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novAA 800
Analytik Jena novAA 800 User Manual
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O
peratin
g Manual
nov
AA
80
0
Atomic Ab
sorption
S
pectrometer
2
Table of Contents
Default Chapter
3
Table of Contents
3
1 Basic Information
7
Notes on this User Manual
7
Intended Use
8
Warranty and Liability
8
2 Safety Instructions
9
General Notes
9
Safety Labeling on the Device
9
Fig. 1 Safety Markings on the Rear of the Device
9
Fig. 2 Safety Markings on the Front and Side Panels of the Device
10
Requirements for the Operating Personnel
11
Safety Instructions, Transport and Installation
11
Safety Instructions for Operation
12
Safety Instructions for Electrical Equipment
12
Hazards Associated with the Operation of the Flame and the Graphite Furnace
13
Safety Instructions Relating to the Formation of Ozone and Toxic Vapors
14
Safety Instructions for Compressed Gas Cylinders and Systems
14
Handling of Samples, Auxiliary and Operating Materials
15
Decontamination in Case of Biological Contamination
16
Behavior During Emergencies
16
Safety Instructions: Service and Repair
17
3 Function and Setup
18
AAS Techniques
18
Fig. 3 Sample Chamber of the Novaa 800 D
18
Optical Principle
19
Fig. 4 Sample Chamber of the Novaa 800 F
19
Fig. 5 Optical Diagram of the Novaa 800
20
Measurement Principle
21
Lamp Turrets and Lamps
21
Electrothermal Atomizer
22
Fig. 6 Lamp Turret with Reader
22
Fig. 7 Graphite Furnace in the Sample Chamber
23
Graphite Tube Furnace
24
Fig. 8 Graphite Furnace, Opened
24
Gas Flows in the Furnace Shroud
25
Fig. 9 Inner and Outer Gas Flows in the Graphite Furnace
25
Graphite Tube Variations, Furnace Parts and Inserts
26
Fig. 10 Graphite Furnace Shroud
26
Fig. 11 Variants of the Graphite Tube
26
Radiation Sensor
27
Furnace Camera
27
Accessories for the Graphite Tube Technique
27
Autosampler AS-GF
27
Fig. 12 Furnace Shroud, Adapters and Inserts
27
Mobile Cooling Unit KM 5
28
Fig. 13 Autosampler AS-GF
28
Flame System
29
Automatic Gas Control
29
Burner-Nebulizer System
30
Fig. 14 Nebulizer-Mixing-Chamber-Burner-System
31
Burner and Flame Type
32
Fig. 15 Mixing Chamber and Nebulizer, Disassembled
32
Sensors
33
Accessories for Flame Technique
33
Autosamplers AS-F and AS-FD
33
Fig. 16 Burner Types
33
Fig. 17 Autosampler AS-FD with Separate Fluidics Module
34
Piston Compressor PLANET L-S50-15
35
Injection Module SFS 6
35
Scraper - Automatic Cleaner of the Burner Head
36
Fig. 18 Injection Module SFS 6
36
Optional Accessory - Air Purge Kit
37
3.10 Optional Accessory - Hydride Systems
37
Fig. 19 Scraper Mounted to a 50-MM Burner Head
37
4 Installation and Initial Start-Up
38
Installation Conditions
38
Environmental Conditions
39
Energy Supply
40
Gas Supply
41
Exhaust Unit
42
Space Requirement, Weight and Device Layout
43
Fig. 20 Dimensions of the Novaa 800 - Front View
45
Fig. 21 Dimensions of the Novaa 800 (with AS-FD and Fluidics Module)
45
Fig. 22 Dimensions of the Novaa 800 (with Autosampler AS-GF)
46
Fig. 23 Installation Diagram Novaa 800 with Exhaust Unit
47
Supply and Control Connections
48
Fig. 24 Novaa 800 - Side View with Carrying Handles
48
Removing the Transport Locks
51
Placing and Connecting the Novaa 800
53
Installing and Starting the Aspect LS Software
53
Loading the Lamp Turret and Adjusting the Lamps
53
Removing and Installing the Hollow Cathode Lamp
55
Removing and Installing the Deuterium Hollow Cathode Lamp
55
Configuring the Lamp Turret in Aspect LS
56
Adjusting the Lamps
58
Changing the Atomization Technique
60
Graphite Tube Technique
62
Connections in the Sample Chamber for the Graphite Tube Technique
62
Default Settings in the Software for the Graphite Technique
63
Inserting the Graphite Tube into the Furnace
65
Formation of the Graphite Tube Furnace
67
Cleaning / Baking out the Graphite Tube
68
Installing and Adjusting the Autosampler AS-GF
68
Installing the Autosampler
68
Adjusting the Sampler
71
Loading the Sample Tray
72
Uninstalling the Autosampler
73
4.10 Installing the Flame Technique
74
4.10.1 Connections in the Sample Chamber for the Flame Technique
74
4.10.2 Software Presettings for the Flame Technique
75
4.10.3 Installation for Manual Sample Introduction
75
4.10.4 Installation for Continuous Operation / Sample Introduction Via Autosampler
77
Installing the Injection Module SFS 6
81
4.10.6 Replacing the Burner
82
4.10.7 Installing the Scraper
82
4.11 Starting up the Novaa 800 with Accessories
83
4.11.1 Switching on Sequence
83
4.11.2 Switching off Sequence
84
5 Service and Maintenance
85
Maintenance Overview
86
Maintaining the Basic Device
88
Replacing the Fuses
88
Cleaning the Sample Chamber
89
Checking the Gas Connections for Leaks
89
Graphite Tube Furnace
89
Cleaning the Furnace Windows
90
Cleaning the Graphite Surfaces
91
Cleaning and Changing the Graphite Tube
91
Replacing Electrodes and Furnace Shroud
92
Burner-Nebulizer System
98
Taking the Burner-Nebulizer System Apart
99
Cleaning the Burner
101
Cleaning the Nebulizer
102
Cleaning the Mixing Chamber
102
Cleaning the Siphon
103
Assembling the Burner-Nebulizer System
103
Aligning the Atomizer Within the Beam Path
105
Cleaning the Sensor for Burner Detection
106
Autosampler Graphite AS-GF
106
Purging the Dosing Tube
107
Servicing the Dosing Tube
108
Replacing the Dosing Syringe
110
Cleaning the Autosampler after Cup Overflow
111
Autosamplers AS-F, AS-FD
111
Washing the Sample Path
111
Washing the Mixing Cup of the AS-FD
112
Replacing the Cannulas and Guide on the Autosampler Arm of the AS-FD
112
Replacing the Cannula on the Autosampler Arm of the AS-F
113
Replacing the Intake Tube
113
Replacing the Tube Set on the AS-FD
113
Cleaning up after Cup Overflow
114
Cooling Unit KM 5
114
Piston Compressor PLANET L-S50-15
115
6 Troubleshooting
116
Troubleshooting According to Software Messages
116
Equipment Faults and Analytical Problems
119
7 Transport and Storage
122
Preparing the Novaa 800 for Transport
122
Ambient Conditions for Transport and Storage
123
8 Disposal
124
9 Specification
125
Technical Data
125
Data on the Novaa 800
125
Minimum Requirements of the Aspect LS Software
129
Data for the Graphite Tube Technique
130
Data for the Flame Technique
131
Accessories Data
132
Guidelines and Standards
134
10 CE Declaration of Conformity
135
11 Index
136
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Analytik Jena novAA 800 Specifications
General
Brand
Analytik Jena
Model
novAA 800
Category
Laboratory Equipment
Language
English
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