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ATAGO PRM-2000 A User Manual

ATAGO PRM-2000 A
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34
(2-2) An Example of How to Create Data Table
To create a data table, first prepare sample solutions of different concentrations.
Then, use an accurate refractometer to measure their refractive indices at different temperatures.
This chapter explains the procedure of creating a data table for caustic soda (NaOH) solutions.
[Items to prepare]
An accurate and precise refractometer (preferably a refractometer equipped with a temperature
regulator function)
A circulating constant temperature bath (unnecessary for a refractometer with an internal constant
temperature feature)
Sample solutions of different concentrations (example: NaOH solutions)
Prepare 6 NaOH solutions diluted with purified water to the following concentrations:
0.00%, 10.00%, 20.00%, 30.00%, 40.00%, 50.00%
Use purified water as the 0.00% sample.
Table 11-5 is the data of conversion between temperature and refractive index of water.
Table 11-5
Temperature
5˚C
10˚C
20˚C
30˚C
40˚C
50˚C
60˚C
nD
1.33388
1.33369
1.33299
1.33194
1.33061
1.32904
1.32725
Next, measure the other 5 NaOH solutions with the refractometer.
Change the temperature to 5.0˚C, 10.0˚C, 20.0˚C, 30.0˚C, and 40.0˚C and measure.
Record the concentration, temperature, and Refractive Index.
m For a data table, use a measurement range that is wider than the range of the actual sample
the PRM-2000α will be measuring.
Accordingly, the user scale in this case has the temperature range of 5 to 40˚C and the
concentration range of 0.00 to 50.00%.
Enter the concentration, Refractive Index, and temperature, following the data table format.
The Table 11-6 below is the compilation of the measurement results of the NaOH solutions expressed in
the format of the Table 11-5.
How to read the Table 11-6
The 20.00% solution measures nD 1.343687 at 20˚C.
The 30.00% solution measures nD 1.349789 at 10˚C.
Table 11-6
0.00%
10.00%
20.00%
30.00%
40.00%
50.00%
0.0
5.0˚C
1.33388
1.339374
1.344782
1.350106
1.355346
1.3605
0.0
10.0˚C
1.33369
1.339141
1.344507
1.349789
1.354987
1.3601
0.0
20.0˚C
1.33299
1.338381
1.343687
1.348909
1.354047
1.3591
0.0
30.0˚C
1.33194
1.337277
1.342531
1.347703
1.352793
1.3578
0.0
40.0˚C
1.33061
1.335935
1.341177
1.346335
1.351409
1.3564
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Fill in any blank cells with "0.0"

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ATAGO PRM-2000 A Specifications

General IconGeneral
BrandATAGO
ModelPRM-2000 A
CategoryMeasuring Instruments
LanguageEnglish

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