety guidelines for handling concentrated ortho-phosphoric acid during analysis.

Technical Data

Analytical Method of Measuring TIC

Explains the process of measuring Total Inorganic Carbon (TIC) using acid addition and CO2 detection.

Manual TIC Solids Module Setup

TIC Reaction Chamber

Details the setup of the Erlenmeyer flask and TIC head for the reaction.

Flow Setting of Carrier Gas

Instructions on setting the carrier gas flow using the "O2" needle valve and measuring glass.

Supply of Acid

Describes the process of metering phosphoric acid using the metering pump and valve.

Measuring Gas Drying and Cleaning

Explains the function of the drying tube, water traps, and halogen trap for gas purification.

Connections

Identifies the power input, gas output, and carrier gas connections on the module.

Operation

Preparing Module and Analyzer

Steps for connecting the manual TIC solids module to the basic unit analyzer.

Performing a TIC Measurement

Detailed procedure for conducting a TIC measurement, including sample handling and parameter settings.

Maintenance and Care

Maintenance Intervals

Lists the recommended frequency for various maintenance tasks like cleaning and component replacement.

Changing Desiccant in Drying Tube

Step-by-step guide on how to replace the desiccant in the drying tube.

Replacing the Halogen Trap

Instructions for replacing the copper and brass wool in the halogen trap.

Cleaning the TIC Reactor

Details the process for rinsing and drying the TIC reactor (Erlenmeyer flask) after use.

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