Thermo Scientific SOLA II User Manual

SOLA II
Su lfur Online Analyzer
User Guide
P/N 90-1307-0
Revision A B
P ar t of Thermo Fisher S cien tific

Thermo Scientific SOLA II Specifications

General

Brand	Thermo Scientific
Model	SOLA II
Category	Measuring Instruments
Language	English

Summary

Safety Information & Guidelines

Safety Considerations

General safety warnings for equipment installation, operation, and maintenance.

Safety Summary

Explanation of admonitions used in the manual to alert users to potential hazards.

Safety Operating Information

General safety and operating information for analytical systems.

Electrical Power

Information on AC power requirements, wiring, and safety precautions.

Product Overview

Function

Description of the SOLA II analyzer's major components and their roles.

Total Sulfur Measurement

Explanation of the principle behind total sulfur measurement using the analyzer.

Principle of Operation

Detailed explanation of the detection process involving UV light and SO2 fluorescence.

PUVF Detector

Details on the PUVF detector's functions and components.

Pyrolyzer

Information on the pyrolyzer's function and design for sulfur oxidation.

Dryer

Description of the optional Perma Pure dryer for moisture removal.

Mixing Chamber

Explanation of the mixing chamber's role in sample vaporization and mixing.

Injection Valve

Information on the injection valve's function in sample transfer.

Specifications

Technical and analytical specifications for the SOLA II analyzer.

Parts List

List of part numbers for the SOLA II and SOLA II Trace units.

Installation

Requirements

Material, power, operating environment, and mounting requirements for installation.

Sample Line Installation

Guidelines for installing sample lines and preparing sample tubing.

Electrical Connections

Details on AC power and wiring specifications for analyzer connection.

DCS & External Connections

Information on connecting to Distributed Control Systems (DCS) or other devices.

Digital Inputs

Overview of digital inputs for controlling the analyzer from external sources.

Optional Analog Inputs

Description of analog inputs for densitometer connections.

Analog Outputs

Details on analog outputs for measured concentration reporting.

Other Outputs

Information on provided alarm and status relay outputs.

Installation Checklist

A checklist for verifying proper installation procedures and connections.

Startup & Shutdown

Initial Startup

Procedure for starting up a new installation or after major service work.

Startup after Short-Term Shutdown

Procedure for restarting the analyzer after a brief shutdown.

Short-Term Shutdown

Procedure for temporarily shutting down the analyzer.

Maintenance Shutdown

Procedure for shutting down the analyzer for maintenance or long-term outage.

Emergency Shutdown

Procedure for safely shutting down the analyzer in an emergency.

Operation

The Interface

Description of the analyzer's user interface and how to navigate it.

Begin Analyzing

Steps to start the analysis process on the SOLA II analyzer.

Suspending an Analysis

Procedure for temporarily suspending the analysis operation.

Injection Valve Failure Alarm

Information on the injection valve failure alarm and its causes.

Configuration

Analyzer Setup

Configuration options for analyzer parameters like passcode and averaging.

Stream Setup

Configuration for selecting stream modes, dwell times, and flow settings.

Clock Setup

Procedure for setting the analyzer's time and date.

Modbus Setup

Configuration of baud rates and IDs for Modbus communication.

Dual Range Setup

Setting up dual range modes for 4-20 mA output signals.

Inject Setup

Configuration of injection time and rate parameters.

Autocal Setup

Configuration options for automatic calibration functions.

Alarms Setup

Setting up various alarm conditions and modes for the analyzer.

Calibration

Overview of the two-point linear calibration process and its graphical representation.

Density Compensation Setup

Configuration for density compensation using densitometers or fixed factors.

Viewing Alarms

View/Ack Alarm Menu

Accessing and acknowledging active alarms on the analyzer.

Diagnostics

Input & Output Test Menu

Menu for testing analyzer inputs and outputs, including relays and signals.

Set Outputs

Controls for toggling associated relays on and off.

View MUX Analogs

Viewing raw analog signals from various system components.

View 4–20 mA Inputs

Accessing and viewing optional 4-20 mA analog inputs.

View Digital Inputs

Viewing the status of digital inputs and their functions.

View Parameters

Displaying parameter names, current, min, and max values for signal stability.

View Com Activity

Monitoring communication activity for Com ports 1-4.

Pulse UV Control

Control options for the Pulse UV system, intended for factory testing.

At Line-Grab Sample

At Line Sample Configuration

Parameters to configure for at-line grab sampling.

Maintenance & Troubleshooting

Safety Precautions

Precautions for handling internal components and preventing static discharge.

Maintenance Schedule

Scheduled maintenance tasks for the SOLA II analyzer.

Visual Inspection & Cleaning

Guidelines for inspecting and cleaning the analyzer's exterior and interior.

Leak Tests

Procedure for verifying the absence of system leaks.

Flow Rate Checks

Procedure for checking and measuring instrument flow rates.

The Rotary Valve

Maintenance instructions for the rotary valve, with reference to Appendix B.

The Mixing Chamber

Procedure for removing and installing the mixing chamber.

Replacing the Pyrolyzer Heater

Step-by-step guide for replacing the pyrolyzer heater assembly.

The Pyrolyzer Reaction Tube

Instructions for replacing the pyrolyzer reaction tube (P/N 30-1025-0).

Decoking

Information on carbon buildup in the pyrolyzer tube and recommendations.

General Troubleshooting

Guidelines and sources for troubleshooting common analyzer problems.

Contact Information

Contact details for support and service from Thermo Fisher Scientific.

Warranty

Information on product warranty terms and conditions.

Items not Covered under Warranty

List of consumable items and parts excluded from the warranty.

Appendix A Watlow EZ-ZONE® PM6 Series

Controller Description

Description of the Watlow EZ-ZONE® PM6 controller's function.

Hardware Setup

Information on the EZ-ZONE PM6 wiring and hardware setup.

Display & Keys

Explanation of the EZ-ZONE PM6 controller's display and keys.

Software Configuration

Methods for configuring the EZ-ZONE PM6 controller's software.

Pyrolyzer Settings

Default configuration settings for the pyrolyzer controller.

Oven Settings

Default configuration settings for the oven controller.

Appendix B Rotary Valve Service

Initial Precautions

Precautions and guidelines for rotary valve maintenance.

Valve Disassembly

Procedure for disassembling the rotary valve for cleaning or repair.

Cleaning the Valve Body

Instructions for cleaning the internal surfaces of the valve body.

Cleaning the Rotor

Instructions for cleaning the rotor of the rotary valve.

Rotor Assembly

Steps for reassembling the rotary valve rotor.

Conditioning Procedure for High Temperature Valves

Procedure for conditioning high temperature rotary valves after rotor replacement.

Two-Position Air Actuator O-ring Replacement

Guide for replacing O-rings in the two-position air actuator.

Replacement

Steps for replacing O-rings in the actuator end caps and plate.

Assembly

Instructions for reassembling the rotary valve actuator components.

Valve Alignment

Procedure for aligning the rotary valve actuator and body.

Rebuild the Assembly

Detailed steps for rebuilding the rotary valve actuator assembly.

Appendix C Dinfa Valve Service

Overview

Introduction to the Dinfa valve and its components.

Troubleshooting

Common troubleshooting tips for the Dinfa valve.

Appendix D TCP/IP Bridge

Hardware Configuration

Description of the TCP/IP Bridge board and its installation.

Software Configuration

Steps for configuring the TCP/IP Bridge IP address and network settings.

The Browser Interface

How to access and use the analyzer's interface via a web browser.

24 Hours Chart

Displaying 24-hour activity graphs for various analyzer parameters.

24 Hours Table Format

Viewing 24-hour activity data in a table format for export.

Configuration

Accessing and configuring analyzer parameters through the workstation.

At Line Sample

Using the SOLA Web Interface for at-line grab sampling.

Appendix E Version 1.20 Modbus Registers

Coils (0)0001 to (0)0040

List of Modbus coils and their descriptions for version 1.20.

Status Inputs (1)0001 to (1)0025

List of Modbus status inputs and their descriptions.

Input Registers (3)0001 to (3)0040

List of Modbus input registers and their descriptions.

Holding Registers (4)0001 to (4)0049

List of Modbus holding registers and their descriptions.

Appendix F The Workstation

Installing Workstation Software

Steps for installing the SOLA II workstation software.

Workstation Operation

Using the workstation application to monitor and control the analyzer.

Statistics

Display of analysis statistics for streams 1 and 2.

Density Values & Trend

Viewing density trend plots from densitometer inputs.

Cal Validation History

Tracking calibration validation results over time.

Stream Plot

Displaying the trend of measured total sulfur for each stream.

Detector Status

List of current status monitors and trend charts for troubleshooting.

Alarms Status

Displaying active alarms, faults, and malfunctions detected by the analyzer.

Remote Controls

Switches used to control analyzer functions remotely from the workstation.

Analyzer Status

Indicators showing the analyzer's current operational status.

Configuration

Accessing configuration screens for analyzer setup and calibration.

Appendix G The X-Purge System

Description

Explanation of the X-Purge assembly for safe operation in hazardous areas.

X-Purge Specifications

General specifications, normal conditions, and utility requirements.

Installation

Information on AC power connections and installation precautions.

Alarm Signal

Details on using X-Purge dry alarm contacts and connection table.

Startup

Procedure for starting up analyzer systems using the X-Purge system.

Shutdown

Procedure for manually shutting down the X-Purge system.

Power or Purge Loss Shutdown

How the X-Purge unit handles power or purge pressure loss.

Maintenance

Precautions and guidelines for system maintenance.

Timer Adjustment

Information on the required time delay for safe operation.

Appendix H Software Menu Tree

Top-Level Menus & Configuration Subgroups

Visual representation of the analyzer's software menu structure.

Diagnostics Subgroups

Breakdown of the Diagnostics menu into its various subgroups.

Appendix I PUVF Optical Bench

Optical bench assembly exploded diagram

Exploded view diagram of the PUVF optical bench assembly.

Appendix J Dual PMT Supply Option

Overview

Introduction to the Dual PMT Supply option and its applications.

Menu Changes for Dual PMT Supply Option

Differences in configuration menus introduced by the Dual PMT Supply option.

Calibration Setup

Configuration of independent calibrations (Cal A and Cal B) for the option.

AutoCal Setup

Configuration for automatic validation/re-calibration of calibrations A or B.

Stream Setup

Configuration of streams to use Cal A, Cal B, or auto range.

4–20 mA Range Setup

Configuration of unique ranges for the 4-20 mA output for each calibration.

Diagnostics Display

Viewing PMT voltage and other parameters in the Diagnostics menu.

At Line-Grab Sample

Using the At Line-Grab Sample function with the Dual PMT Supply option.

Installation

Information on retrofitting the Dual PMT Supply option to existing units.

APPENDIX K Toxic & Hazardous Substances Table – SOLA-II

Names and Content of Toxic and Hazardous Substances or Elements

Table listing toxic/hazardous substances in SOLA-II parts per Chinese regulation.

Appendix L Connecting to a Sarasota FD910 Density Meter

Purpose

Purpose of connecting the Sarasota FD910 density meter for live density compensation.

Connections

Information on making connections between the density meter and SOLA II.

Connecting One Density Meter to a Dual Stream System

Configuration for using one density meter on a dual stream system.

Appendix M Related Technical Bulletins

Technical bulletins

List of technical bulletins related to the SOLA II product.

Appendix N Trace level measurements

Description of the SOLA II Trace

Description of the SOLA II Trace, its modifications, and improved detection.

Calibration method

Explanation of the calibration method for the SOLA II Trace.

Combustion gas for the SOLA II Trace

Guidance on combustion gas selection for accurate low-level sulfur measurements.

Appendix O: Vapour sample measurements

Additional guidance on the SOLA II for Vapours

Guidance on performance, ranges for vapour samples, especially high dewpoint.

SOLA 11 for Condensable Vapours (CV)

Description of the SOLA II CV modification for high dew point samples.