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Thermo Scientific TSQ 9610 User Manual

Thermo Scientific TSQ 9610
492 pages
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TSQ 9610
Mass Spectrometer
Hardware Manual
1R120622-0003 Revision A April 2022

Table of Contents

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Thermo Scientific TSQ 9610 Specifications

General IconGeneral
Mass AnalyzerTriple Quadrupole
Resolution0.7 FWHM
Ion SourceAPCI
Data AcquisitionSIM
SoftwareThermo Scientificâ„¢
Power Requirements100-240 V, 50/60 Hz
Dynamic Range> 5 orders of magnitude

Summary

Preface

About Your System

Overview of the Thermo Scientific GC/MS instrumentation and its capabilities.

Related Documentation

Lists associated guides and help resources for the TSQ 9610 system.

System Requirements

Specifies the minimum hardware and software requirements for the TSQ 9610 data system.

Safety and Special Notices

Highlights important safety information and special notices presented in the manual.

Safety Symbols and Signal Words

Explains the meaning of various safety symbols and signal words used in the manual.

Hydrogen Safety Precautions

Details the hazards associated with hydrogen gas and necessary safety measures.

Hydrogen Connection Guidelines

Provides guidelines for safely connecting hydrogen gas to the system.

Properly Storing Hydrogen

Offers guidelines for the safe storage of hydrogen gas cylinders.

Hazardous Substances Precautions

Outlines precautions for handling hazardous substances.

Contacting Us

Provides information on how to contact Thermo Fisher Scientific for support.

Chapter 1 Performing Routine Maintenance

Maintenance Supplies and Tools

Lists the necessary supplies and tools for performing routine maintenance.

Configuring the TSQ 9610 System

Provides steps for initial system configuration and setup.

Powering On the TSQ 9610 System

Details the procedure for powering on the TSQ 9610 mass spectrometer.

Powering Off the TSQ 9610 System

Describes the steps required to safely power off the TSQ 9610 system.

Replacing a Column

Step-by-step instructions for replacing the GC column.

Maintaining the Foreline Pump

Guidance on the maintenance of the foreline pump.

Removing the Ion Source Cartridge for Cleaning

Procedure for removing the ion source cartridge for cleaning.

Disassembling the ExtractaBrite Ion Source Cartridge

Instructions for disassembling the ExtractaBrite ion source cartridge.

Disassembling the NVAEI Ion Source Cartridge

Instructions for disassembling the NVAEI ion source cartridge.

Maintaining the Calibration Gas Module

Describes the maintenance procedures for the calibration gas module.

Refilling the Calibrant Reservoir

Steps for refilling the calibrant reservoir in the calibration gas module.

Replacing a Dual Filament

Procedure for replacing the dual filament in the ion source.

Replacing the Electron Multiplier

Steps for replacing the electron multiplier component.

Cleaning Durable Components

Instructions for cleaning durable components within the vacuum manifold.

Cleaning Delicate Components

Instructions for cleaning delicate components within the vacuum manifold.

Cleaning the Filters

Procedures for cleaning and replacing the instrument's filters.

Chapter 2 Troubleshooting

Using Diagnostics

Guide to using software diagnostics to detect and solve instrument problems.

Investigating Communication Issues

Troubleshooting steps for issues related to instrument communication.

Investigating Contamination Issues

Addresses common causes of chemical noise and contamination.

Investigating Filament and Lens Control Issues

Troubleshooting for filament and lens control problems.

Investigating Temperature Issues

Diagnosing problems related to heated zones like ion source and transfer line.

Investigating Vacuum Issues

Steps to diagnose and resolve issues with the instrument's vacuum system.

Investigating Power Supply Issues

Troubleshooting guide for problems with the instrument's power supply.

Investigating RF/DC Issues

Diagnosing and resolving problems with the RF/DC system.

Investigating Sensitivity Issues

Troubleshooting steps for low sensitivity or sudden loss of sensitivity.

Investigating Stability Issues

Addresses issues related to instrument consistency and reproducibility.

Investigating Tuning Issues

Guidance for resolving problems encountered during automatic tune.

Contacting Technical Support

Information on how to contact technical support for unresolved issues.

Chapter 3 Advanced Troubleshooting

Replacing Components of the Analyzer

Procedures for replacing components of the analyzer tray.

Replacing Components of the Ion Source

Instructions for replacing various components of the ion source.

Replacing Components of the Vacuum Interlock

Steps for replacing components of the vacuum interlock system.

Replacing Components of the Manifold

Procedures for replacing components of the instrument's manifold.

Replacing Components of the Electron Multiplier

Instructions for replacing components of the electron multiplier.

Reinstalling the TSQ 9610 System Software

Guide to upgrading instrument firmware and computer software.

Replacing the Covers of the TSQ 9610 Instrument

Instructions for replacing damaged covers and panels of the instrument.

Replacing Components of the Front Door

Procedures for replacing components of the instrument's front door.

Replacing the Boards in the TSQ 9610 Instrument

Instructions for replacing various circuit boards within the instrument.

Replacing the Power Supplies

Steps for replacing the instrument's power supply components.

Replacing the Calibration Gas Components

Instructions for replacing calibration gas system components.

Replacing the Collision Gas Components

Procedures for replacing collision gas system components.

Replacing Fans and Filters

Guide for replacing cooling fans and filters to maintain instrument temperature.

Replacing the Turbomolecular Pump

Instructions for installing or replacing the turbomolecular pump.

Convectron Gauge and Foreline Adapter with Hose

Procedure for replacing the convectron gauge and foreline adapter.

Chapter 4 Upgrade Equipment

Advanced EI Ion Source

Instructions for installing an Advanced EI ion source.

Dust Filter

Information on installing an optional dust filter for the system.

CI Reagent Gas Flow Module

Steps for installing a new CI reagent gas flow module.

CI Ion Volume

Instructions for replacing the EI ion volume with a CI ion volume.

EI/CI Ion Volume

Guide for installing a combined EI/CI ion volume for dual-mode operation.

Ion Gauge and Tube Shield

Procedure for installing an ion gauge and tube shield.

Probe Controller

Instructions for installing a DIP or DEP direct probe controller.

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