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FreeZone 7750000
Labconco FreeZone 7750000 User Manual
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Fr
eeZone® Benchtop and Console
Fre
eze
D
r
y Sy
s
t
em
s
Models
775
0000
7751000
775
0001
7751001
775
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7751003
775
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4
775100
4
User’s Manual
LABCONCO CORPORA
TION
8811 PROSPECT A
VENUE
KANSAS CITY
, MO 64132-2696
800-821-5525, 816-333-8811
FA
X 816-363-0130
E-MAIL labconco@labconco.com
HOME P
AGE www.labconco.com
Labconco’
s Mascot,
Labby the LABster
Register your product online at
www
.labconco.com/productreg.html
or return the attached card and
receive
FREE LabbyWear
™
!
2
Table of Contents
default chapter
4
Table of Contents
4
Chapter 1: Introduction
6
Freeze Dry Process
6
Freeze Dry Rates
7
Freeze Dry Capacity
9
Samples Containing Volatile Substances
10
About this Manual
10
Typographical Conventions
12
Your Next Step
12
Chapter 2: Prerequisites
15
Electrical Requirements
15
Location Requirements
15
Vacuum Pump Requirements
15
Space Requirements
16
Your Next Step
16
Chapter 3: Getting Started
16
Unpacking Your Freeze Dryer
19
Freeze Dryer Components
19
Setting up Your Freeze Dryer
20
Component Orientation
20
Vacuum Pump Connection
21
Electrical Connection
21
Solvent Safety Precautions
21
Your Next Step
23
Chapter 4: Using Your Freeze Dryer
24
Freeze Dryer Controls
25
Operation Checklist
27
Vacuum Pump Ballast Setting
27
Operating the Freeze Dryer
28
Automatic Start-Up
28
Manual Start-Up
28
Adding Sample
29
Alarms & Informational Messages
31
Shut down
32
Defrosting
33
Chapter 5: Maintaining Your Freeze Dryer
35
Chapter 6: Using the Recorder Jack
36
Recorder Jack Pin Configuration
36
Computer Connection
37
Chapter 7: Troubleshooting
42
Vacuum Pump
42
Gaskets, Tubing, Connections, Sample Valves
43
System Components & Collection Chamber Isolation
45
Refrigeration Module Operation
47
Appendix A: Freeze Dryer Components
48
Appendix B: Freeze Dryer Dimensions
55
Appendix C: Freeze Dryer Specifications
56
Electrical Specifications
56
Environmental Conditions
57
Wiring Diagram (115V)
58
Wiring Diagram (230V)
59
Appendix D: Freeze Dryer Accessories
60
Declaration of Conformity
70
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Labconco FreeZone 7750000 Specifications
General
Brand
Labconco
Model
FreeZone 7750000
Category
Laboratory Equipment
Language
English
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