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Thermo Scientific Dionex User Manual

Thermo Scientific Dionex
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Dionex Integral Process Analytical
Systems Operators Manual
Document No. 065250
Revision 06
March 2020

Table of Contents

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Thermo Scientific Dionex Specifications

General IconGeneral
CategoryAnalytical Instruments
BrandThermo Scientific
ManufacturerThermo Fisher Scientific
Product LineDionex
Detector TypesConductivity, Electrochemical, UV-Vis
SoftwareChromeleon
Compliance21 CFR Part 11
Column TypesIon Exchange

Summary

1 Introduction

1.1 Dionex Integral Process Analytical Systems

Overview of system design, capabilities, and main components (AE, LE, SP, SS).

1.2 Operator's Manual Overview

Describes the structure and content of the operator's manual.

1.3 Related Documentation

Lists other available manuals and resources for the system.

1.4 Safety Information

Covers safety messages, warnings, precautionary statements, and symbols.

1.5 Regulatory Compliance

Details EMC standards, safety specifications, and EU directives.

2 Dionex Integral System Configurations

2.1 Example Configurations

Illustrates typical system configurations with various modules.

3 SP Sample Preparer Description

3.1 SP Overview, Versions, and Enclosures

Introduces the SP, its versions (SP1, SP2, generic) and enclosure types.

3.2 SP Power, Connections, and Leak Detection

Details power, USB, leak sensor, and drain port functions.

3.3 SP Components and Configurations

Covers components (valves, pumps, vessels) and panel configurations.

3.4 SP Options and Input/Output Lines

Details I/O lines, analog inputs, TTL/relay, sensors, and control options.

4 SS Stream Selector Description

4.1 SS Overview and Stream Selection

Introduces the SS and its stream selection capabilities.

4.2 SS Enclosures, Power, and Connections

Covers enclosure types, power, computer connections, and leak sensor.

5 AE Analyzer Enclosure Description

5.1 AE Overview and Enclosure Types

Introduces the AE enclosure and its NEMA environmental ratings.

5.2 AE Exterior and Interior Features

Details exterior features (Emergency Off) and interior features (shelves, outlets).

5.3 AE Power, Connections, and Optional Features

Covers power, computer connections, TTL/relay, ventilation, A/C, purge, and tower light.

6 LE Liquids Enclosure Description

6.1 LE Overview and Containers

Introduces the LE enclosure and types of containers it accommodates.

6.2 LE Control Panel and Pneumatics

Explains the control panel, gas pressure, and pneumatic requirements.

6.3 LE Liquid and Gas Connections

Details tubing and fittings for liquid and gas connections.

7 Startup, Operation, and Shutdown

7.1 Initial Startup Procedures

Steps for preparing site, connecting facilities, cables, and inlet lines.

7.2 System Setup and Calibration

Procedures for initial power-on, software setup, and system calibration.

7.3 Routine Operation

Guides for routine startup, operation monitoring, and checks.

7.4 System Shutdown Procedures

Instructions for short-term and long-term system shutdowns.

8 Maintenance

8.1 Daily Maintenance

Daily checks for gas pressure, reagent supplies, and lines.

8.2 Weekly Maintenance

Weekly tasks including standard solutions and pump maintenance.

8.3 Biweekly Maintenance

Biweekly tasks for reagent reservoirs and eluent trap columns.

8.4 Monthly Maintenance

Monthly tasks like replacing in-line filters and guard columns.

8.5 Quarterly Maintenance

Quarterly tasks including pump seals and rotary valve maintenance.

9 Troubleshooting

9.1 Troubleshooting Strategies

General strategies for isolating and resolving system problems.

9.2 Audit Trail Error Messages

Explains error messages, severity levels, and their meanings.

9.3 Liquid Leaks and Alarms

Addresses liquid leaks, leaking fittings, and broken lines.

9.4 Air and Gas Leaks

Discusses detection and resolution of air and gas leaks.

9.5 System or Component Power Issues

Troubleshoots issues where the system or components do not power up.

10 Service

10.1 Eliminating Fluid System Restrictions

Procedure to identify and remove restrictions in the fluid system.

10.2 Replacing Pump Check Valve Cartridges

Step-by-step guide for replacing pump check valve cartridges.

10.3 Replacing Pump Check Valves

Instructions for replacing defective pump check valves.

10.4 Replacing Pump Seals

Procedure for replacing pump piston and backup seals.

10.5 Replacing the Waste Valve Seal

Guide for replacing the seal in the waste valve.

10.6 Accessing SP Electronics Board

Provides instructions to access the SP electronics board.

10.7 Replacing SP Solenoid Valve

Steps for replacing solenoid valves on the SP panel.

10.8 Pump Speed and Calibration

Adjusting peristaltic pump speed and calibrating system components.

10.9 Changing Power Fuses

Steps for safely replacing main power fuses for SP or SS.

A Specifications

A.1 Environmental Specifications

Operating temperature and humidity ranges for all components.

A.2 AE and LE Enclosure Specs

Electrical and physical specifications for AE and LE enclosures.

A.3 SP/SS Specs

Electrical and physical specs for SP/SS, including pumps and valves.

A.4 Air Conditioner/Heater Specs

Electrical and physical specifications for the air conditioner/heater.

B Reordering Information

C TTL and Relay Installation Instructions

C.1 SP TTL and Relay Kit Installation

Provides parts and steps for installing SP TTL and relay control.

C.2 AE TTL and Relay Kit Installation

Details installing TTL/relay connectors on AE and connecting to SP.

C.3 Installing TTL and Relay Breakout Boards

Instructions for connecting wires to breakout boards and installing them.

C.4 AE Tower Light Kit Installation

Steps for mounting the tower light and connecting its cable.

D AE Purge Kit Installation Instructions

D.1 Overview

Lists parts and requirements for the AE purge kit installation.

D.2 Installation Procedure

Steps for installing the purge control unit and related components.

E Peristaltic Pump Kit Installation Instructions

E.1 Overview

Lists parts and requirements for installing a peristaltic pump.

E.2 Installation Procedure

Covers installing pump, cable, tubing, and configuring in Chromeleon.

F Liquid Level Sensor Installation Instructions

F.1 Overview

Lists parts and requirements for installing liquid level sensors.

F.2 Installation Procedure

Steps for attaching the sensor to containers and connecting the cable.

G Thermal Options Installation Instructions

G.1 Installing Thermal Control Board

Details parts and steps for installing the thermal control board.

G.2 Installing Vial Cooler

Steps for mounting the vial cooler and connecting its cable.

G.3 Installing Heated Dilution Vessel

Procedures for connecting and installing the heated dilution vessel.

H Lockout Instructions for AE, SP, or SS

H.1 Lockout Device Installation Procedure

Steps for notifying, turning off power, and installing lockout devices.

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