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Thermo Scientific iCAP Q User Manual

Thermo Scientific iCAP Q
134 pages
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Part of Thermo Fisher Scientific
Revision B - 1288090
Thermo Fisher Scientific
iCAP Q
Operating Manual

Table of Contents

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Thermo Scientific iCAP Q Specifications

General IconGeneral
Sample IntroductionStandard or optional autosampler
InterfaceNickel cones
DetectorDiscrete dynode detector
Plasma Generator27.12 MHz free-running RF generator
Spray ChamberQuartz cyclonic spray chamber (standard); Optional: Peltier cooled spray chamber
NebulizerConcentric glass nebulizer
RF Generator27.12 MHz
Operating SoftwareQtegra Intelligent Scientific Data Solution (ISDS) Software
WeightApproximately 150 kg (330 lbs)
Power Requirements200-240 V, 50/60 Hz
Detection Limitsppt to sub-ppt levels
Vacuum SystemDual stage rotary vane pump and turbo molecular pump

Summary

Using the iCAP Q Operating Manual

About the iCAP Q Operating Manual

Provides an overview of the manual's content, including precautionary statements and instrument descriptions.

Typographical Conventions

Details text formatting, signal words, and notation conventions used throughout the manual.

Topic Headings

Explains the heading structure used to organize topics within chapters.

Reference Documentation

Lists additional reference documents and resources for the iCAP Q mass spectrometer.

iCAP Q Scope of Delivery

Standard System Components

Lists the standard components included with the iCAP Q system.

Optional System Components

Lists frequently shipped optional components for the iCAP Q MS system.

iCAP Q System Description

General Description of the iCAP Q

Overview of the iCAP Q mass spectrometer's design and models.

iCAP Q Instrument Layout

Details the four main components of the iCAP Q instrument.

Sample Introduction System

Describes the components of the sample introduction system, including pump and nebulizer.

iCAP Q Ion Optics

Explains the ion optics region, including RAPID lens and QCell.

iCAP Q Mass Analyzer and Detector

Details the quadrupole mass analyzer and detector components.

iCAP Q Vacuum System

Describes the three-stage pumping system for the iCAP Q instrument.

iCAP Q Gas Supply

Covers argon and other gas requirements for operating the iCAP Q.

iCAP Q Cooling System

Specifies requirements for the cooling water used by the iCAP Q.

iCAP Q Exhaust System

Details the exhaust ports and system requirements for the iCAP Q.

iCAP Q Connections

Illustrates the various connection points on the iCAP Q instrument.

iCAP Q Safety Information

Safety Symbols and Signal Words

Explains safety symbols, signal words, and their meanings in the manual.

Safety Symbols on the Instrument

Lists and describes safety labels found on the iCAP Q instrument.

iCAP Q Rating Plate Information

Details the system information found on the instrument's rating plate.

Intended Use of the iCAP Q

Defines the proper usage and limitations of the iCAP Q mass spectrometer.

Qualified Personnel and Permitted Materials

Specifies requirements for personnel and materials for iCAP Q installation and operation.

Electrical Safety Precautions

Outlines essential safety measures related to electrical hazards.

Residual Hazards and Precautions

Highlights potential residual hazards and necessary precautions during operation.

Personal Protective Equipment (PPE) Guidelines

Provides recommendations for eye protection, clothing, and gloves.

EMC Information for iCAP Q

Details electromagnetic compatibility information and usage guidelines.

In Case of Emergency Procedures

Explains steps to shut off the plasma or the entire system in an emergency.

iCAP Q System Setup

Safety Guidelines for Installation

General safety guidelines to follow during the installation of the iCAP Q.

Placing the iCAP Q System

Guidelines and dimensions for positioning the iCAP Q instrument.

Laboratory Conditions for iCAP Q

Specifies requirements for power supply, temperature, and humidity.

iCAP Q Operation Guide

Safety Guidelines for Operation

Key safety precautions to observe while operating the iCAP Q system.

iCAP Q System Controls and Status LEDs

Details the instrument's front panel controls and status indicator lights.

Starting Up the iCAP Q System

Procedure for safely starting the iCAP Q instrument.

Shutting Down the iCAP Q System

Instructions for switching to standby or completely shutting down the system.

Getting Ready for Analysis

Steps to prepare the iCAP Q for analysis, including performance checks.

Working with LabBooks for Data Analysis

Guidance on loading, submitting, and working with LabBooks for data evaluation.

After Operation Procedures

Recommended procedures after completing experiments, like flushing and cleaning.

iCAP Q Troubleshooting Guide

General Remarks and Safety Guidelines for Troubleshooting

General advice, rules, and safety precautions for diagnosing and solving instrument problems.

iCAP Q Error Messages and Table

Lists common error messages and their corresponding causes and remedies.

Troubleshooting: Plasma Not Lit

Step-by-step guide to resolve issues with the plasma not igniting.

Troubleshooting: Sensitivity Problems/No Signal

Guidance for resolving issues related to low or no signal output.

Troubleshooting: Signal Drifts with Time

Procedures to address and correct signal drift issues.

Troubleshooting: Poor Signal Stability

Steps to diagnose and improve poor signal stability.

iCAP Q Interlocks and Their Resolution

Explanation of instrument interlocks and how to reset them.

iCAP Q Maintenance Procedures

Safety Guidelines for Maintenance

Essential safety precautions to follow during maintenance tasks.

General Advice for iCAP Q Maintenance

Provides general recommendations and rules for performing maintenance.

iCAP Q Servicing Plan

Lists routine and infrequent maintenance procedures with their frequency.

General Maintenance Routines

Covers cleaning surfaces, agents, and checking warning labels.

Maintaining the Air Filter

Instructions for checking and cleaning the instrument's air filter.

Maintaining the iCAP Q Inlet System

Procedures for maintaining the nebulizer, pump, and spray chamber.

Maintaining the iCAP Q Interface

Guidance on cleaning and replacing sample/skimmer cones and extraction lens.

Thermo Fisher Scientific Service Information

Information on maintenance tasks performed by Thermo Fisher Scientific personnel.

Additional Safety Information for iCAP Q Components

Fore Vacuum Pump Safety

Safety precautions specific to the fore vacuum pump.

Recirculating Chiller Safety

Safety warnings and precautions for the recirculating chiller unit.

Dionex ICS-5000 Safety Information

Safety guidelines and warnings related to the Dionex ICS-5000 system.

Legal Documents for iCAP Q

FCC Compliance Statement

Statement regarding the device's compliance with FCC rules.

WEEE Compliance Information

Information on compliance with the Waste Electrical and Electronic Equipment Directive.

Declaration of Conformity

Manufacturer's declaration of conformity with relevant EC directives.

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