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SP Scientific VIRTIS 2K - User Manual

SP Scientific VIRTIS 2K
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FREEZE DRYER OPERATOR’S MANUAL
VIRTIS BENCHTOP 2K, 4K AND 6K
FREEZE DRYERS

Table of Contents

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Summary

Introduction to VirTis Bench Top Freeze Dryers

Features, Usage, and Cold Trap Module

Covers unit features, basic usage, and the condenser's role as a cold trap.

Installation and Startup Guide

Initial Inspection and Service Connections

Guides on shipment inspection, damage handling, and electrical service connections.

Vacuum Pump Installation and Setup

Details vacuum pump installation, connection, and basic bench top unit setup.

Vacuum Baffle Plate Functionality

Explains the two positions of the vacuum baffle plate and their usage.

Freeze-Drying Concepts Explained

Overview and Elements of Freeze-Drying

Introduces the freeze-drying process phases and its four key elements: Freeze, Vacuum, Heat, Condenser.

Heat, Condenser, and Product Dependencies

Explains heat application, condenser function, and how product affects the drying process.

Sentry 2.0 Control System

LED Display and Button Functions

Describes the LED wave display for status and the functions of control panel buttons.

LCD Display, Menu Navigation, and Vacuum Control

Details the LCD display, menu navigation, and vacuum level control settings.

Maintenance, Alarms, and Setpoints

Covers vacuum pump maintenance, alarm management, and setpoint adjustments.

Calibration Procedures for Temperature and Vacuum

Outlines the steps for calibrating temperature and vacuum settings.

Basic Operation Procedures

Getting Started and Product Preparation

Outlines initial steps and sample preparation for flask/manifold and drum/shelf drying.

Operation Instructions and Meltback Prevention

Provides step-by-step operating procedures and guidance on preventing product meltback.

Glassware Breakage and Stoppering Options

Offers tips to prevent glassware breakage and details the optional stoppering process.

Cold Trap Condenser Applications

Overview and Product Requirements

Explains cold trap function and factors to consider for solvent condensation.

Cold Trap Setup Guide

Guides on configuring the Bench Top unit for cold trap applications.

Optional Components for Versatility

Manifolds and Shelf Racks

Describes various available manifolds and shelf racks for different drying configurations.

Liquid Nitrogen Trap, Filter Trap, and Cold Plate

Details optional Liquid Nitrogen Trap, Filter Trap, and Bench Top Cold Plate.

General Maintenance Procedures

Vacuum System and Pump Oil Maintenance

Covers vacuum pump checks, oil changes, and the maintenance alarm.

Tubing, Gaskets, and Quickseal Valves

Guides on inspecting and maintaining vacuum tubing, gaskets, and Quickseal valves.

Condenser and Airflow System Cleaning

Provides instructions for cleaning the condenser, chamber, and ensuring proper airflow.

Appendix A: Troubleshooting Common Issues

Vacuum Problems and Product Melting Solutions

Offers solutions for common vacuum issues and addresses product melting causes.

Appendix B: Serum Vial Capacities

Serum Vial Part Numbers and Capacities

Lists various serum vial part numbers, dimensions, and capacities for reference.

Appendix C: Stainless Steel Cleaners

Stainless Steel Cleaners and Application Methods

Provides a guide to cleaning stainless steel surfaces and their chemical resistance.

SP Scientific VIRTIS 2K Specifications

General IconGeneral
ModelVIRTIS 2K
TypeFreeze Dryer
Shelf SizeVaries depending on configuration
Vacuum ControlAutomatic
Shelf AreaVaries depending on configuration
Shelf Temperature Uniformity±1°C
Cooling Rate1°C/min
Heating Rate1°C/min
Condenser Temperature-55°C

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