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Thermo Scientific iCAP 6000 Series User Manual

Thermo Scientific iCAP 6000 Series
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iCAP 6000 Series
ICP-OES Spectrometer
User Guide

Table of Contents

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Thermo Scientific iCAP 6000 Series Specifications

General IconGeneral
BrandThermo Scientific
ModeliCAP 6000 Series
CategoryMeasuring Instruments
LanguageEnglish

Summary

Chapter 1 Introduction to the iCAP 6000 Series

Overview

Provides an overview of the iCAP 6000 Series ICP-OES Spectrometer and its core components.

User Documentation

Details the various manuals and help systems available for the iCAP 6000.

Chapter 2 Instrument Set-up

Pre-Installation Manual

Details the services and environment required before instrument installation.

Standard Sample Introduction Glassware Assembly

Describes the assembly of glassware for the sample introduction system.

Assembling the Torch

Instructions for correctly assembling the torch component of the instrument.

Inserting the Torch and Centre Tube into the instrument

Guidance on inserting the torch assembly into the instrument's torch box.

Connecting the Spray Chamber and Nebuliser

Steps for connecting the spray chamber and nebuliser for sample introduction.

Connecting up the sample and drain pump tubing

Details on connecting sample and drain tubing to the peristaltic pump.

Torch Alignment

Procedure for aligning the torch for optimal sensitivity and results.

Auto Peak Adjust

Process for automatically adjusting analyte wavelengths for accurate measurements.

Sample Introduction System Set-up

General setup procedures for the sample introduction system.

Peristaltic Pump Tubing Options

Information on available peristaltic pump tubing options for different sample types.

Internal Standards

Explanation of internal standards and their use in correcting signal intensity.

Application-Specific Hardware

Details on hardware configurations required for specific analytical applications.

Chapter 3 Databases

Local Database Creation

Steps to create a new local database for storing iCAP results.

Creating a Database Connection

Instructions for establishing a connection to a database server.

Chapter 4 Using the iCAP

Preparing the System for Use

Steps to prepare the instrument and system for analytical use.

Instrument Shut-down

Procedure for safely shutting down the iCAP instrument.

Analytical Operation

Overview of analytical operations and method verification.

Method Optimisation

Parameters affecting data and how to optimise them for analysis.

Running the iCAP

Steps to begin using the instrument for analysis.

Sequence of operation

Detailed sequence of steps for operating the iCAP instrument.

How to Run an Analysis

Guide to performing a simple analysis and creating a method.

Creating a Method

Steps involved in creating a new analytical method within the iTEVA software.

Running the Analysis

Instructions on how to run an analysis after creating a method.

Spectrometer Optimise

Procedure for optimizing the spectrometer and positioning lines on the detector.

Calibration

Steps to calibrate the method using blank and standard samples.

Analysing Unknowns

How to analyze unknown samples after the method has been calibrated.

Shutting Down the System

Procedure for safely shutting down the iCAP instrument and its components.

Chapter 5 Maintenance

Instrument Cleaning

Guidelines for keeping the iCAP 6000 instrument clean.

Sample Introduction System Cleaning and Decontamination

Procedures for cleaning and decontaminating the sample introduction system.

Torch Cleaning

Detailed instructions for cleaning the torch assembly.

Spray Chamber Cleaning

Steps for cleaning the spray chamber to maintain performance.

Nebuliser Cleaning

Procedures for cleaning the nebuliser to prevent blockages.

Purged Optical Path Window Cleaning

Instructions for cleaning the Purged Optical Path (POP) window.

Preventive Maintenance

Information on periodic checks and maintenance for performance.

Water Chiller

Maintenance requirements for the water chiller unit.

Gas Filters

Guidance on checking and maintaining gas filters for optimal performance.

Chapter 6 Safety

iCAP 6000 Safety

General safety information for the iCAP 6000 instrument.

Introduction

Introduction to safety precautions and personnel qualifications.

Safety Precautions

Details general and specific safety procedures and symbols.

Electrical Safety

Safety guidelines related to electrical connections and power.

Equipment Cleaning and Decontamination

Procedures for cleaning and decontaminating equipment, especially after spills.

Impaired Safety Protection

Actions to take when safety protection features are impaired.

WEEE Compliance

Information regarding Waste Electrical & Electronic Equipment compliance.

Regulatory Notices

Notices regarding CE marking and compliance with European directives.

Chapter 7 EC Declaration of Conformity

SOFTWARE LICENSING AGREEMENT

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