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CEM MARSXpress Plus - User Manual

CEM MARSXpress Plus
30 pages
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MARSXpress Plus
110 mL Microwave Digestion Vessel
Manual

Questions and Answers

  • C
    Carol NewtonAug 5, 2025
    Why does a TempGuard message appear during a run on my CEM MARSXpress Plus?
    • K
      Kari HebertAug 6, 2025
      If a TempGuard message appears during a run with your CEM Laboratory Equipment, it could be because some vessels are hotter than others. Also, avoid mixing old and new liners; run them in separate turntables.
  • K
    kaguilarAug 13, 2025
    Why is my CEM MARSXpress Plus Laboratory Equipment experiencing excessive venting?
    • H
      Hannah StewartAug 13, 2025
      If your CEM Laboratory Equipment experiences excessive venting, it could be due to several reasons. First, check that the "Sample Type” selected in the method is correct; “Organic” is recommended for most samples. Also, ensure the vessel plug is correctly placed on top of the liner before securing it with the cap. Finally, verify that the vessels are properly torqued using the provided torque tool.
  • S
    Stephanie JohnsonAug 19, 2025
    What to do if I see uneven bar graphs during a run with my CEM Laboratory Equipment?
    • N
      Nathaniel JacksonAug 19, 2025
      Uneven bar graphs during a run with your CEM Laboratory Equipment can be caused by several factors. Ensure that the samples have similar properties and weights, or use the same sample in all vessels with similar amounts. Also, make sure you're using the same acid(s) and acid volume in each vessel. Finally, consider that some vessels might be hotter than others. Also, consider that some vessels may contain acid blanks.
  • K
    Kristina DonaldsonAug 28, 2025
    How to address sleeve appearance changes in CEM MARSXpress Plus Laboratory Equipment?
    • L
      Lauren JohnsonAug 28, 2025
      If the sleeve of your CEM Laboratory Equipment has turned white or is stained on the ends, replace it. To prevent sleeve damage, avoid high temperatures for extended periods. If the sleeve comes into contact with acid, wipe it with a damp cloth and allow it to dry.

Summary

Safety

Safety Notations

Explains the use of three safety alert words (NOTE, CAUTION, WARNING) and their meanings.

Introduction

About the MARSXpress Plus Vessels

Describes the MARSXpress Plus vessel, its applications, and compatibility with MARS 6 systems.

Important Safeguards

Operating Parameters

Details maximum acid volume, temperature, hold time, and sample weight for MARSXpress Plus vessels.

Microwave Safeguards

Provides essential safety guidelines for operating the MARS 6 microwave digestion system.

Sample Preparation Safeguards

Outlines safe practices for preparing samples before microwave digestion.

Vessel Safeguards

Lists precautions for using, assembling, and conditioning MARSXpress Plus vessels and components.

Unsuitable Compounds for Digestion

Highlights chemical compounds that should not be digested in closed vessels due to hazard.

Vessel and Accessories Overview

Vessel Components

Details the individual components of the MARSXpress Plus vessels, including liners, plugs, and caps.

System Accessories

Presents images and names of optional accessories for the MARSXpress Plus system.

New Liner, Plug, and Cap Conditioning

Nitric Acid Conditioning

Step-by-step guide for conditioning liners, plugs, and caps for use with nitric acid.

Non-Nitric Acid Conditioning

Step-by-step guide for conditioning liners, plugs, and caps for non-nitric acid applications.

Perform a Digestion

Vessel Assembly

Instructions on how to correctly assemble the MARSXpress Plus vessels before loading into the turntable.

Turntable Setup

Guides on how to correctly load the assembled vessels and turntable into the MARS 6 cavity.

Load and Run Method

Steps for loading the prepared samples and running a digestion method on the MARS 6.

Vessel Removal

Cleaning and Inspection

Liner, Plug, and Cap Cleaning

Procedures for cleaning and inspecting the vessel liners, vent plugs, and caps.

Liner Bake-out Procedure

Describes the bake-out process to remove residual acid vapors from Teflon liners.

Sleeve Maintenance

Guidance on cleaning, inspecting, and maintaining the vessel sleeves.

Turntable Cleaning

Instructions for cleaning and maintaining the MARSXpress Plus turntable.

Vessel Distribution

Methods

Create One Touch Method

Step-by-step guide to programming custom One Touch digestion methods on the MARS 6.

Fiber Optic Temperature Control (optional)

Fiber Optic Probe Installation

Procedure for connecting and configuring the fiber optic probe for temperature measurement.

Fiber Optic Verification

How to verify the accuracy of the fiber optic probe's temperature readings.

Fiber Optic Probe Care

Best practices for handling and storing the fiber optic temperature probe.

Routine Maintenance

Routine Maintenance: After Every Use

Tasks to perform immediately after each use of the MARSXpress Plus vessels.

Routine Maintenance: As Needed

Maintenance procedures to be performed when specific issues arise or as required.

Routine Maintenance: Annually

Annual service recommendations for the MARSXpress Plus system.

Troubleshooting

Troubleshooting: Problems and Solutions

Lists common issues encountered with MARSXpress Plus and their corresponding solutions.

Technical Assistance

Technical Assistance: Applications Support

Information on how to get application-specific help and resources from CEM.

Technical Assistance: Technical Support

Contact details for obtaining technical support for the MARSXpress Plus system.

CEM MARSXpress Plus Specifications

General IconGeneral
TypeMicrowave Digestion System
Vessel Capacityup to 40 vessels
Power1800 Watts
Frequency2450 MHz
Temperature RangeUp to 300 °C
Pressure Rangeup to 800 psi
Cavity MaterialStainless Steel
DisplayTouchscreen
Cooling SystemIntegrated cooling system
Pressure ControlYes
Safety FeaturesOver-temperature protection, over-pressure protection
Power Output1800 W
Voltage Requirements220-240 V
Temperature ControlYes

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