119
Agilent 5977B Series MSD
Operating Manual
Agilent Technologies
5
Operating in CI Mode
General Guidelines 120
CI Autotune 121
To Operate the CI MSD 123
To Pumpdown the MSD in CI Mode 124
To Set Up the Software for CI Operation 125
To Operate the Reagent Gas Flow Control Module 127
To Set Up Methane Reagent Gas Flow 130
To Use Other Reagent Gases 132
To Perform a PCI Autotune (Methane Only) 135
To Perform an NCI Autotune (Methane Reagent Gas) 137
To Verify PCI Performance 139
To Verify NCI Performance 140
To Monitor CI Mode High Vacuum Pressure 141
This chapter provides information and instructions for operating the
5977B Series CI MSDs in CI mode. Most of the information in the preceding
chapter is also relevant.
Most of the material is related to methane CI but one section discusses the use
of other reagent gases.
The software contains instructions for setting the reagent gas flow and for
performing CI autotunes. Autotunes are provided for PCI with methane
reagent gas and for NCI with any reagent gas.
If you are using the Agilent Intuvo 9000 Gas Chromatograph with your MS,
Chemical Ionization (CI) and the JetClean system are not currently supported.
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