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Endress+Hauser Analytik Jena TOPwave User Manual

Endress+Hauser Analytik Jena TOPwave
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Operating Manual
TOPwave
Microwave System for Pressure Digestion

Table of Contents

Questions and Answers:

Endress+Hauser Analytik Jena TOPwave Specifications

General IconGeneral
BrandEndress+Hauser
ModelAnalytik Jena TOPwave
CategoryLaboratory Equipment
LanguageEnglish

Summary

Basic Information

User Manual Notes

Explains the purpose, conventions, and signal word meanings of the user manual.

Intended Use

Details the specific applications and limitations of the TOPwave microwave digestion system.

Warranty and Liability

Outlines the terms and conditions of the product warranty and manufacturer liability.

Safety Instructions

General Safety Notes and Unit Markings

Covers general safety guidelines, warning symbols, and labels on the unit.

Qualified Users

Specifies the required qualifications and training for operating personnel.

Transport and Commissioning Safety

Provides safety precautions for moving and setting up the equipment.

General Safety Information

Highlights crucial safety precautions for microwave digestion procedures and handling vessels.

Safety Equipment and Emergency Procedures

Details essential safety equipment and actions in case of emergencies.

Installation and Setup

Ambient Conditions

Specifies the environmental requirements for system installation and operation.

Device Description

Basic Unit Overview

Describes the main components and features of the TOPwave microwave system.

Temperature Control System

Explains how the system monitors and regulates sample temperatures.

Pressure Monitoring System

Details the optional system for measuring and controlling internal vessel pressure.

Pressure Vessels and Rotor System

Describes the different types of pressure vessels and their rotor configurations.

Installation and Setup

Unpacking the System

Provides instructions for safely removing and inspecting the equipment from packaging.

Installing the TOPwave System

Guides the user through the physical setup and connection of the microwave.

Selecting Setup Parameters

Details how to configure system settings and parameters via the control unit.

Operating the TOPwave

Setup Methods and General Notes

Explains basic operating principles, sample heating, and pressure management.

Control Unit Operation

Describes how to interact with the touch-screen control interface and its functions.

Selecting and Modifying Applications

Guides users on choosing, customizing, and saving digestion programs.

Developing New Applications

Outlines a systematic procedure for creating and optimizing new digestion methods.

Performing a Digestion Procedure

Provides step-by-step instructions for running a digestion process.

Sample Loading Procedures

Details the correct methods for loading different types of pressure vessels.

Handling PM 40, PM 60, PL 100 Vessels

Specific instructions for loading and preparing PM 40, PM 60, and PL 100 pressure vessels.

Handling QX 20/QX 22 Vessels

Specific instructions for loading and preparing QX 20/QX 22 pressure vessels.

Handling CX 100 Vessels

Specific instructions for loading and preparing CX 100 pressure vessels.

Sample Removal and Cooling

Instructions for safely removing and cooling digested samples from the oven.

Digestion Reports and Data Display

How to access, view, and interpret recorded digestion data and reports.

Data Export via USB

Procedure for transferring saved digestion data to a USB storage device.

Evaporating Unit Operation

Instructions for using the optional evaporating unit for sample concentration.

Evaporating Unit Installation & Commissioning

Steps for setting up and preparing the optional evaporating unit.

Evaporating Unit Operating Procedures

Guidance on operating the evaporating unit after installation.

PC Control and Network Setup

Instructions for connecting and controlling the TOPwave via a PC.

PC Control Safety Information

Safety precautions related to using the PC control software.

PC Security Settings

Steps for configuring browser security settings for PC control.

PC Control via Web Visualization

How to access and use the system's web-based control interface.

Data Transfer Methods

Procedures for transferring data using FTP and web visualization.

Care and Maintenance

General Safety Information for Care

Safety precautions to observe during cleaning and maintenance operations.

Cleaning Procedures

Detailed instructions for cleaning different parts of the TOPwave system.

Oven Chamber Cleaning

Specific guidance on cleaning the microwave oven chamber.

Control Unit and Gas System Cleaning

How to clean the control unit and gas collection system.

Vessel Cleaning Methods

Procedures for cleaning digestion vessels after use.

Cap for Pressure Control Cleaning

Instructions for cleaning the pressure control cap components.

Maintenance Procedures

Aligning Pressure Measurement

Steps for calibrating the pressure measurement system using pure water.

Output Power Measurement

Procedure to check and verify the magnetron's output power.

Troubleshooting Common Issues

Provides solutions for common faults encountered with the microwave device and control unit.

Fuse Replacement Guide

Instructions on how to safely replace the unit's fuses.

Information on Disposal

Proper Disposal Guidelines

Information on how to dispose of the TOPwave and its components responsibly.

Specifications

Technical Data of the System

Lists detailed technical specifications for the microwave oven and control unit.

Pressure Vessel Specifications

Details specifications for different types of pressure vessels, including volume and limits.

Guidelines and Standards Compliance

Outlines the standards and directives the TOPwave complies with.

Appendix

Tips and Tricks for Operation

Provides helpful advice and techniques for optimizing TOPwave usage.

Small Sample Quantity Handling

Guidance on digesting very small sample amounts efficiently.

Multiple Samples per Vessel

Tips for increasing sample throughput by processing multiple samples in one vessel.

Higher Sample Throughput Techniques

Methods to maximize sample processing speed and efficiency.

Cooling Down Samples Safely

Recommended procedures for cooling digested samples after the process.

Rupture Discs and Locking Lids

Information on rupture discs, locking lids, and their maintenance.

Weighing Cup Usage

Instructions on using weighing cups for sample preparation.

Available Applications

Information on obtaining and using various pre-defined applications.

Vessel Positioning in Rotors

Illustrates the optimal placement of vessels within the turntable rotors.

Unit Conversation

Provides conversion factors for common units used in the manual.

Abbreviation Glossary

Defines common abbreviations and acronyms used in the documentation.

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