TA Instruments Q10 User Manual

DSC Q Series Getting Started Guide
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Using the DSC
All of your DSC experiments will have the following general outline. In some cases, not all of these steps will
be performed. The majority of these steps are performed using the instrument control software. The instructions
needed to perform these actions can be found in the online help in the instrument control program; therefore,
they will not all be covered in detail here.
• Calibrating the instrument
• Selecting the pan type and material
• Preparing the sample
• Creating or choosing the test procedure and entering sample and instrument information through the TA
instrument control software
• Setting the purge gas flow rate
• Loading the sample and closing the cell lid
• Starting the experiment.
To obtain accurate results, follow procedures carefully.
Before You Begin
Before you set up an experiment, ensure that the DSC and the controller have been installed properly. Make
sure you have:
• Made all necessary cable connections from the DSC to the computer
• Connected all gas lines
• Powered up the unit
• Connected any desired accessories
• Connected the instrument with the controller
•Become familiar with controller operations
•Calibrated the DSC, if necessary.
Chapter 3
Use, Maintenance, & Diagnostics

TA Instruments Q10 Specifications

General

Brand	TA Instruments
Model	Q10
Category	Measuring Instruments
Language	English

Summary

Notices

Regulatory Compliance

Safety Standards

Lists safety requirements for electrical equipment from various regulatory bodies.

Electromagnetic Compatibility Standards

Details EMC standards for industrial, scientific, and medical equipment.

Safety

Instrument Symbols and Electrical Safety

Explanation of warning symbols and electrical safety precautions.

Handling Liquid Nitrogen

Safe handling procedures and precautions for using liquid nitrogen.

Thermal Safety and Instrument Handling

Precautions for thermal hazards and lifting the heavy DSC instrument.

Introducing the DSC

Overview and System Components

General introduction to DSC and its main components, including the cell.

Cooling Accessories

Description of FACS, RCS, Quench Cooler, and LNCS for temperature control.

DSC Touch Screen and Keypad Interfaces

Operation of Q2000/Q200 touch screen, Q1000/Q100 touch screen, and Q20/Q10 keypad.

Options, Accessories, and Specifications

Overview of accessories, specialized cells, and instrument specifications.

Installing the DSC

Initial Setup and Connections

Covers unpacking, inspecting, choosing location, and connecting cables/lines.

Gas Lines and Cooling Setup

Procedure for connecting purge and cooling gas lines to the DSC.

Power Configuration and Startup

Covers voltage configuration, power, starting, and shutting down the DSC.

Installing Cooling Accessories

Step-by-step guide to installing FACS, Quench Coolers, and additional items.

Using, Maintaining, and Diagnosing the DSC

DSC Experiment Workflow

Steps for preparing, running, and stopping DSC experiments.

DSC Calibration Procedures

Detailed procedures for various DSC calibrations including Tzero, heat capacity, and pressure.

Autosampler Calibration

Instructions for calibrating the DSC Autosampler for accurate sample handling.

Instrument Maintenance and Parts

Procedures for cleaning, troubleshooting, and replacing fuses and parts.