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iCAP Q
Thermo Scientific iCAP Q User Manual
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Part of Thermo Fisher Scientific
Revision B - 1288090
Thermo Fisher Scientific
iCAP Q
Operating Manual
2
Table of Contents
Default Chapter
5
Table of Contents
5
Chapter 1 Using this Manual
9
About this Manual
9
Typographical Conventions
10
Signal Word
10
Viewpoint Orientation
10
Data Input
10
Topic Headings
11
Reference Documentation
12
Chapter 2 Scope of Delivery
13
Standard System Components
13
Optional System Components
14
Chapter 3 System Description
15
General Description
16
Instrument Layout
17
Sample Introduction System
18
Peristaltic Pump
18
Nebulizer
19
Spray Chamber
19
Injector
20
Torch
20
Interface
21
Sample Cone and Skimmer Cone
21
Extraction Lens
22
Ion Optics
23
RAPID Lens
23
Qcell
23
DA Assembly
24
Mass Analyzer
24
Quadrupole
24
Detector
24
Vacuum System
25
Forepump
26
Turbomolecular Pump
26
Pressure Measurement
26
Gas Supply
27
Connections
27
Plasma and Cooling Gas
28
CCT Gas
29
Additional Gas
31
Cooling System
33
Connections for Water Supply
33
Recirculating Chiller
34
Exhaust System
35
Connections
36
Main Power Switch
37
Power Connections
37
Fore Vacuum Pump Connections
38
Connection to Computer and Peripherals
39
Chapter 4 Safety
42
Safety Symbols and Signal Words in this Manual
42
Observing this Manual
42
Safety Symbols on the Instrument
43
Rating Plate
45
Intended Use
46
Qualified Personnel
47
Permitted Materials
47
Electrical Safety Precautions
48
Residual Hazards
49
Personal Protective Equipment
50
EMC Information
51
In Case of Emergency
52
Chapter 5 System Setup
54
Safety Guidelines for Installation
54
Placing the System
55
Instrument Dimensions
55
Moving the Instrument
56
Workbench for Instrument
57
Laboratory Conditions
59
Power Supply
59
Gas Supply
59
Laboratory Temperature
60
Humidity
60
Ventilation and Fume Exhaust
61
Vibration
61
Airborne Noise Emission
61
Chapter 6 Operation
63
Safety Guidelines for Operation
64
System Controls
66
System Status Leds
66
Power Panel
67
Starting up the System
68
Shutting down the System
69
Switching to Standby Mode
69
Shutting down the Complete System (Instrument Vented)
69
Shutting down the Instrument Only (Instrument Not Vented)
70
Getting Ready
71
Before Operating the System
71
Getting Ready with the Experiment Editor
71
Going to Operation Status with Instrument Control
75
Working with Labbooks
76
Loading a Labbook
76
Submitting a Labbook
77
Starting the Data Acquisition
77
After Operation
78
Run the System with Blanks
78
Release Peristaltic Pump Tubing
78
Emptying the Waste Container
78
Chapter 7 Troubleshooting
80
General Remarks
80
Administrator/User
80
Safety Guidelines for Troubleshooting
80
Error Messages
82
Plasma Not Lit
83
Sensitivity Problems/No Signal
85
Signal Drifts with Time
86
Poor Signal Stability
87
Interlocks
88
Door Lock
88
Interface Temperature
88
Low Water Flow
88
Hardware Lock Open
89
Water Valve Closed
89
Low Argon Pressure
89
Low Cool Gas Flow
89
Low Exhaust Gas Flow
90
Plasma Lit Sensor
90
Chapter 8 Maintenance
91
Safety Guidelines for Maintenance
92
General Advice for Maintenance
94
Returning Parts
94
Servicing Plan
95
General Maintenance Routines
97
Cleaning the Surface of the Instrument
97
Cleaning Agents
97
Checking Warning Labels
97
Checking Gas Lines for Leaks
98
Maintaining the Air Filter
99
Maintaining the Inlet System
101
Maintaining the Nebulizer
101
Maintaining the Peristaltic Pump
102
Maintaining the Spray Chamber
103
Maintaining the Injector
104
Maintaining the Torch
105
Cleaning the Glassware
106
Maintaining the Interface
107
Tools
107
Maintaining the Sample Cone
107
Maintaining the Skimmer Cone
110
Maintaining the Extraction Lens
113
Thermo Fisher Scientific Service
116
Health and Safety Form
116
Services to be Performed by Thermo Fisher Scientific Service Only
116
Chapter 9 Additional Safety Information
118
Fore Vacuum Pump
118
Recirculating Chiller
120
Dionex ICS-5000
121
Legal Documents
124
Glossary
127
Index
131
4
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Thermo Scientific iCAP Q Specifications
General
Brand
Thermo Scientific
Model
iCAP Q
Category
Laboratory Equipment
Language
English
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