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Thermo Scientific TRACE 1600 User Manual

Thermo Scientific TRACE 1600
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Thermo Scientific
TRACE 1600/1610
Hardware Manual
Gas Chromatographs
MI-317000-0033 Revision A April 2022

Table of Contents

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Thermo Scientific TRACE 1600 Specifications

General IconGeneral
TypeGas Chromatograph
ColumnCapillary
Oven Temperature RangeAmbient +4 °C to 450 °C
Maximum Heating Rate120 °C/min
Maximum Number of Injectors2
Temperature ProgrammingYes
DetectorsFID, TCD, ECD, NPD, FPD
Data System CompatibilityChromeleon Chromatography Data System (CDS)
Autosampler CompatibilityYes

Summary

Declaration and Regulatory Compliance

Safety

Information regarding safety precautions and warnings for instrument operation.

Electromagnetic Compatibility

Details on compliance with electromagnetic compatibility standards.

Safety Information

Safety Alerts and Important Information

Guidance on following precautionary notices and understanding safety symbols and signal words.

Safety Symbols and Signal Words

Explanation of WARNING and CAUTION signal words and associated safety symbols.

Hydrogen Safety Precautions

Hydrogen Connection Guidelines

Guidelines for safely connecting hydrogen to the system, covering piping, fittings, and valves.

Purchasing Hydrogen

Guidelines for purchasing hydrogen, recommending generators and proper use.

Properly Storing Hydrogen

Guidelines for storing compressed hydrogen gas and cryogenic liquid hydrogen safely.

1 Installation

Positioning the TRACE 1600/1610

Instructions for correctly placing the TRACE 1600/1610 instrument on a workbench.

Installing the Injector and Detector Modules

Procedures for installing front/back injector and detector modules into their respective housings.

Making the Gas Supply Plumbing Connections

Instructions for connecting gas supply lines to the GC gas inlets using proper fittings.

Testing for Leaks

Procedure to test gas supply lines for leaks after connecting them to the GC.

Connecting the Oven Cryogenic System

Instructions for connecting a coolant supply (CO2 or N2) to the GC's cryogenic cooling option.

Connecting the PTV/PTVBKF Cryogenic System

Instructions for connecting a coolant supply for PTV/PTVBKF injectors with cryogenic cooling.

Coupling to a Mass Spectrometer

Instructions for opening the duct to introduce the transfer line inner tube into the GC oven for MS coupling.

Installing the Autosampler

Instructions for installing and connecting TriPlus RSH, TriPlus 100 Liquid Sampler, or AI/AS 1610 autosamplers.

Installing the Data System Software

Steps for installing the Chromeleon and SII for Xcalibur data systems software on a PC.

Making Power Connections

Instructions for connecting the GC and external modules to the power supply.

Setting the LAN Communication

Procedures for setting the desired IP address and LAN communication port for the GC.

Column Installation Requirements

Guidelines for positioning and connecting capillary columns within the GC oven.

Installing the Column the First Time

Instructions for installing a capillary column, connecting it, and performing initial conditioning.

2 Performing Routine Maintenance

Read Me First

Important safety and operational notes before performing routine maintenance.

Maintenance Supplies and Tools

List of necessary supplies and tools for performing routine maintenance on the GC.

Powering On the TRACE 1600/1610

Step-by-step instructions for powering on the GC instrument.

Powering Off the TRACE 1600/1610

Procedure for safely shutting down the GC instrument.

Cleaning the Instrument Externally

Instructions for cleaning the exterior of the GC instrument to remove dirt and debris.

Replacing a Column

Procedure for replacing the GC column when performance degrades or troubleshooting indicates maintenance.

3 Performing Injectors Routine Maintenance

Maintaining a Split/Splitless Injector (SSL)

Instructions for maintaining the Instant Connect Split/Splitless injector (SSL).

Maintaining a Split/Splitless Injector with Backflush (SSLBKF)

Procedures for maintaining the SSLBKF injector for backflush applications.

Maintaining a Gas Sampling Valve Injector (GSV)

Instructions for maintaining the Instant Connect Gas Sampling Valve injector (GSV).

Maintaining an Instant Connect Helium Saver Injector (HeS-S/SL)

Procedures for maintaining the Instant Connect Helium Saver Injector Module (HeS-S/SL).

Maintaining a Programmable Temperature Vaporizing Injector (PTV)

Instructions for maintaining the Instant Connect Programmable Temperature Vaporizing injector (PTV).

Maintaining a Programmable Temperature Vaporizing Injector with Backflush (PTVBKF)

Procedures for maintaining the PTVBKF injector for backflush applications.

4 Performing Detectors Routine Maintenance

Maintaining a Flame Ionization Detector (FID)

Instructions for maintaining the Instant Connect Flame Ionization Detector (FID).

Maintaining a Nitrogen Phosphorous Detector (NPD)

Procedures for maintaining the Instant Connect Nitrogen Phosphorous Detector (NPD).

Maintaining a Thermal Conductivity Detector (TCD)

Instructions for maintaining the Instant Connect Thermal Conductivity Detector (TCD).

Maintaining an Electron Capture Detector (ECD)

Procedures for maintaining the Instant Connect Electron Capture Detector (ECD).

Maintaining a Flame Photometric Detector (FPD)

Instructions for maintaining the Instant Connect Flame Photometric Detector (FPD).

Maintaining a Pulsed Discharge Detector (PDD)

Information on maintenance for the Pulsed Discharge Detector (PDD).

5 GC Main Frame Advanced Maintenance

Removing/Replacing the GC Top Cover

Instructions for removing and replacing the GC's top cover to access internal compartments.

Removing/Replacing the GC Left Side Panel

Procedure for removing and replacing the GC's left side panel.

Removing/Replacing the GC Right Side Panel

Instructions for removing and replacing the GC's right side panel.

Removing/Replacing the GC Back Cover

Procedure for removing and replacing the GC's back cover for accessing rear compartments.

Removing/Replacing the GC Front Door Cover

Instructions for removing and replacing the GC's front door cover.

Removing/Replacing the Electronic Module

Procedures for removing and replacing the instrument's Electronic Module.

Replacing the Oven Heater Baffle

Instructions for replacing the complete oven heater baffle assembly.

Replacing the Oven Heater Temperature Sensor

Procedure for replacing the oven heater temperature sensor.

Replacing the Oven Motor

Instructions for replacing the oven motor, requiring removal of several parts.

Replacing the Flap Motor

Procedure for replacing the oven flap motor and cooling duct assembly.

6 Injectors Advanced Maintenance

Baking-out Contaminants from SSL, SSLBKF, HeS-S/SL, PTV, and PTVBKF Injectors

Procedure to remove contaminants from SSL, SSLBKF, HeS-S/SL, PTV, PTVBKF injectors.

Removing/Replacing an Injector Module

Instructions for removing/replacing a front/back injector module.

Cleaning the SSL Injector Body

Procedures for cleaning the SSL injector body.

Cleaning the PTV Injector Head Assembly

Procedures for cleaning the PTV injector head assembly.

Cleaning the PTVBKF Injector Head Assembly

Procedures for cleaning the PTVBKF injector head assembly.

7 Detectors Advanced Maintenance

Removing/Replacing a Detector Module

Instructions for removing/replacing a front/back detector module.

Maintaining a Flame Ionization Detector (FID)

Instructions for maintaining the Instant Connect Flame Ionization Detector (FID).

Maintaining a Nitrogen Phosphorous Detector (NPD)

Procedures for maintaining the Instant Connect Nitrogen Phosphorous Detector (NPD).

Maintaining a Thermal Conductivity Detector (TCD)

Instructions for maintaining the Instant Connect Thermal Conductivity Detector (TCD).

Maintaining an Electron Capture Detector (ECD)

Procedures for maintaining the Instant Connect Electron Capture Detector (ECD).

Maintaining a Flame Photometric Detector (FPD)

Instructions for maintaining the Instant Connect Flame Photometric Detector (FPD).

8 Installing Optional Kits

Installing the Oven Exhaust Kit

Instructions for installing the optional oven exhaust kit to vent hot air away from the working area.

Installing the Merlin Microseal High Pressure Valve Kit

Procedures for installing the Merlin Microseal High Pressure Valve kit on specific injectors.

Installing the Purge & Trap Adapter Kit on the SSL/SSLBKF Injector

Instructions for installing the Purge & Trap Adapter kit for use with a Purge & Trap system.

Installing the Packed Column Adapters

Procedures for installing adapters for connecting metal packed columns to injectors and detectors.

Installing the HS Adapter Kit on the SSL/SSLBKF Injector

Instructions for installing the HS Adapter kit for use with a TriPlus 300 Headspace sampling system.

Installing the Large Volume Splitless Kit

Procedures for installing the Large Volume Splitless kit for introducing large liquid samples.

Connecting a SSL/PTV Backflush System

Instructions for connecting SSLBKF/PTVBKF injector modules with precolumn and capillary column.

Connecting a SSL/PTV Backflush System for High Temperature

Procedures for connecting SSLBKF/PTVBKF injectors with precolumn and capillary column for high temperature applications.

Installing the NoVent Microfluidics

Instructions for installing the NoVent Microfluidics on TRACE GC and mass spectrometer.

Installing a FTIR Make-up Module

Procedures for installing the FTIR Make-up module for connection with FT-IR Spectrometer.

Installing the Hot Injection Adapter Kit on the SSL/SSLBKF Injector

Instructions for installing the Hot Injection Adapter kit for use with external gas sampling devices.

Performing the Dual FPD Detector Configuration

Instructions for performing Dual FPD configuration by connecting a second photomultiplier tube.

Installing the Pressure Regulator Kit for Gas Sampling Valve

Instructions for installing a kit to adjust carrier gas pressure for GSV injector.

Installing the Packed Columns Support Kit

Procedures for installing the support kit for packed columns into the GC oven.

Installing the ECD Exhaust Vent Kit

Instructions for installing the ECD Exhaust Vent Kit to vent exhaust gases to a fume hood.

9 Adding Modules

Adding a SSL, SSLBKF, PTV, or PTVBKF Injector Module

Instructions for adding front/back SSL, SSLBKF, PTV, or PTVBKF injector modules.

Adding a GSV Injector Module

Procedures for adding front/back Gas Sampling Valve injector modules.

Adding a FID, TCD/TCD In-Series, ECD, or FPD Detector Module

Instructions for adding front/back FID, TCD/TCD In-Series, ECD, or FPD detector modules.

Adding a NPD Detector Module

Procedures for adding front/back NPD detector modules.

Adding an Aux Temperature/Cryo Module

Instructions for updating the GC with the Aux Temperature/Cryo module.

Adding a Helium Saver Injector Module

Procedures for installing the Instant Connect Helium Saver Injector Module (HeS-S/SL).

Adding a PDD Module

Instructions for adding front/back PDD detector modules.

Adding a Generic Detector Interface

Procedures for installing detector and control modules of the Generic Detector Interface.

Adding an Analog Output Interface

Instructions for installing the Analog Output Interface (AOI) on the GC.

10 Adding Systems

Adding the Oven Cryo System

Instructions for installing and configuring the Oven Cryo system on TRACE 1600/1610.

Adding the PTV and PTVBKF Cryo System

Procedures for installing and configuring PTV/PTVBKF Cryo system on TRACE 1600/1610.

Adding an Auxiliary Gas System

Instructions for updating TRACE 1600/1610 with the Auxiliary Gas System.

Adding the Hydrogen Sensor

Instructions for updating TRACE 1600/1610 with the hydrogen sensor.

11 Upgrading Equipment

Upgrading a TRACE 1600 to a TRACE 1610

Instructions for upgrading a TRACE 1600 GC to a TRACE 1610 GC.

Upgrading a Stand Alone TRACE 1600/1610 to MS Version

Procedures for updating TRACE 1600/1610 stand alone to MS version with upgrade kit.

Updating HMI Software From USB Stick

Instructions for updating the TRACE 1610 HMI software using a USB stick.

12 Troubleshooting

Investigating Power Supply Issues

Guidance on verifying correct power supply and troubleshooting power-on issues.

Investigating Communication Issues

Steps to verify instrument communication with the computer and software.

Investigating Sensitivity Issues

Troubleshooting common causes of sensitivity issues like air leaks, contamination, or simple problems.

Error Messages

Information on error messages visualized during GC malfunctioning and how to reset alarms.

Contacting Technical Support

Information on how to contact Technical Support, including required details like model and serial number.

Glossary

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