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Thermo Scientific TSQ Series User Manual
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TSQ Series
Hardware Manual
70111-97163
Revision E
June 2014
2
Table of Contents
Default Chapter
13
Default Chapter
13
Table of Contents
13
Preface
17
Related Documentation
17
Safety and Special Notices
18
Safety Precautions
18
Solvent and Gas Purity Requirements
19
Service Philosophy
20
Level of Repair
20
Contacting Us
21
Chapter 1 Introduction
23
Ionization Modes
25
Ion Polarity Modes
25
Scan Modes
25
Q1MS and Q3MS Scan Modes
27
Product Scan Mode
27
Parent Scan Mode
28
Neutral Loss Scan Modes
29
Data Dependent Scan Mode
31
Scan Types
32
Full Scan
32
Selected Ion Monitoring
32
Selected Reaction Monitoring
33
Autosim
33
Data Types
33
Profile Data Type
34
Centroid Data Type
34
Mass/Charge Range
34
Chapter 2 Functional Description
35
Autosampler
36
Liquid Chromatograph
37
Syringe Pump
37
Divert/Inject Valve
38
Mass Spectrometer
40
Controls and Indicators
41
API Source
44
Ion Source Interface
44
Ion Optics
46
Mass Analyzer
50
Ion Detection System
57
Vacuum System and Inlet Gases Hardware
59
Electronic Assemblies
65
Data System
66
Computer Hardware
67
Data System / Mass Spectrometer / LC Communication, Contact Closure, and Line Power Connections
67
Data System / Local Area Network Interface
68
Printer
68
Chapter 3 System Shutdown, Startup, and Reset
71
Shutting down the System in an Emergency
71
Placing the System in Standby Condition
73
Shutting down the System Completely
74
Starting up the System after a Complete Shutdown
76
Starting up the LC
76
Starting up the Data System
76
Starting up the Mass Spectrometer
76
Starting up the Autosampler
77
Setting up Conditions for Operation
78
Resetting the Mass Spectrometer
79
Resetting the Data System
79
Resetting the Data System by Using the Windows Shutdown and Restart Procedure
80
Then on
80
Turning off Selected Mass Spectrometer Components
81
Chapter 4 Daily Operation
85
Things to Do before Operating the TSQ System
85
Checking the Argon and Nitrogen Supplies
86
Checking the ESI Fused-Silica Sample Tube for Elongation
86
Checking the System Vacuum Levels
86
Things to Do after Operating the TSQ System
88
Flushing the Sample Transfer Line, Sample Tube, and API Probe
88
Placing the System in Standby Condition
89
Cleaning the Ion Sweep Cone and Ion Transfer Tube
90
Emptying the Solvent Waste Bottle
90
Chapter 5 Removing and Reinstalling the Ion Source Housing
91
Removing the Ion Max or Ion Max-S Ion Source Housing
91
Installing the Ion Max or Ion Max-S Ion Source Housing
93
Ion Max and Ion Max-S Housing Maintenance
95
Chapter 6 Maintenance
97
Frequency of Cleaning
99
Maintaining the Ion Sweep Cone and Ion Transfer Tube
101
Removing and Cleaning the Ion Transfer Tube
101
Maintaining the Ion Source Interface Assembly
106
Shutting down and Venting the System
106
Removing the Ion Max or Ion Max-S Ion Source Housing
106
Removing the Ion Source Interface
107
Removing the S-Lens and Exit Lens (TSQ Vantage)
108
Cleaning the S-Lens and Exit Lens (TSQ Vantage)
109
Removing the Tube Lens and Skimmer (TSQ Quantum Access, TSQ Quantum Access MAX, or TSQ Quantum Ultra)
109
Cleaning the Tube Lens and Skimmer (TSQ Quantum Access, TSQ Quantum Access MAX, or TSQ Quantum Ultra)
110
Reinstalling the S-Lens and Exit Lens (TSQ Vantage)
111
Reinstalling the Tube Lens and Skimmer (TSQ Quantum Access, TSQ Quantum Access MAX, or TSQ Quantum Ultra)
111
Reinstalling the Ion Source Interface Assembly
112
Reinstalling the Ion Max or Ion Max-S Ion Source Housing
112
Starting up the System
112
Cleaning the Q00 Ion Optics
113
Shutting down and Venting the System
113
Removing the Ion Max or Ion Max-S Ion Source Housing
113
Removing the Ion Source Interface Assembly
113
Removing the Ion Optics Cage Assembly
114
Disassembling the Ion Optics Cage Assembly
118
Cleaning Q00 and L0
119
Reassembling the Ion Optics Cage Assembly
120
Reinstalling the Ion Optics Cage Assembly
121
Reinstalling the Ion Source Interface Assembly
122
Reinstalling the Ion Max or Ion Max-S Ion Source Housing
122
Starting up the System
122
Maintaining the Forepump
123
Cleaning the Fan Filters
123
Chapter 7 Diagnostics and PCB and Assembly Replacement
125
Running the TSQ System Diagnostics
126
Replacing a Fuse
127
Replacing Pcbs and Power Supplies
127
Chapter 8 Replaceable Parts
129
MS Accessory Kit
129
TSQ Vantage Instrument Specific Accessory Kit
130
TSQ Quantum Ultra, Ultra AM, and Ultra EMR Instrument Specific
130
Accessory Kit
130
HESI-II Probe Kit
131
TSQ Quantum Access Instrument Specific Accessory Kit
131
TSQ Accurate Mass Calibration Compounds Kit
131
Fittings, Ferrules, and Sample Loops
131
Index
133
4
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Thermo Scientific TSQ Series Specifications
General
Brand
Thermo Scientific
Model
TSQ Series
Category
Laboratory Equipment
Language
English
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