Metrohm 813 - Conditions to be Met

3 Operation
813 Compact Autosampler
29
Sample method for the 746 VA Trace Analyzer:
Instructions t/s Main parameters Auxiliary parameters
------------- ----- ------------------------- ------------------------
1 STIR Rot.speed 2000 /min
2 PURGE
3 SMPL/M V.fraction mL V.total L
4 SETCTRL 1.0 Code *****1** Message
5 SETCTRL Code *****0** Message
6 REM 30.0 move to sample
7 SETCTRL 1.0 Code *****1** Message
8 SETCTRL Code *****0** Message
9 REM 300.0 transfer sample
10 SETCTRL 1.0 Code *****1** Message
11 SETCTRL Code *****0** Message
12 REM stop pump
13 DOS>M Soln.name Buffer V.add 2.000 mL
14 PURGE 90.0
15 (ADD
16 STIR Rot.speed 2000 /min
17 PURGE 30.0
18 (REP
19 SEGMENT Segm.name NiCoAdSV
20 REP)1
21 ADD>M Soln.name Standard V.add 0.010 mL
22 ADD)2
23 RINSE Cycles 1 V.rinse 20.000 mL
24 SETCTRL 1.0 Code *****1** Message
25 SETCTRL Code *****0** Message
26 REM 20.0 move to rinsing position
27 SETCTRL 1.0 Code *****1** Message
28 SETCTRL Code *****0** Message
29 REM 300.0 rinse tubes
30 SETCTRL 1.0 Code *****1** Message
31 SETCTRL Code *****0** Message
32 REM stop pump
33 RINSE Cycles 1 V.rinse 40.000 mL
34 RINSE Cycles 2 V.rinse 15.000 mL
35 END
3.7.3 Conditions to be met
For the correct intercommunication of the 813 Compact Auto-
sampler and the 746 VA Trace Analyzer the following conditions
must be met:
• Method 2 of the 813 Compact Autosampler has to be se-
lected.
• Always start the method of the 813 Compact Autosampler
first, then you can start the 746 VA Trace Analyzer.
• Ensure that the control line 2 (Remote output 2) of the 746
VA Trace Analyzer is reset (inactive state) before you start the
sample series.