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ATAGO AP-300 User Manual

ATAGO AP-300
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P-OQ0612-5291-E03
1/7
Operational
Qualification (OQ
Automatic Polarimeter
AP-300
Operational Qualification of Automatic Polarimeter AP-300
Preface
The Operational Qualification performance test of the Automatic Polarimeter AP-300 is d escribed
herewith.
The instructions below assume that the performance test of the AP-300 is condu cted by a regular
user of the unit who is familiar with the operation. For daily check and maintenance, please refer
to the Standard Operational Procedure document (SOP).
1. Test Environment and Preparation
Conduct the performance test in an environment which meets the conditions outlined below.
Keep the measurement sample and the AP-300 at an am bient tem perature of 18.0°C to 22.0°C
for at least 30 minutes to let them acclimate to the ambient temperature.
If the following environmental conditions are not met, an appropriate measurement result
may not be obtained.
Environment for performance test
2. Establishing a Discretionary Measurement Standard
A performance test requires a discretionary measurement standard.
Establish a set measurement standard for your samples, taking the accuracy of the AP-300
into accou nt. Please refer to the product literature and/ or the instruction manual for the
specifications, features, and measurement accu racy of the AP-300. These sp ecifications are
guaranteed at the time the AP-300 is shipped as a brand-new product. It is d ifficu lt to obtain
an accuracy level greater than the prod u ct sp ecifications under different environmental
conditions. It is recommended setting the discretionary measurement standard lower than the
stated specifications.
Example: Judgment standard measurement
Accuracy: Angle of rotation ±0.03°
3. Confirmation of Measurement Accuracy (Accuracy and Repeatability)
Check the accuracy (accuracy and repeatability) of the m easurement values by measuring a
sample of a known concentration.
The AP-300 is an optical instrument designed to measure the angle of rotation of a sample
solution by utilizing two polarizing plates.
Ambient temperature: 18.0°C to 22.0°C Relative humidity: less than 75%
Power supply: AC 100 to 240V, 50/ 60Hz
The Automatic Polarimeter AP-300 should be used indoors and placed on a flat,
level surface, such as a work desk or laboratory table.
Question and Answer IconNeed help?

Do you have a question about the ATAGO AP-300 and is the answer not in the manual?

ATAGO AP-300 Specifications

General IconGeneral
ModelAP-300
Measurement Range (Refractive Index)1.3000 to 1.7000
Resolution (Refractive Index)0.0001
Minimum Indication (Optical Rotation)0.01°
Measurement Wavelength589 nm
Measurement Range (Brix)0.0 to 95.0%
Resolution (Brix)0.1%
Accuracy (Brix)±0.1 %
DisplayLCD
Light SourceLED
Temperature CompensationAutomatic
Sample Volume0.3 mL
Power SupplyAC adapter or battery
BatteryLithium-ion

Summary

Test Environment and Preparation

Environment for performance test

Specifies ambient temperature, power supply, and humidity for testing.

Establishing a Discretionary Measurement Standard

Judgment standard measurement example

Provides an example of setting accuracy standards for measurements.

Confirmation of Measurement Accuracy

Accuracy and Repeatability

Describes checking accuracy and repeatability using known concentration samples.

Items to Prepare

Standard quartz control plate (with traceability certificate)

Lists ATAGO part numbers for quartz control plates used for calibration.

Standard sucrose solution preparation

Details how to prepare a 100°Z standard sucrose solution for measurements.

Recording chart for measurement data

Mentions the need for a recording chart for measurement data.

Preparation of Instrument

Instrument setup and checks

Outlines initial steps for powering on, setting mode, date, time, and printer.

Measurement

Measurement procedure

Instructions for zero-setting and measuring quartz plates or sucrose solutions.

Confirmation of Recorded Data

Data verification and memory recall

Explains how to check recorded data consistency with printer output and memory.

Operation Qualification Results Report

Report filling and assessment

Steps for filling out the report, calculating errors, and assessing results.

Preparation of Instrument

Instrument connection and setup

Covers instrument connection, power-on, mode setting, and printer checks.

Items to Prepare

Standard quartz control plate

Lists standard quartz control plates or sucrose solutions needed for function tests.

Function Examination

Key Functions in Each Mode

Details navigating menus using the MENU, cursor, and ENTER keys.

Error Messages

ZERO SET ERROR

Explains the condition for a ZERO SET ERROR during zero-setting.

OUT OF RANGE

Describes how to trigger and interpret the OUT OF RANGE error message.

TEMP. ERROR

Details the steps to cause and identify a TEMP. ERROR.

Password Function

Default password and system level

Describes the default password and system level settings for security.

SYSTEM LEVEL

System Level check

Instructions to verify the SYSTEM LEVEL is set to 0.

Operation Qualification Results Report

Performance Test Data

Section for recording standard values, test results, average, and difference.

Function Examination

A checklist for evaluating switch, key, display, error, and output functions.

Evaluation

Fields for Pass/Fail evaluation and signatures of operator and supervisor.

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