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5977 MSD
Agilent Technologies 5977 MSD Operation Manual
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2
Installing GC Columns
32
5977B Series MSD Operation Manual
W
ARNING
Always wear safety glasses when handling capillary columns. Use care to avoid
puncturing your skin with the end of the column.
31
33
Table of Contents
About this Manual
3
Hardware User Information
4
5977B Msd
4
5975/5977 Series MSD Prior to the 5977B MSD
4
Table of Contents
5
Introduction
10
5977B Series MSD Version
10
Abbreviations Used
11
The 5977B Series MSD
13
MSD Hardware Description
15
Important Safety Warnings
16
Hydrogen Safety
18
GC Precautions
18
Precautions
20
Safety and Regulatory Certifications (5977B)
23
Cleaning/Recycling the Product
26
Liquid Spillage
26
Moving or Storing the MSD
26
To Replace the Primary Fuses
27
Installing GC Columns
29
Columns
30
To Install a Capillary Column in a Split/Splitless Inlet
33
To Condition a Capillary Column
36
To Install a Capillary Column in the GC/MS Interface Using the Self-Tightening Column Nut
37
GCMS Transfer Line Tip Seals
41
To Install a Capillary Column in the GC/MS Interface Using a Standard Column Nut
42
Operating in Electron Ionization (EI) Mode
46
Operating the MSD from the Data System
46
Operating the MSD from the GC Control Panel
47
Configuring the MSD through the Web User Interface (WUI)
51
To Change the Network Settings of the MSD
51
Operating the 5975/5977 MSD from the Local Control Panel (LCP)
54
Modes of Operation
54
To View System Status During Startup
57
Emodule Mini Display Readout
61
Front Panel Instrument Status LED
61
The GC/MSD Interface
62
Before You Turn on the MSD
64
Pumping down
65
Controlling Temperatures
65
Controlling Column Flow
65
Venting the MSD
66
Set MS Analyzer Temperatures
67
Enable the GC/MS Interface and Oven
69
View MSD Temperatures and Vacuum
70
To Calibrate Column Flow Linear Velocity
72
To Run an Autotune
74
To Open the MSD Covers
76
Vent the MSD
77
To Pump down the MS
79
To Move or Store the MSD
82
General Maintenance
85
Before Starting
86
Maintaining the Vacuum System
91
Maintaining the Analyzer
92
To Open the Analyzer Chamber
94
To Remove the EI Ion Source
96
To Disassemble the Standard or Inert EI Ion Source
99
To Disassemble the Extractor EI Ion Source
102
To Clean the EI Ion Source
105
To Assemble a Standard or Inert EI Ion Source
110
To Assemble the Extractor EI Ion Source
113
To Replace a Filament in an EI Ion Source
116
To Install the EI Ion Source
118
To Attach Wiring from the Ion Source to the Feedthrough Board
119
To Replace the Electron Multiplier Horn
122
To Close the Analyzer Chamber
125
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Operating Manual
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Agilent Technologies 5977 MSD Specifications
General
Brand
Agilent Technologies
Model
5977 MSD
Category
Measuring Instruments
Language
English
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