Contents
Overview....................................................................................................................................4
Typical Installations .................................................................................................................4
Setting Up..................................................................................................................................5
Checking the Installation Site .....................................................................................................................................5
Unpacking...................................................................................................................................................................5
Connecting Components ............................................................................................................................................5
Setting Up the GC.....................................................................................................................8
Filling the Cal Gas Vial ...............................................................................................................................................8
Plumbing and Purging ................................................................................................................................................8
Installing the Column in the GC..................................................................................................................................9
Installing the Column in the MS..................................................................................................................................9
Setting Up the Foreline Pump .................................................................................................9
DS-42 Pump ...............................................................................................................................................................9
Powering Up the MS...............................................................................................................11
Baking Out the GC/MS .............................................................................................................................................11
Preliminary Tuning.................................................................................................................12
Monitoring the System..............................................................................................................................................12
Adjusting the RF Ramp ............................................................................................................................................13
Adjusting Cal Gas.....................................................................................................................................................15
Auto Tuning ............................................................................................................................16
Auto Tuning ..............................................................................................................................................................16
Testing Specifications............................................................................................................17
Specification Table ...................................................................................................................................................17
EI Methodology.........................................................................................................................................................17
Acquiring OFN ..........................................................................................................................................................18
Reviewing the Data...................................................................................................................................................18
Calculating the Signal to Noise Ratio .......................................................................................................................20
Library Searching......................................................................................................................................................22
CI Methodology.........................................................................................................................................................25
Installing Liquid CI ....................................................................................................................................................25
Adjusting Liquid CI Reagent Flow ............................................................................................................................26
Methodology .............................................................................................................................................................27
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