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Beckman Coulter SA 3100 Series User Manual

Beckman Coulter SA 3100 Series
166 pages
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Beckman Coulter SA 3100 Series Specifications

General IconGeneral
Power Requirements100-240 VAC, 50/60 Hz
Adsorptive GasNitrogen
Surface Area Range0.01 m²/g to no upper limit
Number of analysis ports1
Measurement PrincipleVolumetric method
Measurement TimeVaries depending on the sample and analysis conditions
Light SourceNot applicable
Operating Humidity20% to 80% non-condensing
CategorySurface Area and Pore Size Analyzer

Summary

About This Manual

General Manual Overview

Manual overview, operating, and maintenance instructions for the SA 3100 analyzer.

Conventions Used in This Manual

Explains conventions for touch-screen interface, messages, and key graphics.

Content of the Manual

Lists chapters and their primary topics covered in the manual.

Precautions and Hazards

General Safety Precautions

Hazards of compressed gases, cryogenic liquids, and general warnings.

Liquid Nitrogen Hazards and Precautions

Details potential hazards and safety measures when handling liquid nitrogen.

Compressed Inert Gas Hazards and Precautions

Outlines risks and safety practices for compressed nitrogen and other inert gases.

Installation and Setup

General Installation Overview

Introduces the installation process, scheduling, and key considerations.

Special Requirements

Lists environmental, electrical, gas, and hardware requirements for installation.

Unpacking and Hardware Setup

Procedures for unpacking the instrument and basic hardware setup.

Vacuum Pump Installation

Step-by-step guide for installing the vacuum pump, including oil and filter.

Gas Supply and Pressure Regulators

Instructions for connecting gas supply, optional regulators, and purging lines.

Saturation Tube and Power-Up

Installing the saturation tube and powering up the analyzer.

Flushing Gas Lines and Printer Installation

Procedures for flushing gas lines and installing a printer.

Advanced Setup and User Interface

Overview of advanced setup options and the analyzer's user interface.

Introducing the SA 3100 Analyzer

System Overview and Function

Describes the analyzer's capabilities, system function, and sample analysis process.

Analyzer Components

Identifies and describes the main physical components of the SA 3100 analyzer.

User Interface Navigation

Explains how to use the touch screen, menus, and various screens.

Profile Management

Covers creating, editing, and deleting analysis profiles for the instrument.

Additional Features

Details optional features like mouse support and configuration kits.

Getting Started - Instrument Verification

Overview of Verification Process

Introduces instrument verification and the steps for sample analysis.

Analyzing the Sample

Outlines the six main steps involved in analyzing a sample.

Weighing Sample Tube Assembly

Procedure for accurately weighing the sample tube assembly.

Adding Sample to Tube

Instructions for adding the prepared sample into the sample tube.

Logging Sample Information

Process for entering sample details and parameters into the analyzer.

Outgassing Sample Procedure

Steps for connecting the sample tube and performing outgassing.

Weighing Outgassed Sample

Procedure for weighing the sample tube after the outgassing process.

Performing Sample Analysis

Steps to select a sample and initiate the analysis process.

Post-Analysis Procedures

Steps for removing the dewar and sample tube after analysis completion.

Reviewing Analysis Results

How to view and interpret specific surface area results on the analyzer screen.

Principles of Operation

Basic Concepts in Gas Sorption

Introduces fundamental concepts like adsorption, absorption, and isotherms.

Theory of Adsorption Measurement

Explains the theoretical basis for adsorption and desorption measurements and calculations.

Operating Instructions

SA 3100 Analyzer Procedures

Details all procedures for operating the SA 3100 analyzer.

SA 3100 Analyzer Configuration

Instructions for configuring settings like screen brightness and printer.

Profile Management

Covers creating, editing, deleting, and managing analysis profiles.

Optimal Sample Quantity Determination

Guidance on selecting the appropriate sample mass for accurate analysis.

Choosing Sample Tubes

Information on selecting the correct sample tube type and size.

Sample Preparation Steps

Covers weighing, adding sample, logging, and outgassing procedures.

Performing Sample Analysis

Steps for selecting and running sample analyses.

Printing and Data File Access

How to print results and access saved data files.

Advanced Setup Options

Details advanced configuration settings for the analyzer.

Cleaning and Maintenance Procedures

General Cleaning and Maintenance

Overview of frequency and general practices for cleaning and maintenance.

Cleaning Sample Tubes

Detailed procedure for cleaning and drying sample tubes.

Cleaning and Greasing O-rings

Instructions for maintaining O-rings on ports and fittings.

Vacuum Pump and Filter Maintenance

Procedures for checking vacuum pump oil, cleaning filters, and changing oil mist filters.

Changing Gas Cylinders

Step-by-step guide for replacing gas cylinders.

Specifications

Environmental Requirements

Specifies operating and storage environmental conditions.

Power Requirements

Lists electrical supply voltage, frequency, and power consumption.

Gas Requirements

Defines the purity and type of gases required for operation.

Measurement Specifications

Details measurement ranges, reproducibility, and resolution.

Vacuum Pump and Outgassing Specs

Specifies performance parameters for the vacuum pump and outgassing system.

Appendix A: Coulter SA-View Software

Software Overview and Installation

Introduction to SA-VIEW software and its installation process.

SA-View Program Structure

Describes the main window, menus, toolbars, and icons of the software.

Using the SA-View Program

Guide to opening files, viewing data, printing, and managing windows.

Appendix B: Outgassing Notes

General Outgassing Information

Provides general notes on sample preparation and the outgassing process.

Outgassing Parameters and Methods

Discusses temperature, time, and system comparisons for outgassing.

Vacuum vs. Flowing Gas Systems

Compares the effectiveness of different outgassing system types.

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