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Thermo Scientific DSQ Series User Manual

Thermo Scientific DSQ Series
116 pages
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Xcalibur
Ion Trap and DSQ
Series
Direct Probe System User’s Guide
119327-0001 Revision G April 29, 2008

Table of Contents

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Thermo Scientific DSQ Series Specifications

General IconGeneral
BrandThermo Scientific
ModelDSQ Series
CategoryLaboratory Equipment
LanguageEnglish

Summary

Regulatory Compliance

EMC Directive 89/336/EEC

Specifies electromagnetic compatibility standards for the instrument.

Low Voltage Safety Compliance

Details compliance with low voltage safety directives and standards.

FCC Compliance Statement

Outlines FCC regulations for digital devices and potential interference.

WEEE Compliance

Instrument Handling and Safety Notices

Notice on Lifting and Handling

Provides safety guidelines for physically moving the instrument.

Notice on Proper Use

Advises on using the instrument as specified to maintain protection.

Notice on Susceptibility to Electromagnetic Transmissions

Warns about potential interference from radio frequency transmitters.

Preface

Safety Alerts and Special Notices

Explains the meaning and use of safety alert words and symbols.

Safety Symbols and Signal Words

Contacting Us

Related Documentation

About Your System

Power Ratings

Specifies the electrical power requirements for the mass spectrometer and GC.

Chapter 1 Using a Direct Insertion Probe (DIP)

How the Direct Probe System Works

Explains the connection and function of the Direct Probe System.

Analyzing Cholesterol with the Ion Trap Series

Step-by-step guide for analyzing cholesterol using the Ion Trap Series.

Step 1: Connect the Direct Probe System

Instructions for connecting the DPC and sample probe.

Step 2: Change the Ion Volume

Procedure to change the ion volume for analysis.

Step 3: Deselect AS and GC Devices

Steps to deselect AS and GC instruments in software configuration.

Step 4: Tune and Calibrate the Mass Spectrometer

Guidance on tuning and calibrating the mass spectrometer.

Step 5: Program the DPC

Instructions for programming the Direct Probe Controller settings.

Step 6: Prepare the Sample

Detailed steps for preparing samples for analysis.

Step 7: Create a Method File

Guide to creating an analysis method file in the software.

Step 8: Create a Sequence File

Steps for creating a sequence file for automated runs.

Step 9: Insert the Probe Using Xcalibur

Procedure for inserting the probe using the Xcalibur software.

Step 10: Remove the Probe Using Xcalibur

Procedure for removing the probe using the Xcalibur software.

Step 11: Analyze the Data File

Steps for processing and analyzing acquired data files.

Loading DIP Samples

Instructions for loading both liquid and solid samples into the DIP.

Top Terms To Know

Glossary of terms related to DIP operation.

DIP Modes

Explains ballistic and temperature-programmed modes for DIP.

Probe Shaft

Description of the DIP probe shaft component.

Probe Tip

Description of the DIP probe tip component.

Sample Cups

Information about the sample cups used with the DIP.

Top Safeguards to Know

Essential safety precautions for operating the DIP.

Hints

Practical tips for optimizing DIP experiments and usage.

Chapter 2 Using a Direct Exposure Probe (DEP)

How the Direct Probe System Works

Explains the connection and function of the Direct Probe System for DEP.

Analyzing Cholesterol with the Ion Trap Series

Steps for analyzing cholesterol using DEP on Ion Trap Series.

Step 1: Connect the Direct Probe System

Instructions for connecting the DPC and DEP probe.

Step 2: Change the Ion Volume

Procedure to change the ion volume for DEP analysis.

Step 3: Deselect AS and GC Devices

Steps to deselect AS and GC instruments for DEP operation.

Step 4: Tune and Calibrate the Mass Spectrometer

Guidance on tuning and calibration for DEP.

Step 5: Program the DPC

Instructions for programming the DPC for DEP.

Step 6: Prepare the Sample

Steps for preparing samples for DEP analysis.

Step 7: Create a Method File

Guide to creating an analysis method file for DEP.

Step 8: Create a Sequence File

Steps for creating a sequence file for DEP runs.

Step 9: Insert the Probe Using Xcalibur

Procedure for inserting the DEP probe using Xcalibur.

Step 10: Remove the Probe Using Xcalibur

Procedure for removing the DEP probe using Xcalibur.

Step 11: Analyze the Data File

Steps for processing and analyzing acquired DEP data.

Analyzing Cholesterol with the DSQ Series

Steps for analyzing cholesterol using DEP on DSQ Series.

Step 1: Connect the Direct Probe System

Instructions for connecting the DPC and DEP probe to DSQ.

Step 2: Change the Ion Volume

Procedure to change the ion volume for DEP analysis on DSQ.

Step 3: Deselect AS and GC Devices

Steps to deselect AS and GC instruments for DEP on DSQ.

Step 4: Tune and Calibrate the Mass Spectrometer

Guidance on tuning and calibration for DEP on DSQ.

Step 5: Program the DPC

Instructions for programming the DPC for DEP on DSQ.

Step 6: Prepare the Sample

Steps for preparing samples for DEP analysis on DSQ.

Step 7: Create a Method File

Guide to creating an analysis method file for DEP on DSQ.

Step 8: Create a Sequence File

Steps for creating a sequence file for DEP runs on DSQ.

Step 9: Insert the Probe Using Xcalibur

Procedure for inserting the DEP probe using Xcalibur on DSQ.

Step 10: Remove the Probe Using Xcalibur

Procedure for removing the DEP probe using Xcalibur on DSQ.

Step 11: Analyze the Data File

Steps for processing and analyzing acquired DEP data on DSQ.

Loading DEP Samples

Cleaning the DEP

Top Terms to Know

DEP Modes

Explains the current-programmed mode for DEP operation.

Probe Shaft

Description of the DEP probe shaft component.

Probe Tip

Description of the DEP probe tip component.

Top Safeguards to Know

Hints

Chapter 3 Getting Help

Who to Call

Provides contact information for technical support and service.

Detuning the Instrument

Getting Spare Parts

Abbreviations

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