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TA Instruments Q1000 Getting Started Guide
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Revision
N
Issued
January
2007
Q Series
TM
Getting Started Guide
DSC
Differential Scanning
Calorimeter
2
Table of Contents
Default Chapter
3
Important: TA Instruments Manual Supplement
3
Table of Contents
4
Notes, Cautions, and Warnings
7
Regulatory Compliance
8
Safety Standards
8
Electromagnetic Compatibility Standards
8
Safety
9
Instrument Symbols
9
Electrical Safety
9
Handling Liquid Nitrogen
10
Thermal Safety
11
Lifting the Instrument
11
Chapter 1: Introducing the DSC
13
Overview
13
DSC System Components
14
DSC Cell
14
Cooling Accessories
15
Finned Air Cooling System (FACS)
15
Refrigerated Cooling System (RCS)
16
Quench Cooler
17
Liquid Nitrogen Cooling System (LNCS)
17
The DSC Q2000/Q200 Touch Screen
18
Primary Function Keys
18
Control Menu
19
Display Touch Screen Options
21
The DSC Q1000/Q100 Touch Screens
22
Primary Function Keys
22
DSC Control Menu Keys
23
Display Menu Keys
24
DSC Auto Q20/Q20/Q10 Keypad
25
Options and Accessories
26
Tzero Sample Encapsulating Press
26
DSC Autosampler
26
Photocalorimeter Accessory (PCA)
26
DSC Pressure Cell
27
Instrument Specifications
28
DSC Instrument Characteristics
28
Chapter 2: Installing the DSC
31
Unpacking/Repacking the DSC
31
Installing the Instrument
31
Inspecting the System
31
Choosing a Location
32
Connecting Cables and Lines
33
Ports
33
Ethernet Switch Setup
35
Purge Lines
37
Cooling Gas Line
38
Base Purge Line
38
Voltage Configuration Unit
39
Power Switch
40
Power Cable
40
Starting the DSC
40
Shutting down the DSC
41
Installing the DSC Cooling Accessories
42
Installing the Finned Air Cooling System
42
Installing the Quench Coolers
43
Quench Cool Accessory for FACS
43
Quench Cooler
44
Installation of Additional Items
46
Installing the Manual Lids
46
Installing the Autosampler Tray and Dust Cover
46
Chapter 3: Use, Maintenance, & Diagnostics
47
Using the DSC
47
Before You Begin
47
Calibrating the DSC
48
Tzero TM
49
Baseline Slope and Offset Calibration
49
Enthalpy (Cell) Constant Calibration
50
Temperature Calibration
50
Heat Capacity (Q2000/Q1000) Calibration
50
Heat Capacity (MDSC ® ) Calibration
50
Pressure Calibration
51
Autosampler Calibration
51
Q2000/Q200/Auto Q20 Autosampler Calibration
51
Q1000/Q100 Autosampler Calibration
53
Running a DSC Experiment
54
Experimental Procedure
54
Loading the Sample
55
Starting an Experiment
55
Stopping an Experiment
56
Maintaining the Instrument
57
Cleaning the Touch Screen
57
Cleaning a Contaminated Cell
57
Cleaning a Contaminated QDSC Standard Cell
57
Burning off Contamination in a DSC Cell with a FACS Installed
58
Burning off Contamination in a DSC Cell with an RCS or LNCS
59
Removing a DSC Q2000/Q1000 Cell
60
Installing a Cell
60
Replacing Fuses
61
Replacing the DSC Fuses
61
Replacement Parts
62
Fuses, Cords, and Cables
62
DSC Cells, Lids, and Accessories
62
Autosampler Accessories
63
Tzero Sample Encapsulation Press
63
DSC Sample Pans, Lids, and Accessories
64
Calibration/Reference Materials
65
Index
67
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TA Instruments Q1000 Specifications
General
Brand
TA Instruments
Model
Q1000
Category
Measuring Instruments
Language
English
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