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55B AA
Agilent Technologies 55B AA User Manual
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Agilent 55B AA Spectromet
er
User’s Guide
2
Table of Contents
Table of Contents
3
Contents
3
Safety Practices and Hazards
11
Verify Safe State
12
Electrical Hazards
12
Heat, Vapors and Fumes
13
Compressed Gases and Cylinders
14
Gas Hoses and Connections
17
Ultraviolet Radiation
18
Other
18
Warning Symbols
18
CE Compliance
20
Electromagnetic Compatibility
21
En55011/Cispr11
21
Ices/Nmb-001
22
Flame Operation
22
Flammable Solvents
22
Burners
24
Nebulizer
25
Liquid Trap
26
Heat Hazards
27
Perchloric Acid
27
Flashbacks
29
What to Do in the Event of a Flashback
31
Introduction
33
Site Preparation Requirements
33
Documentation
34
Conventions
34
Specifications
34
Environmental Specifications
34
Overview
37
Installation Checklist
37
Instrument Overview
37
Power
39
Gas Hoses
39
Printer
39
Accessories
39
Moving Your Instrument
40
Lamp Compartment
40
Hollow Cathode Lamps
40
Deuterium (D ) Lamp
41
Sample Compartment
41
Nebulizer Block Assembly
42
Burner
46
Sample Compartment Front Panel
46
Flame Shield
47
Chimney
48
Interface
49
Front Panel Overview
49
Display Screen
50
Keypad
53
Navigating the Interface
56
Changing Pages
56
Selecting Menus
56
Moving between Fields
58
Display Pages
58
Load Method Page
58
Instrument Parameters Page
58
Measurement Parameters Page
60
Options Page
61
Optimization Page
63
Calibration Parameters Page
64
Results Page
64
Operation
67
Pre-Analysis Checklist
67
Start the System
69
Method Development
69
Select the Language of the Interface
69
Load a Method
70
Save/Delete Methods
71
Set the Instrument Parameters
72
Set the Measurement Parameters
72
Define the Calibration Standards
73
Optimization
74
Align Lamps
74
Align the Burner
76
Light the Flame
78
Optimize the Flame Signal
80
Nebulizer Setup
81
High Vacuum Setting
82
Low Vacuum Setting
83
Set Zero Uptake Rate - Organic Solvents
83
Set the Uptake Rate for Organic Solvents
84
Flame Types
84
Performance Checks
85
Calibrate the Method
86
Measure Standards Manually
86
Measure Standards Using SIPS 10
86
Display the Calibration Graph
87
Reslope the Calibration
87
Sample Measurement
88
Measure Samples Manually
88
Measure Samples with SIPS
88
Results
89
Print the Results
89
Output to LIMS System
90
Shut down the System
90
Maintenance
91
Maintenance Schedule - General
91
Maintenance Schedule - Nebulizer/Spray Chamber
92
Cleaning
93
General
93
Windows
93
Filters
93
Nebulizer
93
Remove the Nebulizer Block
94
Disassemble the Nebulizer
95
Clean a Blocked Nebulizer
96
Reassemble the Nebulizer Block
97
Impact Bead
101
Spray Chamber
108
Disassemble the Spray Chamber
108
To Clean the Spray Chamber
109
To Assemble the Spray Chamber
109
Assemble the Spray Chamber and Nebulizer Block
111
Attach the Drain Tube/Float/Liquid Trap to the Nebulizer Block
111
Installing the Spray Chamber/Nebulizer Assembly
113
Burners
116
To Install a Burner
116
Clean the Burner
118
Gas Supplies
122
Lamps
122
To Install a Hollow Cathode Lamp
122
Removing Hollow Cathode Lamps
123
D 2 Lamp
124
Fuses
126
Spare Parts
129
Sample Lists
129
Other
132
Covers/Doors
132
Fuses
132
Miscellaneous
133
Troubleshooting/Errors
135
Common Problems
137
Error Messages
140
0804 LIMS Port Error
140
2851 SIPS Comms Error
140
3800 EEPROM Storage Error
140
5004 Signals Not Increasing
141
5005 Slope Test Failure
141
5006 Calibration Fit Failure
141
5008 Reslope Signal out of Range
141
6000 Check HC Lamp Selection
141
9159 EEPROM Checksum Zero Wl
141
9160 EEPROM Checksum Mono Correction
142
9307 Rbc/Mains Frequency below 48Hz
142
9308 Rbc/Mains Frequency
142
9309 Rbc/Mains Frequency above 62Hz
142
9310 Optical RBC Frequency
143
9311 Instrument Fault +12V PSU
143
9312 Instrument Fault -12V PSU
143
9313 Instrument Fault 5V PSU
143
9316 Wavelength out of Range
143
9317 No Peak: Low HC Lamp Energy
143
9318 No Peak: High HC Lamp Energy
144
9319 No Peak: Low BC Lamp Energy
144
9320 No Peak: High BC Lamp Energy
144
9321 No Peak: Low HC Lamp Energy
145
9322 No Peak: High HC Lamp Energy
145
9323 Low Emission: no Peak
145
9324 High Emission: no Peak
146
9329 No Peak Detected
146
9330 No Peak Detected
146
9337 Instrument Fault 310V PSU
147
9339 Mono Resetting. Please Wait
147
9415 Instrument Fault: Lamp Code
147
9422 Instrument Fault: Lamp Current
147
9514 Instrument Signal Saturation
148
9517 Low HC Lamp Energy
148
9518 High HC Lamp Energy
148
9524 Low BC Lamp Energy
148
9525 High BC Lamp Energy
149
9527 Instrument Fault: EHT Failed
149
9528 Background Lamp Failed
149
9529 Background Lamp Interlock
149
9530 Instrument Fault: Signal Diagnostics
149
9531 No Lamp Current Detected
150
9602 Instrument Fault: Mono Datum
150
9911 No Burner Fitted
150
9912 N2O Burner Not Fitted
150
9914 No Gas Control Unit
150
9915 Flame Shield Open
150
9916 Fault: Gas Pressure Sensor
151
9917 No Oxidant Gas Pressure
151
9920 Fault: Flame Detected
151
9921 Flame out Detected
151
9922 Flame Shutdown: Gas Type
151
9923 Flame Ignition Timeout
152
9934 Flame Shutdown: Host Offline
152
9937 Flame Pressure Relief Bung
152
9938 Liquid Trap Not Ready
152
9Xxx GPIB Fault
152
9Xxx Instrument Error
152
9Xxx Spectraa Error
152
4
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Agilent Technologies 55B AA Specifications
General
Brand
Agilent Technologies
Model
55B AA
Category
Measuring Instruments
Language
English
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