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Spectrum 100 FT-IR
PerkinElmer Spectrum 100 FT-IR User Manual
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S
PECTRUM
100
S
ERIES
User’s Guide
MOLECULAR SPECTROSCOPY
2
Table of Contents
Default Chapter
3
Table of Contents
3
Contents
3
Introduction
5
About this Manual
6
Conventions Used in this Manual
7
Notes, Cautions and Warnings
7
Warning Signs on the Instrument
9
Warnings and Safety Information
11
Safety Summary
12
General Safety
13
Location and Ventilation
14
Electrical Safety
14
Laser Safety Regulations
16
Explanation of the Laser Radiation Hazard and Its Classification
17
Laser Apertures
18
Radiation Emitted by the Spectrum 100N FT-NIR
18
Labels
19
Spectrum 100 FT-IR and Spectrum 100N FT-NIR Laser Safety Labels
19
Product Identification Label
20
EMC Compliance
21
EC Directive
21
FCC Rules and Regulations
21
Use of Flammable Solvents and Samples
22
An Overview of the Spectrometers
23
A Guided Tour of the Spectrum 100 Series
24
Top Panel Controls
25
Sample Compartment
26
Power Switch and Communications Ports
27
Optical System
27
Accessories for the Spectrum Instrument
28
Unpacking and Installation
29
Requirements
30
Electrical Requirements
30
Environment
30
Unpacking the Spectrometer
31
Opening the Shipping Container
31
The Desiccant Indicator
33
Connecting up the Spectrometer
34
Connecting to the PC
34
Other Connectors
35
Connecting the Spectrometer to the Electrical Supply
37
Installing the Spectrum Software
38
Minimum PC Requirements
38
Installing Spectrum Software
38
The Instrument Install Wizard
39
Using the Instrument Install Wizard to Install an Accessory
48
Using the Spectrometer
53
Basics of Software Control
54
Switching on the Spectrometer
54
Controlling the Instrument
55
Working with the Instrument Display and Go Button
59
Using the Spectrum On-Screen Help System
60
Atmospheric (CO O) Suppression
61
What Is Atmospheric Suppression
61
What Does Atmospheric Suppression Do
61
AVI Correction
63
What Is AVI Correction
63
What Does AVI Correction Do
63
Look Ahead
64
What Is Look Ahead
64
What Does Look Ahead Do
64
Quality Checks
65
What Are Quality Checks
65
What Do Quality Checks Do
65
Quality Checks and the Multiple Sample Tab
65
Routine Maintenance
67
Cleaning the Spectrometer
68
Cleaning the Display
68
Moving the Spectrometer
69
Condensation
69
The Desiccant Indicator in Detail
70
Changing the Desiccant
71
Resetting the Desiccant Change Interval
72
Renewing the Disposable Desiccant
73
Installing Rechargeable Desiccant
75
Purging the Spectrometer
76
Changing the External Fuse
79
Cooling the MCT Detector (Spectrum 100)
81
Advanced Maintenance
83
Opening the Main Cover
84
Replacing the Source
87
Replacing the Beamsplitter
89
Installing/Replacing Windows
91
Installing Filters in the Filterwheel
93
Installing an AVI Cell in the Filterwheel Assembly
96
Replacing the Laser and Power Supply
97
Instrument Performance Validation
99
Performance Validation Kits
100
Principles of Use
100
Validating Instrument Calibration
101
Collecting the Reference Spectra
101
Printing the Certificate of Performance Validation
102
Possible Reasons for Validation Failure
104
Printing the Certificate
104
Re-Printing the Information on a Certificate
106
When Should I Recalibrate My Instrument
107
Appendices
109
Appendix 1: Changing the Sampling Accessory
110
Appendix 2: Instrument Self-Checks
113
Appendix 3: WEEE Instructions for Perkinelmer Products
115
Index
116
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PerkinElmer Spectrum 100 FT-IR Specifications
General
Brand
PerkinElmer
Model
Spectrum 100 FT-IR
Category
Measuring Instruments
Language
English
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