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Thermo Scientific thermoscientific VC-P20-A-01 User Manual

Thermo Scientific thermoscientific VC-P20-A-01
296 pages
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thermo
scientific
Vanquish
Pumps C, Pumps F
VC-Pxx, VF-Pxx
Operating Manual
4820.4405-EN Revision 4.0 December 2019

Table of Contents

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Thermo Scientific thermoscientific VC-P20-A-01 Specifications

General IconGeneral
Product TypeVacuum Controller
Model NumberVC-P20-A-01
BrandThermo Scientific
Voltage100-240 VAC
Frequency50/60 Hz
Power Consumption20 W
DisplayLCD
Operating Temperature5°C to 40°C
Storage Temperature-20°C to 60°C
Humidity Range20% to 80% RH (non-condensing)
Communication InterfaceRS-232

Summary

Using this Manual

About this Manual

Describes the manual's purpose, scope, and notes for users.

Conventions

Explains safety messages, special notices, and informational notes used in the manual.

Typographical Conventions

Details typographical conventions for data input, references, viewpoint, and important words.

Reference Documentation

Lists additional hardware and software documentation available for reference.

Safety

Safety Symbols and Signal Words

Explains safety symbols, signal words, and how to observe manual safety messages.

Safety Symbols on the Device

Lists safety symbols found on the device or labels and their meanings.

Intended Use

Defines the intended use of the device and recommends laboratory best practices.

Safety Precautions

Outlines general safety information and precautions for installation, operation, and transport.

Electrical Safety Precautions

Details electrical safety measures to prevent shock or damage to the device.

General Residual Hazards

Warns about hazardous substances and biohazards, and provides handling precautions.

In Case of Emergency

Provides instructions for emergency situations, emphasizing power disconnection.

Solvent and Additive Information

Provides recommendations for compatible solvents and additives to ensure optimal system functionality.

Allowed pH Ranges

Specifies allowed pH ranges for different system configurations and notes impact on detectors.

Allowed Concentrations

Lists allowed concentrations for chloride and buffer in different system configurations.

Compliance Information

Details compliance with EMC and safety standards and notes that changes may void compliance.

Device Overview

Pump Features

Describes the main and special features of the Vanquish pump, including its piston design and degasser.

Operating Principle

Explains the general and pump-specific operating principles, including dual-piston and degasser functions.

Interior Components

Explains how to access interior components by opening the front doors for maintenance.

Piston Seal Wash System

Details the active piston seal wash system for prolonging piston and seal lifetime by keeping them wet.

Purge/Sensor Unit

Describes the purge/sensor unit, comprising the purge valve and system pressure sensor.

Mixing System

Explains the mixing system components (capillary and static mixers) and their role in baseline smoothing.

Leak Detection

Details the leak sensor's function in monitoring leaks, alerting the user, and stopping the pump if unresolved.

Operation

Describes device operation via computer (Chromeleon) and the availability of an internal keypad for basic functions.

Unpacking

Unpacking

Provides instructions for unpacking the device, inspecting for damage, and handling heavy loads safely.

Scope of Delivery

Lists the items included in the pump's delivery package.

Installation

Safety Guidelines for Installation

Presents safety guidelines for installation, including handling heavy devices and electrical precautions.

Installing the Device

Outlines the steps for installing the device hardware, flow connections, and software setup, including qualification.

Site Requirements

Specifies environmental requirements for the installation site to ensure optimal device performance.

Accessing the Interior Components

Explains how to access interior components by opening the front doors for maintenance.

Setting Up the Hardware

Describes how to set up the hardware, including system arrangement and device connectors/cables.

Connecting the Device

Details the electrical connectors and device connection ports available on the pump.

Connecting the Power Cord

Provides instructions for connecting the power cord, emphasizing correct country-specific cords and condensation prevention.

Setting Up the Flow Connections

Guides on setting up flow connections, including general rules, handling components, and flushing.

Guiding Capillaries and Tubing Through the System

Explains how to route capillaries and tubing through the system using tubing chases and guides.

Connecting Fittings, Capillaries, and Tubing

Provides general guidelines and specific instructions for connecting Viper and non-Viper capillaries and tubing.

Guiding Liquids to Waste

Describes how liquids collected in the leak tray are guided to the drain port and waste system.

Connecting the Solvent Lines

Details how to install solvent lines between pump inlet ports and solvent reservoirs.

Installing Solvent Shut Off Valves

Provides steps for installing solvent shut-off valves in solvent lines for flow control.

Seal Wash System

Outlines the components of the seal wash system and steps for setup, interconnection, and flushing.

Setting Up the Seal Wash System

Lists parts and tools required and provides instructions for setting up the seal wash system.

Flushing the Seal Wash System

Describes alternatives for flushing the seal wash system, including using software or manual methods.

Connecting the Pump and Autosampler

Guides on connecting the pump and autosampler using capillaries and routing them through guide holes.

Turning On the Device

Details the procedure for turning on the device, including power button and main power switch usage.

Setting Up the Device in the Software

Instructs on setting up the device within the chromatography software, referring to manuals and help files.

Operation

Introduction to this Chapter

Introduces the chapter on device control, routine operation, and shutdown, assuming prior setup completion.

Safety Guidelines for Operation

Highlights safety guidelines for operating the device, including LED luminosity and system operation precautions.

Control Elements

Describes the control elements, including the keypad and status indicators for device operation.

Status Indicators

Explains the status LED bar, STATUS LED, and pump block LED for monitoring device operational status.

Power On/Off Control

Details the main power switch and system power button for controlling device power, including startup sequences.

Use of Solvents and Additives

Provides guidelines for using solvents and additives to prevent system contamination and ensure optimal performance.

Preparing the Device for Operation

Covers additional steps required to prepare the device for operation and sample analysis, including first-time use.

Important Operating Parameters

Discusses key operating parameters like flow, flow ramps, and pressure limits for routine device operation.

Purging the Pump

Explains the purpose and settings for purging the pump, including automatic and manual procedures.

Optimizing the Performance of the Device

Offers information and hints to optimize device performance, including component monitoring and solvent handling.

Shutting Down the Device

Provides instructions for shutting down the device for short-term or long-term interruptions.

Maintenance and Service

Introduction to Maintenance and Service

Introduces routine maintenance and service procedures that users can perform, noting service personnel requirements.

Safety Guidelines for Maintenance and Service

Outlines safety guidelines for performing maintenance and service, covering high voltage, hazardous substances, and solvent spraying.

General Rules for Maintenance and Service

Lists general rules and recommendations for successful maintenance and service procedures.

Routine and Preventive Maintenance

Describes routine and preventive maintenance for optimal device performance and uptime.

Flushing the Pump

Explains procedures for flushing the pump to avoid contamination or address persistent contamination issues.

Flushing with Persistent Contamination Only

Details a harsher cleaning procedure for persistent contamination, including specific reagents and steps.

Cleaning or Decontaminating the Device

Describes cleaning and decontamination procedures, including safety precautions for alcoholic detergents.

Predictive Performance

Explains the Predictive Performance function in Chromeleon software for scheduling maintenance based on usage.

Seal Wash System

Outlines maintenance steps for the seal wash system, including leakage testing and component replacement.

Testing the Seal Wash System for Leakage

Provides steps to test the seal wash system for leakage, especially after maintenance.

Replacing the Seal Wash Lines

Guides on replacing seal wash lines due to damage, blockage, or regular maintenance.

Replacing the Seal Wash Detector

Details the procedure for replacing the seal wash detector due to contamination or impaired functionality.

Pump Head

Lists maintenance procedures related to the pump head, including replacement of seals and pistons.

Replacing the Pump Head

Guides on replacing the pump head due to damage or performance issues, including preparations and steps.

Replacing the Pistons

Details the process for replacing pistons when damaged, including cleaning and seal replacement.

Cleaning the Piston

Explains how to clean pistons, including inspection for damage and proper reinstallation.

Replacing the Piston Seals or Support Ring

Guides on replacing piston seals or support rings due to leaks or unstable flow rates.

Recommendations for New Piston Seals

Provides recommendations for running in new piston seals to ensure performance and longevity.

Replacing the Seal Wash Seals

Details the procedure for replacing seal wash seals due to damage, leakage, or regular maintenance.

Replacing the Pump Head Seals

Guides on replacing pump head seals due to damage or leakage.

Testing the Piston Seals for Leakage

Explains how to test piston seals for leakage, especially when pressure issues are observed.

Check Valves

Outlines maintenance procedures for check valves, including replacement of inlet and outlet valves.

Replacing the Outlet Check Valves

Guides on replacing outlet check valves due to damage or leakage.

Cleaning the Check Valves

Details the process for cleaning check valves using isopropanol and an ultrasonic bath.

Mixing System

Describes the mixing system, including testing static mixer permeability and replacement.

Replacing the Static Mixer or Capillary Mixer

Guides on replacing static or capillary mixers due to permeability issues or damage.

Solvent Lines and Solvent Line Filters

Covers maintenance for solvent lines and filters, including emptying, replacing, and cleaning.

Replacing Solvent Lines

Details the procedure for replacing solvent lines based on pump type and flow path.

Replacing the Solvent Line Filter

Guides on replacing solvent line filters due to damage or impaired permeability.

Replacing the Purge Valve Knob

Details the process for replacing the purge valve knob when leakage is observed.

Testing the Pump for Leakage (General Test)

Provides a general test procedure to check the pump for leakage after maintenance.

Replacing the Main Power Fuses

Guides on replacing main power fuses, emphasizing safety precautions and correct fuse types.

Updating the Device Firmware

Explains how to update the device firmware using the Instrument Configuration Manager and Chromeleon software.

Replacing the Doors

Details how to remove and install the device doors, emphasizing careful handling to avoid hinge damage.

Transporting or Shipping the Device

Prepares the device for transport or shipping, including safety guidelines.

Replacing the Slide-In Module

Guides on removing and installing slide-in modules, stressing safe handling of heavy components.

Troubleshooting

General Information about Troubleshooting

Provides general information on troubleshooting, including status indicators, alarms, and audit trail messages.

Messages

Lists common messages appearing in the Chromeleon Audit Trail and their description and remedial actions.

Testing the Pump for Leakage

Details tests to help identify leakage sources in the pump, such as general pump leak tests and seal leak tests.

Resolving Liquid Leaks

Provides steps to resolve liquid leaks by locating the source and taking appropriate remedial action.

Pressure Issues or Shifts in Retention Time

Addresses pressure issues and retention time shifts, guiding users to identify and eliminate problem sources.

Removing Persistent Air Bubbles

Offers solutions for persistent air bubbles, suggesting purging against backpressure and referring to piston seal procedures.

Pump-Specific Information

Introduction to this Chapter

Introduces the chapter on pump-specific information, covering interior components and operating principles.

Quaternary Pump and Dual Pump

Provides specific information on quaternary and dual pumps, including components, operating principles, and dwell volume.

Binary Pump

Details specific information for the binary pump, including its interior components, operating principle, and solvent composition settings.

Isocratic Pump

Covers specific information for the isocratic pump, including its interior components and operating principle.

Modifying the Pump for Specific Applications

Gradient Delay Volume, Dwell Volume and Ripple

Explains gradient delay volume, dwell volume, and ripple in HPLC systems and how pump mixing systems affect them.

Available Mixing Systems

Lists available mixing systems, their volumes, and remarks on compatibility and requirements.

Exchanging the Mixing System

Guides on removing and installing different mixing systems to adapt dwell volume or ripple.

Normal-Phase Compatible Solvents and Additives

Discusses considerations for using normal-phase compatible solvents and additives, including pump and autosampler modification.

Specifications

Performance Specifications

Details performance specifications for quaternary, dual, binary, and isocratic pumps.

Physical Specifications

Lists physical specifications of the device, including operating conditions, power, dimensions, and weight.

Accessories, Consumables and Replacement Parts

General Information

Provides general information on operating the device with authorized parts and compatibility of updated components.

Ship Kit

Lists the items included in the Binary Pump VC-P10 ship kit and reordering information.

Dual Pump

Lists items included in the VC-P32/VC-P33 and VF-P32 ship kits for dual pumps.

Isocratic Pump

Lists items included in the VC-P40 ship kit for the isocratic pump.

Quaternary Pump

Lists items included in the VC-P20/VC-P21 and VF-P20 ship kits for quaternary pumps.

Optional Accessories

Lists optional accessories, including miscellaneous items, mixing systems, and inline filters.

Consumables and Replacement Parts

Details available consumables and replacement parts, including maintenance kits for VC and VF pumps.

Appendix

Compliance Information

Provides declarations of conformity, cTUVus compliance, and RoHS compliance information for the device.

WEEE Compliance

States compliance with the European Union's Waste Electrical & Electronic Equipment (WEEE) Directive.

FCC Compliance

Confirms compliance with U.S. FCC Rules for Class A digital devices.

Manual Release History

Lists the manual revisions and the corresponding product model coverage.

Digital I/O

Explains the functionality of digital I/O ports for exchanging signals with external devices and pin assignments.

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