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Micromass ZQ 2000
Waters Micromass ZQ 2000 User Manual
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W
a
te
rs Micromass
ZQ Detector
Oper
ator’
s G
uide
34 Maple Street
Milf
ord, MA
01757
71500044702, Re
vision B
2
Table of Contents
Default Chapter
15
Table of Contents
15
Preface
23
Chapter 1 Overview
27
About the Micromass ZQ Detector
27
Theory and Principles of Operation
28
Masslynx 4.0 Software
29
Chapter 2 Installing
30
Installing the Detector
30
Site Selection and Power Requirements
31
Installation Site Requirements
31
Unpacking and Inspecting
32
Installing the Detector
33
Installing the Rotary Pump
33
Pump Oil Level
33
Installing the Oil Return Connection Kit
34
Connecting the Nitrogen Supply and Exhaust
35
Fitting the Gas Ballast and Hose Adaptors to the Rotary Pump
35
ZQ Detector Rear Panel
36
Nitrogen Stud
36
Connecting the Rheodyne Injector (for Manual Injections)
37
Drying Gas Exhaust Bottle
37
Installing the ESI Probe
38
Rheodyne Injector
38
Connecting the Workstation
39
ESI Probe in Situ
39
Preparing the Syringe and Syringe Pump
40
Syringe Pump
40
Chapter 3 Tuning
41
Opening Masslynx and Starting the Instrument
41
Masslynx Login Dialog Box
41
Masslynx Main Window
42
Tuning in ESI Mode
43
Tune Window Displaying the ES+ Source Page
43
ES+ Source
43
Specifying Parameter Settings on the ES+ Source Page
44
Source and Desolvation Temperature Settings
44
Syringe Selection Dialog Box
45
Specifying Parameter Settings on the Analyser Page
46
Tuning in APCI Mode
47
Tune Window Displaying the Analyser Page
47
Preparing the Source for APCI Operation
48
Installing the Tee Fitting
49
Specifying Parameters on the APCI+ Source Page
49
Combined Flow into the Tee
49
APCI+ Source
49
Tune Window Displaying the APCI+ Source Page
50
Readbacks
52
Readbacks Dialog Box
52
Diagnostics Page Readbacks
53
Chapter 4 Calibrating
54
Setting up the Calibration File
54
Calibration Window
54
Setting Calibration Parameters
55
Tune Window Settings
55
Open Dialog Box
55
Tune Window Displaying the ES+ Source Page
57
Instrument Threshold Settings Dialog Box
58
Tune Window Displaying Analyser
58
Automatic Calibration Check Dialog Box
59
Instrument Threshold Settings Dialog Box
59
Calibration Parameters Dialog Box
60
Mass Measure Dialog Box
62
Automatic Calibration Dialog Box
63
Calibration Acquisition Dialog Box
64
Calibration Acquisition Setup Dialog Box
65
Recommended Calibration Acquisitions Setup Parameters
65
Display Calibration Graphs Dialog Box
67
Calibration Failure Troubleshooting
69
Calibrate Window Showing ZQ-4000 Calibration Graphs
69
Chapter 5 Maintaining
73
Considerations
73
Maintenance Schedule
74
Routine Maintenance
75
Checking the Rotary Pump Oil
75
Replacing the Pump Oil
75
Rotary Pump Assembly Fitted with Oil Mist Filter
76
Rotary Pump Oil Filler Plug, Drain Plug, and Sight Glass
77
Gas-Ballasting the Rotary Pump
78
Replacing the Oil Mist Filter
79
Isolation Valve
79
Cleaning the Source Assembly
80
Oil Mist Filter Assembly
80
Pumping Block Assembly
82
Ion Block Assembly
83
Probe Assembly in Position on the Source
84
ZQ Detector Front View
85
Source Showing the Corona Discharge Needle
86
Ion Block
86
Sample Cone and Cone Gas Nozzle
87
Ion Block Rear View
88
Hexapole Assembly
89
Cleaning the APCI Probe Tip
91
Cleaning and Replacing the Corona Discharge Needle
91
Replacing Parts
92
Replacing the Ion Block Cartridge Heater
92
Ion Block Cartridge Heater
92
Replacing the Stainless Steel Capillary
93
Replacing the ESI Probe Tip
95
Replacing the APCI Fused Silica Capillary and Filter Pad
96
Replacing the APCI Probe Heater
98
Chapter 6 Troubleshooting
99
Safety and Handling
99
Component Hardware Troubleshooting
101
Hardware Troubleshooting
101
Inspecting the APCI Probe
107
Appendix A Using the Esci Multi-Mode Ionization Source
108
Preparing for Operation
108
Installing the Corona Discharge Needle
108
ZQ Mass Detector, Front View
109
Setting up Masslynx
110
Installing the Corona Needle
110
Tune Window
110
Tune Window Showing Options List with Esci Mode Selected
111
A-5 Tune Window, Diagnostics
112
Selecting the Esci+ or Esci- Ionization Mode
112
Selecting the Ion Mode in the Masslynx Peak Editor
113
Tune Window as It Appears During Esci Operation
114
Function List Editor Window (Blank)
115
Function:n MS Scan Dialog Box
115
Function List Editor Window Showing Specified Functions
116
Daidzein Test
117
Test Conditions
118
Signal-To-Noise Ratio
118
HPLC Conditions
118
MS Conditions
118
Appendix B Specifications
119
ZQ Detector Specifications
119
ZQ Detector Operational Specifications
119
ZQ Detector Dimensions
120
ZQ Detector Electrical Specifications
120
Esci Multi-Mode Ionization Source Specifications
121
ZQ Detector Environmental Specifications
120
Esci Electrical Specifications
121
Esci Environmental Specifications
121
Accessories and Spare Parts
122
Appendix C
122
Probe Components
122
Vacuum Components
123
Valves and Flow Meters
124
C-5 Kits
125
Power Supplies
125
Index
129
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Waters Micromass ZQ 2000 Specifications
General
Brand
Waters
Model
Micromass ZQ 2000
Category
Security Sensors
Language
English
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