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General| Brand | Bruker |
|---|---|
| Model | NMR |
| Category | Thermometer |
| Language | English |
Introduction to the software implementation for configuring solvent and lock parameters.
Guidance on system setup, including lock, shimming, and parameter optimization for the thermometer.
Demonstrates practical usage scenarios, starting with a methanol sample for calibration.
Details the steps and interface for observing temperature and system parameters in real-time.
Explains how to enable and use the temperature regulation feature for experiments.
Procedure for adding custom NMR thermometer substances and their parameters to the edlock table.
Guidance on choosing suitable compounds for temperature measurement based on properties and applications.
Lists pre-calibrated solvents and their specific compositions for NMR Thermometer usage.
Discusses important factors like signal-to-noise ratio and intensity ratio for reliable measurements.
Instructions on adapting the shimming routine for new solvents or specific experimental setups.
Demonstrates using the NMR Thermometer as an internal reference for accurate temperature correction across spectrometers.
Explains the ability to compensate for sample heating from RF or spinning speed during experiments.
Details how the NMR Thermometer compensates for heating caused by RF pulses in sequences like TOCSY.
Covers compensation for frictional heating in HR-MAS experiments due to varying spinning speeds.
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