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Hach Lange DR 3900 User Manual

Hach Lange DR 3900
150 pages
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DOC022.52.90323
DR 3900
USER MANUAL
04/2013 Edition 3A
© HACH-LANGE GmbH, 2011, 2013. All rights reserved. Printed in Germany.

Table of Contents

Questions and Answers:

Hach Lange DR 3900 Specifications

General IconGeneral
TypeSpectrophotometer
Wavelength Resolution0.1 nm
Spectral Bandwidth5 nm
Display7-inch color touchscreen
Operating Temperature5 to 40 °C
Wavelength Range190 - 1100 nm
Photometric Accuracy± 0.005 Abs
Stray Light< 0.1 %
InterfacesUSB, Ethernet
ConnectivityEthernet
Power Supply100-240 V AC
Measurement ModesAbsorbance, Transmittance, Concentration

Summary

Section 1 Specifications

Performance Specifications

Details the instrument's performance metrics like display mode, wavelength, accuracy, etc.

Physical and Environmental Specifications

Covers the instrument's dimensions, mass, and operating environment requirements.

Additional Technical Data

Includes details on power supply and interface specifications for the instrument.

Section 2 General Information

Safety Information

Provides crucial safety instructions for operating the spectrophotometer safely.

Chemical and Biological Safety

Addresses potential hazards and safe handling procedures for chemicals and biological samples.

Overview of Product

Introduces the DR 3900 spectrophotometer and its key features and programs.

Section 3 Installation

Unpack the Instrument

Lists the items included with the DR 3900 spectrophotometer upon delivery.

Operating Environment

Outlines the recommended conditions for instrument setup and operation.

Front and Back View

Illustrates the physical layout and key components of the instrument's front and back.

Power Connections

Details the steps required to connect the instrument to a power source.

Interfaces

Describes the instrument's connectivity options, including USB and Ethernet ports.

Cell Compartments and Adapters

Explains the different cell compartments and the types of adapters and cells they accommodate.

Installation of Cell Adapter

Provides instructions on how to correctly install the cell adapter into the instrument.

Use of the Light Shield for Measurements

Explains the purpose and usage of the light shield for specific measurement scenarios.

Beam Path

Illustrates the optical path of the light beam within the DR 3900 spectrophotometer.

Section 4 Start up

Switch on the Instrument and Startup Process

Guides the user through powering on the instrument and its initial startup sequence.

Language Selection

Explains how to select and change the instrument's operating language.

Self-check

Describes the automatic diagnostic test performed each time the instrument is powered on.

Sleep Mode

Details how to put the instrument into and wake it from sleep mode to save power.

Power Off the Instrument

Provides instructions on how to properly shut down the instrument.

Section 5 Standard programs

Overview of Standard Programs

Provides a general introduction to the instrument's standard programs and operating modes.

Tips for Using the Touch Screen

Offers guidance on interacting with the instrument's touch screen interface effectively.

Use of the Alphanumeric Keypad

Explains how to use the on-screen keypad for data entry and programming.

Main Menu

Describes the options available in the instrument's main menu and their functions.

Instrument Setup

Covers the various settings and configurations for the instrument.

Operator ID

Details how to set up and manage operator identification for tracking measurements.

Operator RFID Tag

Explains the functionality and setup of the optional RFID tag for operator identification.

Sample ID

Guides on entering and managing sample identification tags for sample tracking.

Sample ID with Scanner Method 1

Describes using a scanner to input sample IDs using the first method.

Sample ID with Scanner Method 2

Details the process for inputting sample IDs via scanner using the second method.

Sample ID and Operator ID with RFID Kit

Explains the use of the optional RFID kit for sample and operator identification.

Security Settings

Covers the configuration of security levels and password protection for instrument access.

Assign Operator Security Level

Details how to assign specific security levels to different operator IDs.

Deactivate Password

Provides instructions on how to remove or deactivate existing passwords.

Date and Time Settings

Guides on setting and formatting the instrument's date and time.

Sound Settings

Explains how to configure various audio feedback options for the instrument.

PC and Printer Connectivity

Describes how to connect the instrument to PCs and printers for data transfer.

Printer Setup

Details the configuration options for connecting and setting up a printer.

Print Data

Explains how to print stored measurement data from the instrument.

Print Data Continuously

Covers the setup for continuous printing of measurement data.

Network Setup

Guides on configuring network connections for data transfer and instrument management.

IP Address Configuration

Details how to set up the instrument's IP address for network communication.

Network Server and Data Folder Setup

Explains how to configure network server access and data folder destinations.

Power Management Settings

Covers instrument power saving features like sleep timers and auto power-off.

Save, Recall, Send, and Delete Data

Outlines procedures for managing measurement data stored in the instrument.

Data Log Storage

Explains how the instrument stores measurement data automatically or manually.

Recall Stored Data from Data Log

Guides on retrieving measurement data previously stored in the instrument's data log.

Send Data from the Data Log

Details how to transfer data from the instrument's data log to external storage or a printer.

Delete Stored Data from Data Log

Explains how to remove measurement data from the instrument's data log.

Control Charts for AQA Log Data

Describes how to generate and interpret control charts for Analytical Quality Assurance data.

Store, Recall, Send, and Delete Wavelength Scan and Time Course Data

Covers data management operations for wavelength scans and time course measurements.

Data Storage for Wavelength Scan or Time Course

Explains the process of saving scan and time course data within the instrument.

Recall Stored Wavelength Scan and Time Course Data

Guides on retrieving previously saved wavelength scan and time course data.

Send Wavelength Scan and Time Course Data

Details methods for transferring scan and time course data to external devices or PCs.

Delete Stored Wavelength Scan and Time Course Data

Explains how to remove scan and time course data from the instrument.

Data Analysis

Introduces the instrument's data analysis capabilities and requirements.

Trends Analysis

Describes how to generate and interpret trend plots for measurement data over time.

Ratios Analysis

Explains how to perform ratio analysis on measured parameters, often using accessory kits.

Interference Check

Details the instrument's automatic detection of potential interferences in measurements.

Stored Programs

Covers how to access and run pre-programmed tests and methods.

Select Saved Test/Method and Basic Data Entry

Guides on selecting tests and entering necessary user-specific data.

Stored Program Options

Lists and describes the various options available for configuring stored programs.

Set Dilution Factor

Explains how to input a dilution factor to adjust measurement results.

Run Standard Adjust

Details the procedure for adjusting calibration curves using a known standard solution.

Set Chemical Form

Guides on selecting the appropriate chemical form for evaluating test results.

Change Default Chemical Form Setting

Explains how to set a new default chemical form for test evaluations.

Run Reagent Blank

Details the process of measuring a reagent blank to account for its value in calculations.

Carry Out Multiple Determination

Explains how to perform multiple measurements on a single sample.

Analysis of Samples

Covers the general process for analyzing samples using stored programs.

Update/Edit Tests

Provides guidance on updating and editing existing test methods.

Manual Update of Test Data

Explains how to manually update test data based on packaging information.

Program a New Test

Guides on creating and programming entirely new test methods into the instrument.

Add Stored Programs to Favorites List

Explains how to add frequently used programs to the Favorites list for quick access.

Barcode Programs

Introduces the functionality of using barcodes for automated test selection and execution.

Perform a Barcode Test

Details the steps for running a test using barcode identification.

Select Chemical Evaluation Form

Guides on choosing the correct chemical representation for displaying test results.

Basic Test-Specific and Sample-Specific Data Settings

Covers settings related to specific tests and individual samples.

Sample Blank

Explains the procedure for taking a sample blank reading to correct for sample matrix effects.

Update/Edit Barcode Tests

Details how to update or modify barcode test data, including test packaging.

Manual Update of Barcode Test

Guides on manually updating the parameters of a barcode test.

Manual Check/Revision of Test Data

Explains how to manually review and correct test data entries.

Update via the Internet

Details how to update instrument software and data using an internet connection.

Program a New Test

Guides on programming new tests, possibly for barcode methods.

Section 6 Expanded programs

User Programs

Introduces the functionality for creating and managing custom user-defined analysis programs.

Program a User Method

Guides on the process of creating a new user-defined analysis method.

Program Number and Name

Explains how to assign unique numbers and names to user-created programs.

Program Type Selection

Covers the selection of program types like Single Wavelength, Multi Wavelength, or Free Programming.

Single Wavelength Settings

Details the parameters to configure for single wavelength measurements.

Multi Wavelength Settings

Covers the configuration parameters for multi-wavelength measurements.

Calibration Settings for Single and Multi Wavelength Modes

Explains how to calibrate methods using standard solutions or formulas.

Store a User Program

Guides on saving the configured user program into the instrument's memory.

Additional User-Defined Parameters and Functions

Covers adding advanced parameters like measuring range limits and timer functions.

"Free Programming" Program Type

Introduces the advanced option for creating custom measurement sequences.

Measurement Process Definition

Explains how to define the steps and readings for a measurement process.

Enter New Element of Measuring Sequence

Guides on adding individual steps to a measurement sequence.

Enter Calibration Formula (Evaluation Formula)

Details how to input mathematical formulas for calculating results and calibration curves.

Enter Variables (Factors, Wavelength, Conversion Factors)

Explains how to input variables like factors, wavelengths, and conversion constants.

Select a User Program

Guides on selecting and running previously created user programs.

Add, Edit, and Delete User Programs from Favorites List

Covers managing user programs within the Favorites list for quick access.

Favorites Management

Explains how to recall and delete programs from the Favorites list.

Standard Addition - Monitoring/Checking Results

Introduces the standard addition method for checking accuracy and identifying interferences.

Complete a Standard Addition

Details the procedures for performing a standard addition analysis.

Single Wavelength Readings

Guides on taking measurements using the single wavelength mode.

Set Up Single Wavelength Mode

Covers the configuration options for single wavelength measurements.

Multi Wavelength Mode Readings

Introduces the multi-wavelength mode for taking measurements at multiple wavelengths.

Set Reading Mode at Different Wavelengths

Explains how to configure settings for multi-wavelength readings.

Multi Wavelength Mode Reading Completion

Details the final steps for completing a measurement in multi-wavelength mode.

Wavelength Scan Mode

Introduces the mode for recording absorbance and transmission spectra across a wavelength range.

Set Up the Wavelength Scan

Guides on configuring parameters for performing a wavelength scan.

Perform a Wavelength Scan

Details the procedure for executing a wavelength scan measurement.

Navigation of Wavelength Scan Graph/Analysis

Explains how to navigate and interpret the results of a wavelength scan.

Work with Reference Scans

Covers using reference scans for comparison with measured spectra.

Time Course of Absorbance/Transmittance

Introduces the time course mode for monitoring changes over time.

Time Course Setup Parameters

Details the settings required to configure a time course measurement.

Time Course Scan Reading

Guides on performing the actual time course scan measurement.

Analysis of Time Course Data

Explains how to analyze the data collected during a time course measurement.

Section 7 Maintenance

Cleaning Requirements

Provides instructions on how to clean the instrument, display, and cells.

Spectrophotometer Cleaning

Details specific cleaning procedures for the main unit and cell compartments.

Display Cleaning

Explains how to clean the instrument's display screen safely.

Cuvettes/Cells Cleaning

Outlines the process for cleaning cuvettes and sample cells after use.

Lamp Replacement Procedure

Provides step-by-step instructions for safely replacing the instrument's lamp.

Exchange of Replaceable Cell Compartment

Guides on how to replace the entire cell compartment if severely soiled.

Section 8 Troubleshooting

Section 9 Replacement Parts

Accessories

Lists various accessories available for purchase to enhance instrument functionality.

Replacement Parts

Lists essential replacement parts for the instrument, such as lamps and power supplies.

Section 10 Contact Information

Section 11 Warranty, Liability, and Complaints

Appendix A Help Guide

Help Guide for Stored Programs

Provides guided instructions for running pre-programmed tests available in the instrument.

Help Guide for Barcode Programs

Guides users through executing tests using barcode identification.

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