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ISQ 7610
Thermo Scientific ISQ 7610 - User Manual
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ISQ 7610
Mass Spectrometers
User Guide
1R120621-0003 Revision A April 2022
2
Table of Contents
Main Page
default chapter
5
Table of Contents
5
About Your System
15
Preface
15
Related Documentation
16
Safety and Special Notices
17
Special Notices
17
System Requirements
17
Safety Symbols and Signal Words
18
Hydrogen Safety Precautions
21
Hydrogen Connection Guidelines
23
Using Hydrogen with ISQ 7610 Mass Spectrometers
23
Properly Storing Hydrogen
25
Purchasing Hydrogen
25
Hydrogen Safety Codes, Standards and References
27
Hazardous Substances Precautions
28
Biological Hazard Warning Note
29
Contacting Us
29
Venting Toxic Gases
29
Checking Power to the System
31
Confirming Your GC/MS System Is Working
31
Verifying the Carrier Gas Flow Rate
32
Checking Your Carrier Gas Supply Pressure
33
Checking the Vacuum and Temperature
34
Chapter 2 Changing the Column
35
Replacing the Factory-Installed Column
36
Replacing a Column in a ISQ 7610 System with no VPI or an AEI Ion Source
37
Replacing a Column on a ISQ 7610 System with a VPI and an Extractabrite Ion Source
47
Installing the Column in the GC Inlet
53
Chapter 3 Tuning the ISQ 7610 Mass Spectrometer
59
Accessing ISQ 7610 Tuning
60
Tune Types
64
EI Initial Tune
64
EI Full Tune
64
EI Tune
66
EI Check
66
EI Diagnostics
67
Negative CI Tune
67
Positive CI Tune
69
AEI Full Tune
71
AEI Tune
71
AEI Check
72
AEI Diagnostics
72
Tuning the ISQ 7610 Mass Spectrometer
72
Using Smarttune
77
Tuning for DFTPP and BFB
83
Chapter 4 Creating a Method
93
Accessing the Method Editor
93
Creating a GC-MS Method in Xcalibur Software
96
Creating an Autosampler Method in Xcalibur Software
97
Creating a Method for the ISQ 7610 Mass Spectrometer
101
Creating a Method for the GC in Xcalibur Software
119
Creating a GC-MS Method in Chromeleon Software
126
Chapter 5 Using Autosim
159
Determining SIM Ions
159
Importing Transitions to the Method Editor
169
Determining SIM Ions in Chromeleon
172
Importing Transitions to the Chromeleon Instrument Method Editor
184
Chapter 6 Running a Sample
187
Preparing Your Sample
187
Running a Sequence in Xcalibur Software
188
Running a Sequence in Chromeleon Software
200
Exploring Your Data
211
Optimizing Your Method
215
Changing the Chromatographic Separation
215
Finding the Best Way to Make an Injection
216
Improving the Way You Prepare Samples
216
Changing the Scan Rate
216
Narrowing the Mass Range
216
Adjusting the Transfer Line Temperature
217
Modifying an Automatic Tune
218
Chapter 9 Troubleshooting
247
Setting Instrument Conditions for Troubleshooting
248
Checking Air/Water Spectra
249
No Ions Present in Scans
255
Checking the ISQ 7610 System Firmware
255
How to Know When Your System Needs Maintenance
258
Investigating Baseline Issues
262
Investigating Peak Issues
264
Investigating Results Issues
267
Reconfiguring Your Instrument
269
Upgrading the Software
285
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Thermo Scientific ISQ 7610 Specifications
General
Brand
Thermo Scientific
Model
ISQ 7610
Category
Laboratory Equipment
Language
English
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