Shimadzu TOC-V CPH - Create Calibration Curve File

TOCV-CP_IMshort_Control-ver-2_Rev07F Page 9 of 22
(Software version ≥ 2.00) effective date: September 2007
1. Create a Calibration Curve File
A Calibration Curve File is used to generate a calibration curve. This file includes standard
solution concentration and measurement parameters
- Click “New” in the Calibration Curve tab of the file viewer or
- Select “File” – “New” – “Calibration Curve”
Calibration Curve Wizard –1 System Information
Parameter
Action/Description
System
Select the instrument to be used for measurement
Operator
Name of current user is automatically entered
Date of Creation
Current date and time are automatically entered
Comment
Enter a comment (512 characters minimum)
Calibration Curve Wizard –2 Calibration Curve Type
- to select options that specify the calibration curve type.
[refer to page 12 to see the different applications and consequences of these types]
Parameter
Action/Description
Calibration points are
distributed uniformly
over the calibration
range
Select this option to calculate the calibration point concentration
automatically. The software will calculate the concentrations by
distributing them in equal amounts over the measuring range of the
calibration curve
Edit calibration points
manually
Select the option to enter the calibration point concentration
manually on a subsequent Wizard page, the calibration Points list.
Calibration Curve
according to
DIN 38402/P-51
Select this option to create a calibration curve according to DIN
38402. This type consists 10 calibration points, with 10 injections of
the lowest and highest standards and a single injection of the
intermediates standards
Calibration curve
according to
USP/EP
Select this option to create a calibration curve according to the
USP/EP standards (2 calibration points with concentration 0 and
500 µg/L)
Div. Standard Solutions
/ Fixed Dilution
Allows for manual entry of different standard solution with one
fixed dilution factor
Div. Standard Solutions
Use of different standard solutions, dilution factor is set
automatically if concentration is too high
Dilution from Standard
Solutions
The instrument automatically prepares the standard solutions from a
stock solution that will be used for generating the calibration curve
Calibration Curve Wizard –3 Analysis Information
Parameter
Action/Description
Analysis
Select the analysis type from drop-down list. Depending of the
analysis type the wizard windows for each single parameter appears
Default Sample Name
Enter the default sample name (64 char. Max.) for the calibration
standards
Default Sample ID
Enter the default sample ID (64 char. Max.) for the calibration
standards