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Hach Micro Dist User Manual
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50
Sulfide–1
13.4
Comp
arison of this method an
d SW–846 Method 903
0B, Revision 2
Both methods use
a trapping solution
which is 0.043 M in
zinc
acetate an
d which contains 1.60%
formaldehyde. The stock 37
%
formaldehyde solution co
ntains 10–15% meth
anol.
2.0 mL of this solution is in
each Sulfide–1 collector tube.
47
49
Table of Contents
Table of Contents
3
Section 1 Specifications
5
Section 2 General Information
7
Safety Information
7
Use of Hazard Information
7
Precautionary Labels
8
Principle of Operation
8
Distilling Calibration Standards with the Micro Dist System
9
Section 3 Installation
11
Unpacking the Instrument
11
Micro Dist Setup
11
Connecting the Power Supply
11
Section 4 Operation
13
Setting the Temperature
13
Heater Block
13
Using Micro Dist™ Tubes
14
Filling and Assembling the User-Fill Collector Tubes
15
Filling and Assembling the Collector Tube
15
Section 5 Startup
19
Section 6 Maintenance
21
Cleaning the Micro Dist
21
Calibrating the Automatic Re-Pipettor
22
Fuse Replacement
22
Parts
22
Section 7 General Procedure
23
General Procedure
23
Micro Dist™ Method (Method Number 10-204-00-1-X)
29
Releasing Agent
30
Sources
31
USEPA Method 335.2 Scaled-Down
31
Calculations Showing Equivalency of Concentrations of Releasing Solutions
32
Micro Dist Method Cyanide-1
32
USEPA Method 335.2
32
USEPA Method 335.4
32
Calculations Showing Equivalency of Concentrations of Trapping Solution
33
Micro Dist Method Cyanide-1
33
USEPA Method 335.2
33
Micro Dist™ Method
35
Section 10 Cyanide-3 (WAD)
37
Micro Dist™ Method
37
Releasing Agent
39
Sources
39
Micro Dist™ Method
41
Section 12 Phenolics-1
43
Micro Dist™ Method
43
Sources
44
Section 13 Sulfide-1
45
Micro Dist™ Method
45
Releasing Agent
47
Sources
47
Comparison of this Method and SW-846 Method 9030B, Revision 2
48
Section 14 Sulfide-2
49
Micro Dist™ Method
49
Sources
51
Releasing Agent
51
Section 15 Ammonia-1: Phenate Method/Ise
53
Micro Dist™ Method
53
Borate Buffer
55
Sources
55
Section 16 Ammonia-2: Nesslerization Method
57
Micro Dist™ Method
57
Borate Buffer
58
Section 17 Tritium-1
59
Micro Dist™ Method
59
Sources
60
Section 18 Replacement Parts and Accessories
61
Section 19 Contact Information
63
Section 20 Limited Warranty
64
Appendix A Micro Dist Methods
65
Methods List
65
Appendix B Troubleshooting
67
Common Problems, Likely Causes, and Possible Solutions
67
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Hach Micro Dist Specifications
General
Brand
Hach
Model
Micro Dist
Category
Measuring Instruments
Language
English
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