Shimadzu ICPE-9000 User Manual

Name: Shimadzu ICPE-9000
Brand: Shimadzu
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116 pages

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Shimadzu Multitype ICP Emission Spectrometer

ICPE-9000 Hardware

INSTRUCTION MANUAL

305-34043C

Table of Contents21
Introduction25
Parts27
P R E P Ar at I O N F O R I29
I N S T al L at I O N E29
I N S T al L I N G an D30
Operating Environment and Storage30
Maintenance30
Other Points30
R I N C I P L E S31
F U N D am E N T al S an D31
Definition of Emission Spectrometry31
Principles of Emission Spectrometry31
Intensity Method (Time Integration Method) and Intensity Ratio Method32
Self Absorption32
Background Equivalent Concentration (BEC) and Limit of Detection (LOD)32
P L as M a33
Definition of Plasma33
Principles of ICP33
Features of ICP34
F U N D am E N T al S O F35
Basic Equations for Diffraction Gratings35
Mounting of Spectrometer36
Detector37
Outline38
Principle of Matching Box38
C O N F I G U R at I O N an D39
Block Diagram39
CCD Detector45
Shutter45
U N I T45
Vacuum System45
O O L I N G S y S T E M46
R G O N Gas S Asy S T E M46
Sam P L E I N T R O D U C T I O N S y S T E M47
(Plasma Stand Interior)49
Jac K E T51
Rad I al52
Observation Kit52
Lis T S O F M a in T E N a N C E P a R T S a N D C O N S U M a B Le I T E M S F O R R a D Ia L- V Ie W56
F P O W E R S U P P L y58
O N N E C T O R Pan E L61
S C - 6 1 0 0 F a U T O S am P L E R62
Specifications65
RF Power Supply65
Spectrometer65
Measuring Unit65
Dat a P R O C E S S I N G U N I T S O F T W Ar E66
Measurement Samples66
Qualitative Analysis66
M E T H O D66
User Support67
Instrument Control67
Utilities67
Power Supply Requirements67
Ground67
Argon Gas67
Cooling Water67
Installation Conditions67
Dimensions and Weight67
Options67
Operation69
I C P E - 9 0 0 069
Starting the ICPE-9000 at Installation69
Starting the ICPE-9000 in Daily Use69
Stopping the ICPE-9000 in Daily Use71
Leak Valve Operation (after Vacuum Pump Is Stopped)72
Checking Operation of Safety Devices73
Response in Emergency73
Recovery after Emergency Stop73
Response to Power Failure73
Maintenance75
Replacing and Inspecting Glassware75
Replacing the Torch75
Nebulizer76
Replacing the Chamber76
Cleaning Glassware76
Removing Glass Parts77
Removing the Chamber and Extension Pipe78
Removing the Nebulizer78
Removing the Leveler79
Removing the Torch80
Attaching the Glassware81
Attaching the Torch81
A T T a C H I N G T H E N E B U L I Ze85
A T T a C H I N G T H E N E B U L I Ze R T O T H E C H a M B E85
Replacing the Sample Introduction Tube87
Replacing the Drain Tube87
C L E an I N G an D R E P L Ac E M E N T O F R E F L E C T M I R R O R I N C O O L I N G Jac K E90
C L E an I N G T H E a X I al92
Attaching and Removing the Cooling Jacket93
L E an I N G T H E E N T R an C E W I N D O W96
Rad I al97
E P L Ac I N G T H E Vac U U M P U M P O I L99
Waste Tank100

Brand	Shimadzu
Model	ICPE-9000
Category	Laboratory Equipment
Language	English

Shimadzu ICPE-9000 User Manual

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