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PerkinElmer OilExpress 4 User Manual

PerkinElmer OilExpress 4
152 pages
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OilExpress 4
Oil Condition Monitoring System
User’s Guide
MOLECULAR SPECTROSCOPY

Table of Contents

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PerkinElmer OilExpress 4 Specifications

General IconGeneral
BrandPerkinElmer
ModelOilExpress 4
CategoryLaboratory Equipment
LanguageEnglish

Summary

Introduction to the Manual

About this Manual

Provides information about the user guide's scope and purpose, including installation notes and related documents.

Using this Guide

Offers recommendations on how to use the guide effectively, suggesting sections to read in sequence for system understanding.

Document Conventions

Conventions Used in this Manual

Explains text formatting like normal text, bold text, and uppercase for keys used in the manual.

Part Numbers

Defines how PerkinElmer part numbers are presented in the document.

Notes, Warnings and Cautions

Details the standard formats used to highlight special circumstances and warnings.

OilExpress 4 System Description

OilExpress 4 Oil Condition Monitoring Systems

Introduces the OilExpress 4 system and its optimization for FT-IR analysis of lubricants.

Introduction to Oil Analysis by Infrared Spectroscopy

Explains the principles of IR analysis for monitoring lubricant condition, additive depletion, and contamination.

Warnings and Safety Information

Overview of Safety Information

Describes general safety practices and precautions for operating the OilExpress 4 System.

OilExpress 4 System Safety Summary

Provides a summary of key safety points and precautions for the OilExpress 4 System.

General and Electrical Safety

Covers general operating conditions and electrical safety requirements for the system.

Mechanical Hazards and Environment

Details mechanical hazards associated with the autosampler and environmental requirements for system operation.

Flammable Solvents and Material Safety

Provides guidance on the safe use, handling, and disposal of flammable solvents and samples.

Material Safety Data Sheets

Explains how to obtain and use Material Safety Data Sheets (MSDS) for hazardous materials.

Overview of the OilExpress 4 System

System Specifications

Lists the technical specifications for the OilExpress 4 system, including throughput and sample volumes.

Liquid Autosampler and Components

Describes the liquid autosampler, its features, and key components like the robotic arm and VersaTips.

Connection Panel

Details the connection panel on the autosampler, including power and communication ports.

Varispan Pipetting Arm and VersaTips

Explains the Varispan pipetting arm, its sampling tips, and their functionality for sample aspiration.

System Liquid Container(s)

Describes the system liquid container, its placement, and associated part numbers.

Labware Configurations

Covers labware positioning on the autosampler deck, including deck layouts and sample rack types.

Sample Racks

Details the types of sample racks supported, such as 96-position and 32-position racks.

Tip Boxes

Explains the use of tip boxes for clean disposable tips and for depositing used tips.

Injection Station

Describes the injection station's function in dispensing samples and cleaning solvent to the flow cell.

Autosampler Safety Shield and Stop Button

Spectrometer Module

Spectrometer Sample Compartment

Details the sample compartment of the spectrometer, including beam path and window types.

Flow Cell

Describes the two-port flow cell, its installation, and connection to the injection station and waste container.

Liquid Presence Sensor

Explains the liquid presence sensor's role in detecting sample flow and its connection to the FCM.

Connections on the Spectrometer

Illustrates the power adaptor and communication ports on the rear of the spectrometer.

Fluid Control Module

Connections on the FCM

Shows the electrical, fluid, and exhaust connections on the rear of the Fluid Control Module (FCM).

Electrical Connections on the FCM

Details the electrical connections for the FCM, including power supply and USB hub connections.

Fluid connections on the FCM

Illustrates the fluid tubing connections for the FCM, including waste and exhaust ports.

Waste Container

Spectrometer and FCM Mounting System

Ultrasonic Liquid Level Sensor Bar (Optional)

FT-IR-Only Analysis with the 96-position Rack Type

Provides specific notes for FT-IR only analysis using the 96-position rack with the sensor bar.

Ultrasonic Height Sensing Errors dialog

Oil Dilution

Overview of the FT-IR Analysis Procedure

Single-spectrometer System

Details the step-by-step procedure for performing FT-IR analysis on a single-spectrometer system.

Dual-spectrometer (DUO) System

Outlines the FT-IR analysis procedure for a dual-spectrometer system.

Getting Started with OilExpress 4

Overview of Getting Started

Introduces the basic functionality of the OilExpress 4 software covered in this section.

Starting OilExpress 4 Software

Provides instructions on how to launch the OilExpress 4 software application.

The OilExpress 4 Window and Controls

Describes the main OilExpress 4 software window, including menus, toolbar, navigation, and status bars.

Sample Preparation and Priming

Covers sample preparation steps and the system priming procedure before analysis.

Defining the Sampling Heights

Explains how to set system options for sampling heights using fixed or ultrasonic methods.

Saving, Exporting, and Reporting Data

Details how to save, export spectra, export results as CSV, and generate reports.

Running an Analysis

Guides users through the process of setting up and running a batch analysis.

Modifying Scan Settings

Explains how to change scan and instrument settings, including resolution and AVI correction.

Absolute Virtual Instrument (AVI)

Covers AVI correction and calibration objectives for consistent instrument performance.

System Validation and Checks

Describes system validation procedures like running control samples and system checks.

Maintenance and Troubleshooting

Flow Cell Maintenance Procedures

Covers flow cell maintenance, cleaning using software, and removal/installation procedures.

Autosampler Maintenance Procedures

Details daily and weekly preventative maintenance for the autosampler, including priming and cleaning.

Spectrometer Maintenance Procedures

Outlines spectrometer maintenance tasks and use of the Adjustments Toolbox.

System Configuration Changes (DUO Systems)

Explains how to change to a single-spectrometer system for DUO systems during maintenance.

Removing and Installing the Sample Shuttle

Provides instructions for removing and installing the sample shuttle from the spectrometer.

Fluid Control Module Maintenance

Covers cleaning and checking connections for the Fluid Control Module (FCM).

Moving the System

Recommends contacting a service representative for autosampler deck calibration after moving the system.

Troubleshooting Common Issues

Lists common problems, their possible causes, and corrective actions for the OilExpress 4 system.

Spares and Consumables

Appendices

Appendix 1: Decontamination

Provides information and procedures for decontaminating equipment before return or service.

Appendix 2: WEEE Instructions for PerkinElmer Products

Details Waste Electrical and Electronic Equipment (WEEE) disposal instructions and environmental objectives.

Appendix 3: Liquid Handling

Explains the principles of liquid handling, including sampling, aspiration, and dispensing for the autosampler.

Appendix 4: Fluid Path Materials

Lists materials in contact with samples and cleaning fluids within the system's fluid path.

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