EasyManua.ls Logo

Thermo Scientific iCAP 7000 Series User Manual

Thermo Scientific iCAP 7000 Series
72 pages
To Next Page IconTo Next Page
To Next Page IconTo Next Page
Page #1 background imageLoading...
Page #1 background image
iCAP 7000 Series ICP-OES Spectrometer
Customer Familiarisation and Maintenance Manual
© March 2013 Thermo Fisher Scientific Inc.
www.thermoscientific.com
http://www.thermofisher.com

Table of Contents

Other manuals for Thermo Scientific iCAP 7000 Series

Question and Answer IconNeed help?

Do you have a question about the Thermo Scientific iCAP 7000 Series and is the answer not in the manual?

Thermo Scientific iCAP 7000 Series Specifications

General IconGeneral
BrandThermo Scientific
ModeliCAP 7000 Series
CategoryLaboratory Equipment
LanguageEnglish

Summary

Instrument Overview

General Instrument Description

Overview of the iCAP 7000 Series ICP-OES spectrometer and its basic components.

Optical System and Light Path

Description of the spectrometer's optical design and light path.

Further Information Sources

Qtegra Software Help and Guides

Accessing software help and user guides within the Qtegra system.

Quick Start Guide

Basic information to start operating the iCAP 7000 Series ICP-OES.

User Manual Details

Instrument operation, maintenance, and safety hazard information.

Online Assistance and Resources

Information sources on Thermo Scientific and iCAP 7000 Series ICP-OES.

Instrument Hardware Components

LED Indicators and Status

Description of LED indicators and their meaning for instrument status.

Preparing the System for Use

Steps to prepare the instrument for operation, including purging and warm-up.

Instrument Shut-down Procedure

Procedure for safely shutting down the instrument after analysis.

Sample Introduction Assembly

Torch and Center Tube Assembly

Assembling Duo/Radial torches, center tubes, and holders.

Nebulizer and Spray Chamber Setup

Positioning nebulizer, drain, and connecting spray chamber adaptor.

Pump Tubing and Sprint Valve Connection

Connecting pump tubing and installing the iCAP Sprint Valve system.

Radial View Window and Other Components

Radial view window on Duo instruments and other assembly details.

iCAP Sprint Valve Installation

Connecting the Tubing

Steps for connecting tubing for the iCAP Sprint Valve system.

Autosampler Operation

Introduction to Autosampler

Introduction to autosampler configuration and sample types.

Autosampler Installation Requirements

Requirements for autosampler installation by certified engineers.

Autosampler Setup Procedure

Connecting autosampler capillary tubing to the iCAP 7000 sample pump.

Instrument Optimization and Analysis Setup

Key Optimization Parameters

Adjusting parameters like gas flow, RF power, and viewing height for optimal results.

Standard Operating Procedures

Guidance on setting up basic analysis and preparing the system.

Plasma Ignition and Interlocks

Steps for striking the plasma and checking instrument interlocks.

Setting Up Analyses

Configuring LabBooks, standards, quality control, and sample lists in Qtegra.

Running, Adjusting, and Monitoring Analysis

Running analysis, auto peak adjust, pump tension, and monitoring.

Torch Alignment and Reporting

Performing torch alignment, setting pump tension, and generating reports.

Data Export and System Shutdown

Exporting LabBooks and safely shutting down the instrument.

Instrument Maintenance

Instrument Cleaning Procedures

Cleaning external covers, sample introduction system, and torch.

Spray Chamber and Nebulizer Cleaning

Cleaning spray chambers and nebulizers with appropriate solutions.

Purged Optical Path Window Cleaning

Instructions for cleaning the Purged Optical Path (POP) window.

Preventive Maintenance Schedule

Checks for chiller, filters, and Sprint Valve system components.

Sprint Valve Maintenance

Inspection, leak checking, and cleaning of the 6-Port valve and tubing.

Analytical Problem Troubleshooting

Poor Precision Troubleshooting

Diagnosing and resolving poor precision issues in the sample introduction system.

Peristaltic Sample Pump Issues

Addressing problems with peristaltic pump speed, tension, and leaks.

Poor Accuracy and Feedback

Troubleshooting inaccurate results by checking pump rate and rinse time.

Poor Detection Limits

Identifying causes of poor detection limits, including optical path issues.

Maintenance for Precision and Detection Limits

Replacing Pump Windings

Guidance on selecting and replacing pump windings based on solvent types.

Preventing Nebulizer Blocking

Methods to prevent nebulizer blockage and maintain performance.

Removing Solids from Nebuliser

Procedures for removing solids and particles from the nebulizer.

Cleaning Glass Mixing Chamber

Cleaning the glass mixing chamber to prevent beading and improve RSDs.

Sample Introduction Spares and Consumables

Spare Parts for Sample Introduction Kits

List of replacement parts for various sample introduction systems.

Related product manuals