Pickering Laboratories PCX 5200 - Default Chapter; Table of Contents

PCX 5200 User’s Manual Contents
Contents
Please Read ..................................................................................................BYS-1
Symbols.........................................................................................................BYS-1
Chapter 1 • Introduction
Why Post-coIumn Derivatization? ...................................................................... 1-1
How Does It Work?............................................................................................. 1-1
What Are the Requirements? ............................................................................. 1-1
Pickering PCX5200 ............................................................................................ 1-2
Reagent Delivery......................................................................................................................1-2
Column Protection....................................................................................................................1-2
Supplement—The Elements of an HPLC with Post-column System.................. 1-4
Design of an HPLC ..................................................................................................................1-4
A Simpler View of an HPLC .....................................................................................................1-5
Designing a Post-column System ............................................................................................1-5
Chapter 2 • PCX5200 System Components
PCX5200 Post-column Instrument ..................................................................... 2-1
Getting to Know Your PCX5200 ......................................................................... 2-1
Front Panels .............................................................................................................................2-1
Internal .....................................................................................................................................2-3
Rear Panel ............................................................................................................................... 2-4
Column Oven ........................................................................................................................... 2-6
Reagent Reservoirs .................................................................................................................2-8
External Reagent Pressurization System ................................................................................ 2-9
Keypad and Liquid Crystal Display User Interface ................................................................ 2-10
Keypad Examples............................................................................................. 2-13
Loading a Preset ....................................................................................................................2-13
Saving a Preset ......................................................................................................................2-15
Flow Diagrams.................................................................................................. 2-18
PRESET Key ..........................................................................................................................2-18
PROG Key..............................................................................................................................2-18
Specifications ................................................................................................... 2-20
Wetted Materials, PCX5200................................................................................................... 2-20
PCX5200 PEEK .....................................................................................................................2-20
Ratings ...................................................................................................................................2-20
RS232 Serial Port .................................................................................................... ....2-21
Downloading firmware............................................................................................................2-21
Radio frequency .....................................................................................................................2-21