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Thermo Scientific DSQ Series User Manual
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Xcalibur
Ion T
rap and DSQ
Series
Direct Probe System User’
s Guide
119327-00
01 Revisi
on G
April 2
9, 2
008
2
Table of Contents
default chapter
3
Customer Registration Card
3
Reader's Survey
3
Table of Contents
9
Preface
13
Safety Alerts and Special Notices
13
Safety Symbols and Signal Words
14
Contacting Us
15
To Contact Customer Service for Ordering Information
15
To Contact Technical Support
15
Related Documentation
16
To Suggest Changes to Documentation or to Instrument Help
16
Using a Direct Insertion Probe (DIP)
19
How the Direct Probe System Works
20
Analyzing Cholesterol with the Ion Trap Series
22
Step 1: Connect the Direct Probe System
23
Step 2: Change the Ion Volume
25
Step 3: Deselect as and GC Devices
27
Step 4: Tune and Calibrate the Mass Spectrometer
28
Step 5: Program the DPC
28
To Retrieve Methods
29
Step 6: Prepare the Sample
30
Step 7: Create a Method File
30
Step 8: Create a Sequence File
31
Step 9: Insert the Probe Using Xcalibur
33
Step 10: Remove the Probe Using Xcalibur
35
Step 11: Analyze the Data File
36
Analyzing Cholesterol with the DSQ Series
38
Step 1: Connect the Direct Probe System
39
Step 2: Change the Ion Volume
41
Step 3: Deselect as and GC Devices
43
Step 4: Tune and Calibrate the Mass Spectrometer
44
Step 5: Program the DPC
44
Step 6: Prepare the Sample
46
Step 7: Create a Method File
46
To Retrieve Methods
46
Step 8: Create a Sequence File
47
Step 9: Insert the Probe Using Xcalibur
49
Step 10: Remove the Probe Using Xcalibur
51
Step 11: Analyze the Data File
52
Loading DIP Samples
53
Loading Liquid Samples
54
Cleaning the DIP
55
Loading Solid Samples
55
DIP Modes
56
Top Terms to Know
56
Probe Shaft
57
Probe Tip
57
Sample Cups
57
Hints
58
Top Safeguards to Know
58
Using a Direct Exposure Probe (DEP)
61
How the Direct Probe System Works
62
Analyzing Cholesterol with the Ion Trap Series
64
Step 1: Connect the Direct Probe System
65
Step 2: Change the Ion Volume
66
Step 3: Deselect as and GC Devices
68
Step 4: Tune and Calibrate the Mass Spectrometer
69
Step 5: Program the DPC
69
To Retrieve Methods
70
Step 6: Prepare the Sample
71
Step 7: Create a Method File
72
Step 8: Create a Sequence File
73
Step 9: Insert the Probe Using Xcalibur
75
Step 10: Remove the Probe Using Xcalibur
77
Step 11: Analyze the Data File
78
Analyzing Cholesterol with the DSQ Series
80
Step 1: Connect the Direct Probe System
81
Step 2: Change the Ion Volume
82
Step 3: Deselect as and GC Devices
84
Step 4: Tune and Calibrate the Mass Spectrometer
85
Step 5: Program the DPC
85
To Retrieve Methods
86
Step 6: Prepare the Sample
87
Step 7: Create a Method File
88
Step 8: Create a Sequence File
89
Step 9: Insert the Probe Using Xcalibur
90
Step 10: Remove the Probe Using Xcalibur
92
Step 11: Analyze the Data File
93
Loading DEP Samples
94
Loading Liquid Samples
95
Cleaning the DEP
96
Loading Solid Samples
96
DEP Modes
99
Top Terms to Know
99
Probe Shaft
100
Probe Tip
100
Top Safeguards to Know
100
Hints
101
Chapter 3 Getting Help
103
Who to Call
104
Technical Support
104
Customer Service
104
Spare Parts
104
Technical Publications Editor
104
Detuning the Instrument
105
Getting Spare Parts
107
Abbreviations
111
Index
115
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Thermo Scientific DSQ Series Specifications
General
Brand
Thermo Scientific
Model
DSQ Series
Category
Laboratory Equipment
Language
English
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