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Hitachi U-2910 User Manual

Hitachi U-2910
78 pages
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INSTRUCTION MANUAL
2J1-9006-009 Ver.10 October. 2020
Double Beam Spectrophotometer
MODEL U-2910 UV-VIS
SPECTROPHOTOMETER
(MAINTENANCE)

Table of Contents

Questions and Answers:

Hitachi U-2910 Specifications

General IconGeneral
BrandHitachi
ModelU-2910
CategoryMeasuring Instruments
LanguageEnglish

Summary

Preface and Manual Overview

About This Manual

Explains the manual's scope, structure, and recommended reading order for users.

Important Product Information

WEEE Compliance & Disposal (EU)

Instructions for WEEE compliance and proper disposal of the equipment in the European Union.

Disposal Guidance for Users Outside EU

Guidance on proper disposal methods for users outside the European Union.

Product Warranty Terms

Details the warranty terms, conditions, and exclusions for the product.

Warranty Limitations and Exclusions

Lists specific conditions and scenarios not covered by the free-of-charge warranty.

Warranty Disclaimer

Outlines the manufacturer's warranty limitations and disclaims implied warranties for specific purposes.

Instrument Service Life & Extended Use

Estimates the instrument's useful service life and requirements for extended use.

Instrument Installation, Relocation & After-Sales Service

Covers procedures for initial installation, relocation, and accessing after-sales technical support.

Technical Training Courses

Informs users about available technical training sessions offered by the manufacturer.

General Operational Precautions

Provides general safety and operational guidelines not covered in specific sections.

Chemical & Sample Handling Precautions

Details the user's responsibility and precautions for handling chemicals and samples safely.

Safety Summary and Alert System

General Safety Guidelines

Introduces the importance of reading and understanding safety instructions provided in the manual.

Understanding DANGER Alerts

Explains the meaning and severity of DANGER alerts, potentially leading to death or serious injury.

Understanding WARNING Alerts

Explains the meaning of WARNING alerts, indicating potentially hazardous situations resulting in death or serious injury.

Understanding CAUTION Alerts

Explains the meaning of CAUTION alerts, indicating hazardous situations leading to minor injury or product damage.

Understanding NOTICE Alerts

Explains the purpose of NOTICE alerts, focusing on preventing instrument/data damage or environmental pollution.

Pre-Operation Safety Checks

Provides essential safety steps and considerations to be followed before operating the instrument.

Safety During Operation

Details safety measures to be taken during the operation of the instrument.

Installation, Maintenance & Relocation Safety

Covers safety considerations specific to the installation, maintenance, and relocation processes.

Specific Installation Safety

Provides specific safety warnings related to the installation, maintenance, and relocation of the instrument.

Manual Safety Instructions Overview

Highlights the safety instructions contained within the manual and their relevance to the instrument.

High Voltage Shock Hazard (Internal)

Details the risk of electric shock from high voltage inside the instrument and precautions before accessing components.

Power Supply Shock Hazard

Describes the risk of electric shock from the power supply and the necessity of proper grounding and avoiding cover removal.

Fatigue & Hot Surface Burn Hazards

Details CAUTION warnings regarding long operation hours leading to fatigue and burns from hot surfaces.

Waste Disposal & Measurement Accuracy Notices

Provides NOTICE alerts for proper disposal of waste solutions and ensuring accuracy of measured values.

Data Backup Importance

Emphasizes the importance of backing up data to prevent loss due to system failures or virus infections.

Computer Virus Protection

Offers guidance on identifying and protecting against computer viruses that may affect the instrument's software and data.

Power Interruption Safety

Advises on protecting the instrument from data loss or damage due to momentary power interruptions using an UPS.

Personal Computer Power Management

Provides instructions on the correct procedure for powering the personal computer on and off to avoid data corruption.

Lithium Battery Safety

Warns about the hazards of lithium batteries and proper handling and replacement procedures.

Safe Instrument Handling & Moving

Details safety precautions for moving the heavy instrument, requiring two persons for safe handling.

Securing Instrument During Installation

Stresses the importance of securing the instrument during installation to prevent accidental falls and injuries.

Instrument Warning Label Guide

Explains the warning labels attached to the instrument and the need for periodic checks and replacement if illegible.

Instrument Caution Label Guide

Explains the caution label regarding hot parts and the necessary waiting time after power-off before handling.

Hot Surface Burn Hazard

Warns about the high temperature of lamps and hot surfaces, advising to cool down before replacement.

Instrument Installation Guide

Unpacking & Initial Placement

Provides instructions on how to unpack the instrument safely and place it for setup.

Installation Site Requirements

Defines the physical space requirements, including floor area and work table strength, for instrument placement.

Electrical Power Specifications

Specifies the required electrical power supply voltage, frequency, and source capacity for the instrument.

Environmental Installation Conditions

Defines the optimal operating temperature, humidity, atmosphere, and other environmental factors for the instrument.

Verify Delivered Contents

Instructs users to verify all delivered items against the packing list and report discrepancies.

Instrument Assembly Procedures

Provides step-by-step instructions for assembling the instrument, including a safety warning.

Earthquake Safety Measures

Explains how to secure the spectrophotometer to prevent damage from earthquakes using threaded screw holes.

Power Voltage & Fuse Check

Guides the user on checking the power voltage setting and selecting the correct fuse capacity for safe operation.

System Cable Connections

Details how to connect various cables for the instrument, computer, and printer, with a safety warning.

Power Cord & Grounding Wire Connection

Provides instructions for securely connecting the power cord and ensuring proper grounding of the instrument.

Post-Installation Inspection Checklist

Lists final checks to perform after installation and assembly to ensure correct setup.

Instrument Power-On Procedure

Describes the procedure for turning on the spectrophotometer's power switch.

UV-Solutions Software Installation

Directs users to the relevant section for installing the UV-Solutions software.

Shutting Down the Instrument

Outlines the steps for properly shutting down and terminating the instrument and associated software after use.

Spectrophotometer Functions and Features

Functional Overview

Provides a general overview of the spectrophotometer's capabilities for photometric analysis.

Instrument Physical Layout

Describes the physical appearance and features of the instrument, including sample compartment and side panel.

Front Panel Features

Describes the appearance and function of components on the front panel, including the RUN lamp.

Operational Principle

Explains the fundamental operational principle of the spectrophotometer.

Optical System Description

Explains the optical path of the spectrophotometer, from the light source through the monochromator to the detectors.

Signal & Control System

Describes how optical signals are converted, processed, and controlled, either via keyboard or PC.

Core Measurement Capabilities

Lists the primary measurement functions offered by the instrument.

Available Measurement Modes

Lists the available measurement modes offered by the UV Solutions program, including quantitative calculation and scans.

Quantitative Analysis Setup

Explains the function for calculating sample concentration by creating calibration curves from standards.

Wavelength Scanning Procedure

Details the parameters and capabilities for performing wavelength scans, including scan speed and data modes.

Time Scanning Procedure

Describes the Time Scan function, allowing measurements over a specified time interval and rate calculation.

Advanced Data Processing

Covers various data processing techniques like automatic readout, peak detection, and scale changing.

Spectral Smoothing

Explains the smoothing function to eliminate noise from spectral data.

Spectral Differentiation

Describes how to differentiate spectral data to analyze derivative orders and smoothing parameters.

Spectral Arithmetic Operations

Details applying arithmetic operations and coefficients to spectral data.

Data File Conversion

Explains converting data files into ASCII text or JCAMP-DX formats.

Display & Print Font Settings

Allows customization of font style and size for displaying and printing data.

Baseline Correction Methods

Explains how to perform baseline correction using system or user baselines to ensure accurate measurements.

Automated Calibration & Diagnostics

Lists the instrument's auto calibration and self-diagnosis features for maintaining accuracy.

Technical Specifications

Provides a comprehensive list of the technical specifications for the Model U-2910 spectrophotometer.

Instrument Calibration Procedures

Calibration Overview

Introduces the instrument calibration process, emphasizing vertical axis for 0%T and horizontal for wavelength.

Calibration Timing Notice

Advises on proper timing and order for calibration procedures, recommending a stabilization period.

Performing 0%T Measurement

Details the procedure for correcting the 0%T (zero absorbance) measurement for accurate sample readings.

Performing Wavelength Calibration

Explains how to perform wavelength calibration using the D2 lamp's emission line for accurate wavelength readings.

Wavelength Calibration Timing Note

Notes that wavelength calibration occurs automatically on startup but recommends re-calibration after stabilization for precise measurements.

System Baseline Measurement

Guides on memorizing the system baseline, a crucial step for consistent measurements.

Instrument Maintenance and Checkups

Maintenance & Checkup Guide

Outlines the importance of regular maintenance and checkups for maintaining instrument accuracy and longevity.

Importance of Maintenance

Explains that proper maintenance is key to ensuring the instrument's superlative accuracy and long-lasting performance.

Cleaning the Sample Compartment

Provides instructions for cleaning the sample compartment base in case of sample spills to maintain optical performance.

Cleaning the Instrument Cover

Details how to clean spills on the instrument cover using a soft cloth and mild detergent.

Cell Cleaning & Storage

Describes the proper method for washing, drying, and storing sample cells to maintain their integrity.

Instrument Lubrication

Mentions that the instrument is factory-lubricated and advises contacting service for abnormalities.

Cleaning Sample Compartment Window Plate

Explains the procedure for cleaning the transmission window plate of the sample compartment.

Performance Verification Procedures

Wavelength Accuracy Verification

Details the process for measuring D2 lamp emission lines to determine and check wavelength accuracy.

Wavelength Setting Repeatability Check

Explains how to measure wavelength repeatability by repeating measurements on a single emission line.

Bandpass Measurement

Describes the procedure to determine the spectral width of monochromatic light emitted from the monochromator.

Noise Level Measurement

Details how to measure the variation range of absorbance values over a short period with no sample to determine noise level.

Baseline Stability Check

Explains how to determine the variation range of absorbance values over time without a sample to check baseline stability.

Baseline Flatness Check

Details the procedure to determine systematic variations in absorbance values across a specified wavelength region.

Troubleshooting and Parts Replacement

Troubleshooting Common Issues

Provides a table of common instrument conditions, possible causes, and recommended actions for troubleshooting issues.

Electrical Hazard Warning

Warns users about the electrical hazard inside the instrument and advises that only qualified personnel should perform inspections.

Parts Replacement Introduction

Recommends keeping spare consumable parts on hand to minimize unintentional instrument downtime.

List of Consumable Parts

Lists the consumable parts for the instrument, including lamps and fuses, with part numbers.

Light Source Lamp Replacement

Provides instructions for replacing the light source lamps.

Lamp Replacement Steps

Provides step-by-step instructions for safely replacing the light source lamps, including necessary precautions.

Lamp Replacement Safety Warnings

Highlights critical safety warnings regarding electric shock and hot surfaces during lamp replacement.

WI Lamp Replacement Procedure

Details the specific procedure for removing and installing the WI lamp.

D2 Lamp Replacement Procedure

Details the specific procedure for removing and installing the D2 lamp.

Lamp Usage Timer Reset

Explains the need to reset the lamp turn-on time after replacement and refers to another volume for details.

Lamp Position Adjustment

Describes how to adjust the light source position if necessary, with safety precautions.

Lamp Adjustment Safety Precautions

Warns users about hot lamps and UV radiation during adjustment, advising protective measures.

WI Lamp Position Adjustment

Details the steps for adjusting the WI lamp's position to ensure proper illumination of the slit.

D2 Lamp Position Adjustment

Details the steps for adjusting the D2 lamp's position to ensure proper illumination of the slit.

Instrument Storage Guidelines

Provides guidelines for storing the instrument properly after use and for long-term periods.

Storage After Use

Provides instructions for proper storage of the instrument after completing measurements, including cover placement.

Long-Term Instrument Storage

Details precautions for long-term storage, including environmental conditions and securing the light source mirror.

Appendices on Spectrophotometry

Appendix 1: Absorption Spectrophotometry Theory

Explains the fundamental principles of absorption spectrophotometry and Bouguer-Beer's Law.

Appendix 2: Spectrophotometer Usage Notes

Provides notes on using the spectrophotometer, including solvent selection.

Solvent Selection Guide

Provides guidelines and a table for selecting appropriate solvents based on their spectral ranges and properties.

Handling Special Sample Types

Discusses handling special sample types like fluorescing samples or those with high turbidity, and provides an equation for solid samples.

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