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Waters 3100 User Manual

Waters 3100
220 pages
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Waters 3100 Detector
Operators Guide
71500135102 Revision E
Copyright © Waters Corporation 2006–2010
All rights reserved

Table of Contents

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Waters 3100 Specifications

General IconGeneral
BrandWaters
Model3100
CategorySecurity Sensors
LanguageEnglish

Summary

Waters 3100 Detector Overview

Overview

Provides a general description of the Waters 3100 Detector.

Ionization Techniques and Source Probes

Details different ionization methods and associated probes for the detector.

Ion Optics

Explains the operation of the instrument's ion optics system.

MS Operating Modes

Describes the different operating modes of the mass spectrometer.

Sample Inlet and Vacuum System

Details sample introduction methods and the vacuum system.

Rear Panel Connections

Illustrates the rear panel connections and ports for external devices.

IntelliStart Fluidics System

Describes the IntelliStart fluidics system and its capabilities.

System Operation

Explains how the IntelliStart fluidics system is operated.

Preparing the Instrument for Operation

Starting the Instrument

Outlines the procedure for powering on and starting the instrument.

Preparing the IntelliStart Fluidics System

Details the preparation steps for the IntelliStart fluidics system.

Rebooting and Standby Procedures

Explains how to restart the instrument and leave it in standby mode.

ESI and ESCi Modes of Operation

Introduction to ESI and ESCi

Provides an introduction to ESI and ESCi ionization modes.

ESI Probe Installation and Removal

Guides on installing and removing the ESI probe.

Corona Pin Installation and Removal

Details the steps for installing and removing the corona pin.

Optional APCI Mode of Operation

Atmospheric Pressure Chemical Ionization

Explains the APCI ionization technique.

IonSABRE APCI Probe Installation

Guides on installing the IonSABRE APCI probe.

APCI Corona Pin and Probe Removal

Explains how to remove the corona pin and IonSABRE APCI probe.

Maintenance Procedures

Maintenance Schedule and Safety

Outlines the maintenance schedule and essential safety precautions.

Preparing for Source Maintenance

Details necessary steps before performing source maintenance.

Source Isolation Valve Operation

Explains how to operate the source isolation valve.

Component Cleaning and Replacement

Procedures for cleaning O-rings, seals, cones, and probes.

Roughing Pump Maintenance

Guides on gas ballasting, checking oil, and replacing oil demister.

Instrument Air Filter Maintenance

Procedures for cleaning and replacing instrument air filters.

Safety Advisories

Warning and Caution Symbols

Explains various warning and caution symbols used in the manual.

General and Specific Warnings

Lists general warnings and specific hazards like burst tubing.

Electrical, Shock, and Biohazard Warnings

Covers electrical hazards, shock risks, and biohazard precautions.

Handling Symbols and Instrument Usage

Explains handling symbols and proper instrument usage.

External Connections

Wiring and Vacuum Connections

Details external wiring and vacuum connections on the rear panel.

Roughing Pump Connections

Instructions for connecting oil-filled and oil-free roughing pumps.

Nitrogen Gas Supply and Exhaust

How to connect the nitrogen gas supply and exhaust lines.

Liquid Waste Line Connection

Instructions for connecting the liquid waste line.

Workstation and Ethernet Connectivity

Steps for connecting the workstation and Ethernet cables.

I/O Signal and Electricity Connections

Details I/O signal connectors and connecting to electricity source.

Materials of Construction and Compliant Solvents

Preventing Contamination and Exposed Items

Information on preventing contamination and items exposed to solvents.

Solvents for Mobile Phase Preparation

Lists common solvents used for mobile phase preparation.

Sample Preparation for System Check

Required Materials for Sample Prep

Lists materials needed for preparing the sulfadimethoxine standard.

Preparing the Sulfadimethoxine Standard

Details how to prepare the sulfadimethoxine standard solution.

Storing and Using the Standard Solution

Guidance on storing and using the prepared standard solution.

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