Bruker NMR - Table of Contents

Contents
Z33085_2_002 3
Contents
1 Introduction......................................................................................................................................... 5
2 Principle of NMR Thermometer......................................................................................................... 7
3 Requirements...................................................................................................................................... 9
4 Getting Started.................................................................................................................................. 11
4.1 The edlock Menu............................................................................................................... 11
4.2 Setting up the NMR System for the NMR Thermometer ................................................... 13
4.3 Examples........................................................................................................................... 15
4.3.1 Monitoring Mode................................................................................................................ 16
4.3.2 Regulation Mode ............................................................................................................... 17
5 Advanced Operation ........................................................................................................................ 19
5.1 Define a New Solvent........................................................................................................ 19
5.2 Selection of NMR Thermometer Compounds ................................................................... 21
5.2.1 Predefined Solvents for the NMR Thermometer ............................................................... 22
5.2.2 Technical Considerations .................................................................................................. 23
5.2.3 Considerations for Shimming with Topshim ...................................................................... 24
6 Applications ...................................................................................................................................... 27
6.1 Identical Chemical Shifts at Different Spectrometers ........................................................ 27
6.2 Identical Chemical Shifts for Experiments with Different Heating due to Experimental
Conditions (Temperature Compensation) ......................................................................... 28
6.2.1 RF Heating ........................................................................................................................ 28
6.2.2 Heating caused by Spinning Speed (HR-MAS)................................................................. 29
7 Frequently Asked Questions (FAQ)................................................................................................ 31
8 Contact .............................................................................................................................................. 33
List of Figures................................................................................................................................... 35
Index .................................................................................................................................................. 37