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Shimadzu AA-6800F User Manual

Shimadzu AA-6800F
302 pages
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Shimadzu Atomic Absorption Spectrophotometer
AA-6800F (P/N 206-50500)
AA-6800G (P/N 206-50700)
AA-6650F (P/N 206-51200)
AA-6650G (P/N 206-51300)
INSTRUCTION MANUAL
206-94425T
Sep. 2011

Table of Contents

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Shimadzu AA-6800F Specifications

General IconGeneral
BrandShimadzu
ModelAA-6800F
CategoryMeasuring Instruments
LanguageEnglish

Summary

Precautions for Safe Operation

General Precautions

Comprehensive precautions for safe operation of the atomic absorption spectrophotometer.

Precautions on Handling High Pressure Gas

Safety measures for handling high-pressure gas cylinders used with the instrument.

Action in the Case of Fuel Gas Leakage

Procedures to follow in the event of a fuel gas leak detected by the instrument.

Precautions on Handling Hollow Cathode Lamp

Safety guidelines for handling and disposing of hollow cathode lamps.

Precautions on Handling Deuterium (D2) Lamp

Safety guidelines for handling and disposing of deuterium lamps.

Handling Waste Liquid

Procedures for safely handling and disposing of waste liquid generated during measurements.

Warning Marking on the Equipment

Explanation of warning labels found on the equipment and their meanings.

Emergency Action

Steps to take in case of an emergency or abnormal condition with the instrument.

Inspection Procedure in Case of Flashback

Steps for inspecting the instrument after a flashback incident occurs.

Moving or Transporting the AA-6800/6650

Instructions for safely moving or transporting the AA-6800/6650 instrument.

Warning on Sample to Be Measured

Warning about measuring explosive samples due to potential risks.

Safety Service Parts List

List of service parts, their replacement intervals, and checking procedures.

Daily Check List

Daily checklist items to ensure safety and proper functioning before operation.

Action for Environment (WEEE)

Information regarding the disposal of electronic equipment in the European Union.

Regulatory Information

Compliance information related to European directives for the product.

Electromagnetic Compatibility

Information on the instrument's compliance with electromagnetic compatibility standards.

Chapter 1 Overview

1.1 Overview of AA-6800/6650

General introduction to the AA-6800/6650 atomic absorption spectrophotometer.

1.2 Specifications

Technical specifications and performance characteristics of the AA-6800/6650.

Chapter 2 Installation

2.1 Parts Inspection

Verification of included standard accessories and system configurations.

2.2 Instrument Placement and Site Requirements

Guidelines for selecting an appropriate installation site and placement of the instrument.

2.3 Equipment Requirements

Necessary power, water supply, and gas requirements for operating the instrument.

2.4 Assembling the AA-6800/6650

Step-by-step instructions for assembling the AA-6800/6650 instrument components.

2.5 Mounting a Hollow Cathode Lamp

Procedure for correctly mounting a hollow cathode lamp into the instrument.

2.6 Installing the ACF-6800

Instructions for installing the ACF-6800 flame unit as an accessory.

Chapter 3 Instrument Constructions

3.1 AA-6800/6650 Configurations

Overview of the main unit's configurations and operation switches.

Chapter 4 Basic Operation

4.1 Switching On the Power and Starting Up the Software

Procedures for powering on the hardware and starting the instrument software.

4.2 Software Basic Operation

Step-by-step guide to basic operations using the software's Wizard function.

4.3 Measurement Procedures

Detailed steps for performing measurements using both manual and automated methods.

4.8 Igniting and Extinguishing the Flame

Procedures and safety precautions for igniting and extinguishing the flame.

4.9 Standard Addition Method and Simple Standard Addition Method

Explanation and procedures for using standard addition and simple standard addition methods.

4.10 Conditions and Operation for Flame Emission Analysis

Specific conditions and procedures for performing flame emission analysis.

4.11 Setting the Optimum Conditions for Fuel Gas Flow Rate and Burner Height (AA-6800)

How to optimize fuel gas flow rate and burner height for improved sensitivity.

Chapter 5 Functions of Operation Menu

5.1 [Wizard Selection] Dialog Box

Overview of the Wizard selection dialog box and its available options.

5.2 [File]

Functions related to file management, including opening, saving, and exporting data.

5.5 [Parameters]

Summary of parameter setup functions and available Wizards.

5.6 [Edit Parameters]

Detailed settings for individual measurement parameters outside of the Wizard.

5.8 [Instrument]

Functions related to controlling and configuring the instrument hardware.

5.9 [Help]

Accessing help resources and software information.

Chapter 6 Maintenance

6.1 Atomizer Position Adjustment

Procedures for adjusting the burner and furnace positions for optimal performance.

6.2 Burner Maintenance

Cleaning and maintenance procedures for the burner head and nebulizer.

6.3 Checking for Gas Leaks in Tubing

Methods for checking gas lines for leaks to ensure safe operation.

6.4 Replacing the Deuterium Lamp

Step-by-step guide for replacing the deuterium lamp.

6.5 Maintenance Parts

List of replacement parts and their recommended replacement intervals.

Chapter 7 Appendix

7.1 Measurement Conditions Table for Flame Atomic Absorption Analysis

Table of recommended measurement conditions for various elements in flame analysis.

7.3 Graphite Tube Type Selection in Furnace Method

Guidance on selecting the appropriate graphite tube type for furnace measurements.

7.4 Error Messages

Troubleshooting guide listing error messages and their corresponding remedial measures.

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