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Pike MIRacle ATR User Manual

Pike MIRacle ATR
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MIRacle
TM
Single Reflection Horizontal
ATR Accessory
Installation and User Guide
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Pike MIRacle ATR Specifications

General IconGeneral
CompatibilityFTIR Spectrometers
Angle of Incidence45 degrees
TypeATR (Attenuated Total Reflectance) Accessory
Crystal MaterialZnSe
Pressure DevicePressure clamp with torque knob for consistent pressure
ApplicationsLiquid and Paste Samples

Summary

MIRacle Pressure Clamp Options

Digital High-Pressure Clamp with Meter

Features a digital meter for precise pressure control.

High-Pressure Clamp

Standard clamp for high pressure applications.

Micrometer Clamp

Offers precise pressure adjustment via a micrometer screw.

MIRacle Accessory Installation

Positioning in Spectrometer

Placing the accessory correctly in the FTIR sample compartment.

Fastening the Accessory

Securing the accessory to the FTIR base plate.

Final Positioning

Ensuring the accessory is ready for optical alignment.

MIRacle Accessory Adjustment

Angle Adjustment

Adjusting mirrors for maximum throughput using thumbscrews.

Height Adjustment

Adjusting mirrors for maximum throughput using hex wrench.

MIRacle Performance Verification

Background Spectrum Collection

Collecting an open beam background spectrum.

MIRacle ATR Spectrum Collection

Collecting a spectrum of the MIRacle ATR.

MIRacle Sampling Procedures

MIRacle Configuration for Solid Sampling

MIRacle Pressure Clamp Tip Attachments

Micrometer Pressure Clamp Operation

Micrometer Pressure Settings

Table of micrometer settings and approximate pressures.

Micrometer Clamp Procedure

Step-by-step guide for using the micrometer clamp.

MIRacle High-Pressure Clamp Operation

High-Pressure Clamp Installation

Steps to install the high-pressure clamp onto the accessory.

MIRacle Crystal Cleaning Procedures

MIRacle Precautions and Safety

MIRacle Pressure Clamps