36 G7200-90210 (Rev. A) MassHunter Workstation Quick Start Guide
4 On the Select Sample Types (or Select QC Items, if the Intelligent Sequence
software is installed) dialog box, set the following parameters, then click
OK:
a Configure the list of Selected QC Items on the right to contain Sample,
SQStd, SQBlk, and SQISTD.
b Depending on the method you started with, you may have to use the
Add- > and <- Remove buttons to create the desired list.
5 Set the Data Acquisition method parameters:
a On the Acquisition Mode dialog box, mark the Spectrum option and click
OK.
b On the Spectrum Acquisition Parameters dialog box, click the Mass
Scale button.
c On the Masses dialog box:
• Click the Clear All button.
• Select all mass numbers by double- clicking on the top, middle, and
bottom rows, then click OK.
d Make the following additional selections on the Spectrum Acquisition
Parameters dialog box, then click OK:
• Select Semi Quant (6) for the Peak Pattern.
• Clear the Set every Mass option, then set the per Point Integration
time to 0.05 or 0.1 sec.
• Set the Repetition count to 1.
e On the Peristaltic Pump Program dialog box, set the following
parameters, then click OK.
• Before Acquisition: Uptake Speed: 0 rps, Uptake Time: 0 sec,
Stabilization Time: 70 sec
• After Acquisition (Rinse Port): Rinse time: 30 sec
• After Acquisition (Rinse Vial)
See online help for more information on these parameters and on the
optional features: Intelligent Rinse and Execute Pre- emptive Rinse.
6 To save the method:
a On the Method Save Options dialog box, mark all items, and click OK.
b On the Save Method As dialog box, enter a name for the method, and
click OK
.
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