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AA-6800F
Shimadzu AA-6800F User Manual
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Shimadzu Atomic Absorption Spectrophotometer
AA-6800F (P/N 206-50500)
AA-6800G (P/N 206-50700)
AA-6650F (P/N 206-51200)
AA-6650G (P/N 206-51300)
INSTRUCTION MANUAL
206-94425T
Sep.
2011
2
Table of Contents
Default Chapter
29
Table of Contents
29
Chapter 1 Overview
35
Overview of AA-6800/6650
36
Specifications
37
Chapter 2 Installation
41
Parts Inspection
42
2.1 Parts Inspection
43
Instrument Placement and Site Requirements
46
Equipment Requirements
48
Power Requirements
48
Water Supply Requirements
48
Gas Requirements
48
Ventilation System
50
Use of an Air Compressor
51
General Precautions for Handling Gas Cylinders
52
Installing Pressure Regulators (Optional) and Checking for Leaks
53
Software Operation Minimum Requirements (to be Provided by User)
55
Assembling the AA-6800/6650
57
Connecting the Drain Tube
57
Assembling the Burner
58
Cable Connections
59
Hose Connections
60
Replacing the AA-6650 Atomizer
61
Installation of PC Software
63
Mounting a Hollow Cathode Lamp
65
Installing the ACF-6800
66
Chapter 3 Instrument Constructions
68
AA-6800/6650 Configurations
68
Operation Switches
68
Hollow Cathode Lamp Turret
69
Deuterium Lamp
70
Burner Module
71
Burner
73
Gas Control Panel
74
Optical System
76
Photometric System
77
Chapter 4 Basic Operation
80
Switching on the Power and Starting up the Software
80
Switching on the Power to Hardware
80
Starting up the Software
81
Software Basic Operation
82
Software Basic Operation (Flame Method)
82
Operation Flowchart (Flame Method)
82
Wizard Selection
83
Element Selection
83
Preparation Parameters
85
Sample ID
88
Sample Selection
89
Connect to Instrument/Send Parameters
90
Optics Parameters
91
Atomizer/Gas Flow Rate Setup (AA-6800)
93
Atomizer/Gas Flow Rate Setup (AA-6650)
95
Software Basic Operation (Furnace Method)
97
Operation Flowchart (Furnace Method)
97
Wizard Selection
98
Element Selection
98
Preparation Parameters
101
Sample ID
106
Sample Selection
107
Connect to Instrument/Send Parameters
108
Optics Parameters
109
Furnace Program
111
Saving the Template
113
Measurement Procedures
114
Measurement Operation (for Flame Method)
114
Measurement Operation (for Furnace Method)
116
Saving/Printing/Deleting the Data
117
Saving the Data
117
Printing the Data
117
Deleting the Data
117
Completing the Measurement
118
Explanation of Main Window
119
Menu Bar
120
Standard Tool Bar
120
Measurement Element Tool Bar
120
Absorbance Digital Display
120
Real Time Graph (and Furnace Program Graph)
120
Peak Profile (Latest Four Measurements and Overlay Display)
122
Calibration Curve Display
123
MRT Worksheet
125
Function Buttons
126
Status Bar
127
Operating the MRT Worksheet
128
Fields of MRT Worksheet
128
Right Mouse Button Menu
132
Right Mouse Button on Summary Table
135
Inserting and Deleting the Measurement Row
135
Active Cell Movement by Shortcut Key and Cell Selection
136
Moving an Active Cell
136
Selecting Cells
136
Copy and Paste
137
Copy
137
Paste
137
Changing Column Width and Column Header Height of MRT Worksheet
138
Igniting and Extinguishing the Flame
139
Operation Locations
139
Safety Precautions Prior to Ignition
139
Igniting and Extinguishing Air-C 2 H 2 , Air (Ar)-H 2 Flames
140
Igniting and Extinguishing N O-C Flame
142
Flame Conditions When Analyzing Organic Solvent Samples
144
Standard Addition Method and Simple Standard Addition Method
145
Setting the [Edit Preparation Parameters] Dialog Box
146
Measurement Procedures on MRT Worksheet
148
Conditions and Operation for Flame Emission Analysis
150
Optics Parameters] Page
150
Atomizer/Gas Flow Rate Setup] Page
152
Aa-6800
152
Aa-6650
154
Line Search and Beam Balance
156
Setting the Optimum Conditions for Fuel Gas Flow Rate and Burner Height (AA-6800)
157
Setting the Optimum Condition of Burner Height
157
Setting the Optimum Condition of Fuel Gas Flow Rate
158
Chapter 5 Functions of Operation Menu
162
Wizard Selection] Dialog Box
162
Wizard] Page
162
Recent Files] Page
162
Recent Templates] Page
162
File]
163
New]
163
Open]
164
Save]
164
Save as
165
Additional Load]
165
File Export
166
Export Items]
166
Auto Save]
167
Print Data/Parameters
169
Print Table Data
170
Print Style]
170
5.2.11.1 [Print Style Setup] Page
170
5.2.11.3 [Font] Page
171
Print Setup]
172
Recent Files
172
Exit]
172
Edit]
173
Insert Row]
173
Delete Rows]
173
Import Other Schedule]
173
Collective Edit]
173
Remeasure Selected Range]
173
Clear Measurement Result]
174
Copy]
174
Paste]
174
Refer to Parameters]
175
Parameters]
177
Element Selection] Page
177
Cookbook] Page
178
Template] Page
179
Preparation Parameters] Page
180
Weight Correction Factors
182
Preparation Parameters]-[Standard Samples]
182
Preparation Parameters]-[Unknown Samples]
183
Preparation Parameters]-[Blank Samples]
183
Mixing Setup and Reagent Setup
184
Coating and Boost Cycles (Only for Furnace Method)
185
Repeat Measurement Conditions
186
Sample ID] Page
186
Sample Selection] Page
188
Connect to Instrument/Send Parameters] Page
188
Optics Parameters] Page
189
Lamp Pos. Setup] Button
192
Warmup Lamp] Button
192
Line Search] Button
193
Atomizer/Gas Flow Rate Setup] Page (for Flame Method by AA-6800)
194
Atomizer Position
194
Burner Position Auto] Button
196
Fuel Gas Flow Rate
197
Gas Flow Auto] Button
198
Atomizer/Gas Flow Rate Setup] Page (for Flame Method by AA-6650)
199
Atomizer Position
199
Fuel Gas Flow Rate
200
Edit Parameters]
208
Default Parameters]
222
Instrument]
223
Help]
245
Chapter 6 Maintenance
248
Atomizer Position Adjustment
248
Burner Positioning Adjustment
248
Furnace Position Adjustment
250
Burner Maintenance
251
Cleaning the Burner Head
251
Cleaning the Nebulizer
252
Nebulizer Maintenance
252
Replacing the Polyethylene Tube
254
Washing the Chamber
254
Checking for Gas Leaks in Tubing
255
Replacing Procedures of Deuterium Lamp
256
Replacing the Deuterium Lamp
256
Specifications of Deuterium Lamp
256
Maintenance Parts
258
Autosampler
260
For Flame Analysis
260
For Furnace Analysis (for GFA-EX7)
260
Special Accessories
260
Hollow Cathod Lamps (Single Element Lamps)
261
Hollow Cathode Lamps (Single Element Lamps, Usable for SR Method)
263
Hollow Cathod Lamp (Multi-Element Lamps)
264
Other Accessories
264
Chapter 7 Appendix
266
Measurement Conditions Table for Flame Atomic Absorption Analysis
266
Analysis Line Wavelength Table for Flame Emission Analysis
269
Graphite Tube Type Selection in Furnace Method
270
When Using a High Density Graphite Tube
270
When Using a Pyrolitic Coating Graphite Tube
271
When Using the Platform Type Tube
271
Error Messages
274
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Shimadzu AA-6800F Specifications
General
Brand
Shimadzu
Model
AA-6800F
Category
Measuring Instruments
Language
English
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