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200A Series
PerkinElmer 200A Series User Manual
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S
ERIES
200
A
F
LUORESCENCE
D
ETECTOR
User’s Guide
LIQUID CHROMAT
OGRAPH
Y
2
Table of Contents
Default Chapter
3
Table of Contents
3
Introduction
5
Note
7
Product Warranty
8
About this Manual
10
Conventions Used in this Manual
11
Notes, Cautions and Warnings
11
Warning Signs on the Instrument
14
Safety Practices
15
Overview
18
Common Safety Precautions
19
Prior to Use
19
In Use
19
Installation, Maintenance, and Relocation
19
Ignition of Flammable Chemicals
20
Explosion of Vapor from Flammable Chemicals
20
Electric Shock Due to Contact with Inside of Instrument
21
Electric Shock Due to Improper Grounding
21
Injury Due to Xenon Lamp Explosion
21
Lamp Replacement
21
Lamp Installation
22
Lamp Disposal
22
Inflammation or Injury Due to Toxic or Corrosive Solvent
23
Touching Hot Part Could Result in Burns
23
Direct Viewing of Xenon Lamp Could Cause Eye Damage
23
Heavy Instrument
23
Prevention of Instrument Tipover
23
Precautions on Use of Solvents
24
Disposal of Waste Solution
25
Accuracy and Precision of Measured Values
25
Possible Carryover
25
Before Turning on Xenon Lamp Again
25
General Operating Conditions
27
Environmental Conditions
28
Electrical Safety
29
EMC Compliance
30
Europe
30
United States
30
WEEE Instructions for Perkinelmer Products
31
Warning Labels on the Instrument
32
System Description
35
Overview
37
Control Switches and Indicators
38
Keyboard on the UI Pad (Option)
39
The Rear Panel
42
Description of Fluorometry
44
Principle of Fluorometry
44
Advantages of Fluorometry
45
Notes on Fluorescence Analysis
47
Principle of Operation
51
Features of Light Source
52
Specifications
53
Installation
55
Unpacking
57
Installation Conditions
58
Installation Space
58
Environmental Conditions for an Installation Location
59
Checking the Contents
59
Assembling
60
Removal of Transport Screws
60
Tubing Arrangements
61
UI Pad
62
Spare Parts Available
65
Operation
67
General Information about Entering Parameters
71
Setup
72
Selecting the Communication Channel
72
Setting the Liquid Crystal Display Contrast
73
Setting of Standard Xenon Lamp Lifetime
74
Operating Instructions
76
To Adjust the Auto Zero
76
Setting the Wavelength
76
Setting the Utility
77
Setting the GLP Function
84
Spectrum Measurement
91
Setting of Recorder and Spectrum Output Factors
95
Operation of Marker
98
Setting of Time Program
98
Edit the Wavelength Program
105
Shutdown Procedure
108
Flushing the Flow Cell after Use
109
Before Performing Analysis
110
Characteristics of Organic Solvents
112
Cautions on Static Electricity
116
Maintenance
117
Operational Check
119
Performance Check
120
Energy Check of Xe Lamp
120
Check of Wavelength Accuracy by Using Hg Lamp
120
Check of Sensitivity
120
Check and Calibration of Wavelength Accuracy
130
Check of Leak Sensor
132
Periodic Checks
134
Maintenance & Inspection Methods
135
Energy Check of Xe Lamp
135
Wavelength Accuracy Check Using Hg Lamp
135
Check of Lamp Logbook
135
Check and Washing of Flow Cell Unit
136
Check and Washing of Flow Cell
136
Disassembly and Cleaning of Flow Cell
138
Leakage from the Flow Cell
140
Cautions on Storage of the Flow Cell
141
Lamp Replacement
142
How to Replace the Xenon Lamp
142
Fuse Replacement
153
Troubleshooting
155
Warnings
157
Troubleshooting
158
Error Messages
160
Appendix
163
Description of Contact Signals
165
Outline
165
Terminology
166
Index
171
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PerkinElmer 200A Series Specifications
General
Brand
PerkinElmer
Model
200A Series
Category
Laboratory Equipment
Language
English
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