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Shimadzu GCMS-QP2010 Series User Manual
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225-1848
1
Mar. 2010
Gas Chromatograph Mass
S
pectrometer
GCMS-QP2010 Series
Operation Guide
For GCMSsolution V
er
. 2.6
2
Table of Contents
Table of Contents
11
Overall Configuration of Gcmssolution
15
Programs
15
Flowchart of Operating Procedure
16
Starting GC/MS
17
Turning on the Power
17
Layout of Operating Areas
18
Inspecting Consumable Items and Maintenance Parts
19
System Configuration
20
Setting the Modules Used for Analysis
20
Checking Column Information
21
Enabling the Modules Used for Analysis
23
Vacuum System Startup
24
Checking for Vacuum Leakage
25
Autotuning
27
Setting Analysis Conditions
27
Executing Autotuning
28
Checking Autotuning Results
31
Creating a Folder
32
Creating a Folder with Data Explorer
32
Qualitative Analysis
34
Creating a Method File
34
Setting Autosampler Parameters
35
Setting GC Parameters
35
Setting MS Parameters
36
Setting Similarity Search Parameters
37
Saving the Method File
39
Repeating Autotuning
39
Sequential Analysis
40
Creating a Batch File
40
Editing a Batch File ^ Ver. 2.5
43
Saving Batch Files
46
Executing Sequential Analysis
47
Analyzing Data
48
Loading Data Files
48
Zoom in on a Peak in the Chromatogram and Displaying Mass Spectra
49
Removing the Background
51
Searching for Similarity ^ Ver. 2.5
52
Displaying Mass Chromatograms
53
Registering Spectra Displayed for Target Compounds ^ Ver. 2.5
54
Editing the Spectrum Process Table
54
Saving Data Files
56
Printing Qualitative Analysis Reports
57
Loading Report Formats
57
Editing Report Formats
58
Outputting Reports
61
Quantitative Analysis
62
Creating a Method File
62
Creating a Compound Table
62
Creating a SIM Table
67
Sequential Analysis
69
Creating a Batch File
69
Editing a Batch File ^ Ver. 2.5
72
Saving Batch Files
72
Executing Sequential Analysis
73
Analyzing Data
74
Checking and Correcting Calibration Curves
74
Re-Quantifying after Correcting a Calibration Curve
81
Checking and Correcting Quantitation Results
83
Printing Quantitative Analysis Reports
87
Creating and Outputting Quantitative Analysis Reports
87
Shutting down GC/MS
90
Vacuum System Shutdown
90
Turning off the Power
91
File Format
92
Appendix B Viewing Help
93
Viewing Help
93
Displaying Help from the Assistant Bar
93
Displaying Help from the Menu Bar
93
Displaying Help with the F1 Key
94
Appendix C Using Data Explorer
95
Appendix D Maintenance
97
Maintenance
97
Easy Stop
99
(Applicable to QP2010 Ultra and QP2010 SE Models)
99
Reset Procedure for Usage Frequencies and Usage Times ^ Ver.2.5
101
Changing Replacement Guidelines for Septa and Glass Inserts
103
Single Analysis (Manual Injection)
106
Appendix F Index Searches
108
Appendix G Displaying Chromatograms
110
Displaying Chromatograms from Fragment Tables
110
Displaying Chromatograms from Mass Spectra
112
Editing Batch Files
113
Adding Batch Files (Batch Queue)
115
Creating Batch Files to Add
115
Adding Batch Files
116
Appendix I Reducing the Carrier Gas Flow Rate after Sequential
119
Reducing the Carrier Gas Flow Rate after Sequential Analysis
119
Creating a Method File that Reduces the Carrier Gas Flow Rate
119
Creating Batch Files
120
Ecology Mode
123
(This Feature Applies to QP2010 Ultra and QP2010 SE Models.)
123
Setting the Mode Manually
123
Setting the Mode Using Batch Processing
124
Printing Reports
126
Printing Images
126
(Printing Spectra and Chromatograms Displayed in Windows)
126
Creating Reports
128
Using Templates
128
Using Previously Created Report Files
129
Manually Setting Report Content
130
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Shimadzu GCMS-QP2010 Series Specifications
General
Brand
Shimadzu
Model
GCMS-QP2010 Series
Category
Measuring Instruments
Language
English
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