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Buchi Rotavapor R-100 User Manual

Buchi Rotavapor R-100
60 pages
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Rotavapor® R-100
Operation Manual
11593663E en

Table of Contents

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Buchi Rotavapor R-100 Specifications

General IconGeneral
TypeRotary evaporator
Rotation Speed20 - 280 rpm
Heating BathHB Digital (optional)
Temperature RangeUp to 180 °C
Power Supply230 V / 50 Hz
Bath TemperatureUp to 180°C
GlasswareVarious glassware configurations available (e.g., A, B, C, D, E, G)

Summary

About This Document

Warning Notices

Explains danger levels and signal words used in the manual.

Symbols

Introduces warning, mandatory, and other symbols used in the manual and on the device.

Languages and Trademarks

Information on instruction translations and trademark usage.

Safety

Intended Use and Prohibited Applications

Defines intended uses and lists applications that are not permissible.

Staff Qualification and Residual Risks

Specifies user qualifications and outlines potential hazards.

Protective Equipment and Modifications

Details necessary PPE and warns against unauthorized modifications.

Product Description

Function and Configuration Overview

Explains the rotary evaporation process and the R-100's general configuration.

Component Views and Interfaces

Details front/rear views, interfaces, and typical application setup.

Application and Type Plate

Illustrates system setup and explains device identification plate information.

Device Symbols and Specifications

Shows device symbols, lists supplied components.

Technical Data

Provides technical specifications for the unit, bath, ambient conditions, and materials.

Safety Features

Details safety mechanisms like overheat cut-out and overload protection.

Installation

Site Requirements and Mounting

Requirements for installation site and mounting the rotary drive unit.

Connecting System Components

Instructions for fitting vapor duct, condenser, stopcock, and tubing.

Electrical Connections and Overview

Details electrical hookups and provides an overview of system connections.

Heating Bath Setup and Quick Check

Instructions for filling the heating bath and performing a quick installation check.

Operation

Preparations and Adjustments

Steps to prepare the heating bath, fit flasks, and adjust angles.

Performing Distillation

Step-by-step guide for carrying out the distillation process.

Distillation Optimization and Control

Guides on flask height, distillation conditions, and process optimization.

Solvent Feeding and Finishing

Instructions for feeding solvent and finishing distillation.

Removing Flasks

Procedures for safely removing the evaporating and receiving flasks.

Cleaning and Servicing

Vapor Duct and Leak Checks

Inspecting and cleaning the vapor duct and checking the system for leaks.

Seals and Condenser Cleaning

Checking seals and cleaning the condenser.

Heating Bath and Solvent Removal

Cleaning the heating bath and removing solvent accumulations.

Help with Faults

Troubleshooting Guide

A guide to common faults, their causes, and remedies.

Safety Feature Resets

Instructions for resetting overheat cut-out and replacing fuses.

Taking Out of Service and Disposal

Decommissioning and Disposal Procedures

Procedures for safely decommissioning and disposing of the equipment.

Appendix

Solvent Table

A table listing various solvents with properties relevant to distillation.

Spare Parts and Accessories

Lists available spare parts, accessories, wear parts, and glass apparatus.

Abbreviations and Safety Information

Provides lists of abbreviations and health/safety approval requirements.

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