25
Troubleshooting
Symptom: No flow (probably cause(s) shown in bold)
Check electrical connections:
1. Is instrument plugged in?
2. Does outlet provide electricity?
3. Is fuse blown? If so, replace.
Is fluid degassed prior to use?
Degass fluid prior to use:
1. Boil.
2. Bubble helium through fluid.
3. Subject fluid to a vacuum.
1. Do not pump fluids with suspended particles (a
particle as small as ten microns can clog a valve).
2. Install an inlet line filter.
3. Flush with liquid detergent or 20% solution of nitric
acid (at max. flow for about 10 minutes), or suck
cleaning fluid through pump with a syringe.
4. Ultrasonicate valve assembly.
Clean filter (clogged filter can create restriction to flow,
causing cavitation).
Is mechanical assembly OK?
Inspect parts of mechanical assembly; is piston broken?,
pushrod frozen in bushing?
Rebuild or replace valves (excessive force used to tighten
fittings to valves or valves to cylinder can cause sapphire
seats to crack, chip, or shatter, thereby inhibiting flow).
Symptom: Erratic flow (probable cause(s) shown in bold)
What is backpressure on pump
Insufficient backpressure, create more pressure on pump so
valves can work properly (install backpressure regulator, or
length of small I.D. tubing).
Is fluid degassed prior to use?
Clean valves as per above, install inlet line filter.
Is there a leak at fitting(s)
Is there a leak at valve
connection?
Rebuild or replace valves.
Symptom: Leakage
Symptom: Steadily decreasing flow rate
Is fluid degassed prior to use?