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HP 6890 series

HP 6890 series
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HP 6890 series Specifications

General IconGeneral
TypeGas Chromatograph
Column Oven Temperature RangeAmbient +4°C to 450°C
Autosampler CompatibilityYes
Maximum Temperature Ramp Rate120°C/min
Carrier GasHelium, Hydrogen, Nitrogen
Detector OptionsFID, TCD, ECD, NPD, FPD
Inlet OptionsSplit/Splitless, PTV
CommunicationRS-232
Power Requirements50/60 Hz
Injection PortsUp to 2
Carrier Gas ControlElectronic Pneumatics Control (EPC)
WeightApproximately 55 kg

Summary

Safety Information

General Safety Warnings and Symbols

Covers warnings, cautions, and safety symbols for safe operation and user protection.

In Vitro Diagnostic Application Information

Environmental Compliance Statements

Flame Photometric Detector Operation

Detector Operating Principle

Explains the process of sample combustion, light emission, and detection by the photomultiplier tube.

Detector Performance Characteristics

Linearity in Detection Modes

Describes how emission intensity relates to concentration in sulfur and phosphorus modes.

Quenching Effects and Mitigation

Explains hydrocarbon and self-quenching, and how to reduce them with proper practices.

Photomultiplier Tube Saturation

Details how high light intensity can saturate the PMT and the symptoms to watch for.

Detector Components and Settings

Optical Filters for Detection

Describes sulfur and phosphorus filters, their colors, and transmission wavelengths.

Fused Silica Liner Usage

Explains the use of inert fused silica liners for column connection and sample integrity.

Detector Temperature Management

Discusses optimal temperatures to prevent condensation and thermal decomposition.

Conditions Preventing Detector Operation

Lists specific conditions like low temperature, gas flow, or ignition failure that stop detector function.

Detector Installation and Configuration

Detector Shutdown Procedures

Explains how a critical gas shutdown affects the detector's operation.

Special FPD Adapters

Details adapters for capillary and PTFE columns to connect to the FPD.

Capillary Column Installation Steps

Provides step-by-step instructions for installing fused silica columns into the FPD.

Changing Wavelength Filters

Installation and Connectivity Requirements

Installation Restrictions and Zones

Covers mounting positions and heater assignments for single and dual wavelength FPDs.

Drip Tubing Installation

Explains the necessity and routing of drip tubing for water vapor management.

Software Compatibility Requirements

Specifies required HP ChemStation software versions for single and dual wavelength FPDs.

Detector Heating Configuration

Describes how AUX heater setpoints are automatically managed with the detector heater.

Electronics Module Components

Lit Offset Configuration

Procedure to Change Lit Offset

Step-by-step guide to adjust the Lit offset setpoint for flame detection.

Flame Ignition Sequence

Lighting the Flame

Manual Flame Ignition

Instructions to manually start the flame ignition sequence via the control table.

Automatic Flame Relighting

Explains the automatic relighting process and detector shutdown on failure.

Electrometer Control

Electrometer OnOff Setting

How to turn the electrometer on or off and the implications for PMT safety.

Electrometer Data Rates and Fast Peaks

Discusses analog output speeds and the 'fast peaks' feature for data acquisition.

Dual Wavelength FPD Operation

Operating the FPD

Recommended Temperature and Flow Rates

Table detailing suggested gas flows and temperatures for Sulfur and Phosphorus modes.

FPD Control Table and Settings

Makeup Gas Flow Modes

Explains different makeup gas flow modes and how to select them.

Procedure: Using the FPD

Troubleshooting Flame Ignition

Leak Testing Procedures

Cleaning and Replacing Detector Components

Windows, Filters, and Seals Maintenance

Instructions for cleaning or replacing optical windows, filters, and seals in the FPD.

Cleaning and Replacing the Jet

Replacing the Transfer Line Fused Silica Liner

Replacing the Photomultiplier Tube (PMT)

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