28 Advanced Operation
3 Method Development
Overview
Figure 10 shows the typical workflow for developing a
headspace sampler method.
Figure 10 Workflow for method development
This chapter describes techniques to create and refine a
method, using the available method parameters and method
features of the 7697A HS. It describes all the method
parameters available, and discusses how various parameters
impact an analysis. This chapter assumes basic familiarity
with the HS as described in the Operation guide. The
Operation guide also includes many useful procedures and
instructions.
Start Up the Headspace
Sampler.
Configure.
Create Method.
Prepare Samples.
Load Samples.
Create Sequence.
Start.
Evaluate.
If Needed, Refine
Method.
Re-evaluate.
If needed, consider
MHE/MHC.
If Needed, Optimize.