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Bruker Ascend 400'54 User Manual

Bruker Ascend 400'54
102 pages
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Version
Innovation with Integrity
400‘54 Ascend
04
User Manual
NMR
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Bruker Ascend 400'54 Specifications

General IconGeneral
Magnet TypeSuperconducting
Magnetic Field Strength9.4 Tesla
Frequency400 MHz
Temperature Range-150°C to +150°C
Magnet Bore54 mm
ConsoleAvance Neo
SoftwareTopSpin
Nucleus1H, 13C, 15N, 31P
Sample TypeLiquids, solids
Probe Typebroadband
Sample Diameter5 mm

Summary

Contact Information

Manufacturer Contact Details

Details for Bruker BioSpin AG, including address, phone, fax, and email.

Introduction to the Ascend Magnet System

General Information and System Overview

Provides essential info on handling the magnet system and its components.

Liability, Service, Warranty, and Copyright

Outlines manufacturer's liability, support, warranty terms, and publication rights.

General View of Magnet System

Illustrates and describes the main components of the NMR magnet system.

Safety Guidelines for Magnet System Operation

Approved Persons

Defines qualifications for personnel operating or servicing the magnet system.

Customer Responsibilities

Details the customer's duties to ensure safe operation and maintenance of the system.

Hazard Indicators and Key Words

Explains the meaning of DANGER, WARNING, CAUTION, and NOTICE indicators.

Residual Risks: Persons and Intended Use

Addresses risks associated with personnel and the system's intended application.

Residual Risks: Safety Devices and Spare Parts

Highlights risks related to safety devices and the use of approved spare parts.

Signs, Labels, and Magnetic Field Risks

Covers risks from unreadable signs, labels, and exposure to magnetic fields.

Cryogenic Agents and Electrical Risks

Details hazards associated with cryogenic agents and electrical components.

Quench and Gas Under Pressure Risks

Addresses risks during a magnet quench and from pressurized gases within the system.

Low Temperature and Ignition/Explosion Risks

Covers hazards from low temperatures and spontaneous ignition/explosion risks.

Tilting and Heavy Weight Risks

Details risks associated with system tilting and handling heavy components.

Transportation Safety Precautions

Provides precautions for safe transport, covering packing and handling.

Personal Protective Equipment (PPE)

Specifies required PPE for safe operation, including goggles, gloves, clothes, and shoes.

Safety Devices Overview and Details

Illustrates and describes the cryostat's safety devices like quench valves and drop-off plates.

Emergency Procedures and Fire Notification

Outlines actions during emergencies and requirements for fire department notification.

Transportation Procedures and Safety

Transportation Safety and Packaging

Covers safety guidelines for transporting the system and details on its original packaging.

Transport Inspection and Disposal

Details how to inspect deliveries for damage and procedures for box disposal.

Handling and Lifting Procedures

Provides instructions for transportation using forklifts, pallet jacks, and cranes.

Storing and Final Disposal

Guidelines for storing the cryostat before installation and information on final disposal.

Assembling the Magnet System

Assembling Safety Guidelines

Specifies that only approved personnel should perform assembly procedures.

Operation of the Magnet System

Operation Safety Warnings

Lists critical safety warnings for operating the magnet system.

Setting Magnet System into Operation

Describes how to start and stop the magnet stand using the pneumatic controller.

Troubleshooting Guide

Troubleshooting Safety and Qualifications

Highlights safety precautions and required qualifications for troubleshooting tasks.

Issues During Transportation and Assembling

Covers common problems encountered during transportation and assembly, with solutions.

Issues During Cooling Down

Addresses problems related to the cooling process, including liquid nitrogen transfer and vacuum levels.

Issues During Energizing, Shimming, Operation, De-energizing

Details problems during magnet energizing, shimming, standard operation, and de-energizing.

Troubleshooting Post-Quench Procedures

Provides steps to follow after a magnet quench event, including safety checks and refills.

Maintenance Procedures

Maintenance Safety and PPE

Lists safety warnings and required PPE for performing maintenance tasks on the system.

Cleaning and Maintenance Schedule

Describes cleaning procedures and provides a timetable for routine maintenance checks.

Disassembling the Magnet System

Disassembling Safety

States that disassembly must only be performed by authorized Bruker Service personnel.

Appendix: Reference Materials

Warning Signs Reference

Lists and categorizes various warning signs used in the manual and on the equipment.

Figures and Tables Index

Lists all figures and tables included in the appendix for easy reference.

Glossary and Abbreviations

Defines key terms and acronyms used throughout the manual for clarity.

Technical Data Specifications

Provides detailed specifications and environmental conditions for the cryostat and magnet system.

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